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60.103448 Tz (2006. ) Tj 17.748621 0 Td 53.224138 Tz (Nanofilms. ) Tj 3.388966 0 Td 56.321839 Tz (Chemistry ) Tj 3.215172 0 Td 56.12069 Tz (of ) Tj 0.782069 0 Td 50.287356 Tz (Materials ) Tj 2.867586 0 Td 50.689655 Tz (\(2010\), ) Tj 2.302759 0 Td 48.275862 Tz (22\(7\), ) Tj 1.955172 0 Td 54.639498 Tz (2248-2254.* ) Tj 45.714286 0 0 45.714286 0 1820.253911 Tm 28.48125 0 Td 53.472222 Tz (Haupt, ) Tj 2.14375 0 Td 51.041667 Tz (Karsten; ) Tj 2.7125 0 Td 58.789062 Tz (Mosbach, ) Tj 3.0625 0 Td 51.649306 Tz (Klaus; ) Tj 2.121875 0 Td 53.693182 Tz (Molecularly ) Tj 3.7625 0 Td 53.06713 Tz (Imprinted ) Tj 3.10625 0 Td 56.510417 Tz (Polymers ) Tj 44.693878 0 0 44.693878 0 1777.309771 Tm 7.338813 0 Td 57.800609 Tz (\(51\) ) Tj 2.237443 0 Td 53.139269 Tz (Int. ) Tj 1.454338 0 Td 58.422121 Tz (Cl. ) Tj 18.078539 0 Td 58.422121 Tz (and ) Tj 1.230594 0 Td 55.190259 Tz (Their ) Tj 1.834703 0 Td 64.63724 Tz (Use ) Tj 1.36484 0 Td 44.748858 Tz (in ) Tj 0.805479 0 Td 57.427702 Tz (Biomimetic ) Tj 3.647032 0 Td 52.207002 Tz (Sensors; ) Tj 2.72968 0 Td 64.14003 Tz (Chem. ) Tj 2.17032 0 Td 49.223744 Tz (Rev.; ) Tj 1.678082 0 Td 50.342466 Tz (Jun. ) Tj 1.454338 0 Td 54.444444 Tz (2000; ) Tj 1.946575 0 Td 50.342466 Tz (100; ) Tj 40.714286 0 0 40.714286 0 1738.685579 Tm 10.536842 0 Td 65.497076 Tz (C08. ) Tj 2.259649 0 Td 85.964912 Tz (7/8 ) Tj 5.673684 0 Td 65.951917 Tz (\(2006.01\) ) Tj 13.484211 0 Td 61.812865 Tz (2495-2504. ) Tj 45.571429 0 0 45.571429 0 1692.863316 Tm 9.413793 0 Td 94.479276 Tz (C83/28 ) Tj 7.087774 0 Td 58.922559 Tz (\(2006.01\) ) Tj 12.047022 0 Td 52.420759 Tz (Marty, ) Tj 2.084639 0 Td 53.944619 Tz (Jean ) Tj 1.514107 0 Td 49.634274 Tz (Daniel; ) Tj 2.260188 0 Td 59.561129 Tz (Mauzac, ) Tj 2.677116 0 Td 58.973354 Tz (Monique; ) Tj 3.028213 0 Td 56.078022 Tz (Molecular ) Tj 3.203762 0 Td 49.206802 Tz (Imprinting: ) Tj 3.510972 0 Td 47.54441 Tz (State ) Tj 45.102041 0 0 45.102041 0 1651.942085 Tm 9.511765 0 Td 105.932629 Tz (CSF ) Tj 2.172851 0 Td 59.125189 Tz (2/46 ) Tj 4.988688 0 Td 59.53578 Tz (\(2006.01\) ) Tj 12.172398 0 Td 59.125189 Tz (of ) Tj 0.776018 0 Td 50.502765 Tz (the ) Tj 1.086425 0 Td 52.966315 Tz (Art ) Tj 1.130769 0 Td 60.356963 Tz (and ) Tj 1.285973 0 Td 48.891983 Tz (Perspectives; ) Tj 4.035294 0 Td 55.429864 Tz (Adv. ) Tj 1.574208 0 Td 56.661639 Tz (Polym. ) Tj 2.261538 0 Td 43.604827 Tz (Sci., ) Tj 1.529864 0 Td 54.690799 Tz (2005; ) Tj 1.906787 0 Td 50.810709 Tz (172; ) Tj 1.529864 0 Td 47.300151 Tz (1-35. ) Tj 45.595238 0 0 45.595238 0 1605.127067 Tm 9.408877 0 Td 73.10705 Tz (C07C38L/00 ) Tj 7.084073 0 Td 58.89179 Tz (\(2006.01\) ) Tj 12.062663 0 Td 45.082681 Tz (Li, ) Tj 0.986945 0 Td 63.603133 Tz (Wuke; ) Tj 2.171279 0 Td 45.082681 Tz (Li, ) Tj 1.030809 0 Td 54.373368 Tz (Songjun: ) Tj 2.895039 0 Td 55.642588 Tz (Molecular ) Tj 3.224021 0 Td 49.513411 Tz (Imprinting: ) Tj 3.53107 0 Td 84.073107 Tz (A ) Tj 0.701828 0 Td 46.707282 Tz (Versatile ) Tj 2.741514 0 Td 54.830287 Tz (Tool ) Tj 1.535248 0 Td 48.738033 Tz (for ) Tj 45.054945 0 0 45.054945 0 1565.523939 Tm 9.521707 0 Td 106.04336 Tz (CSF ) Tj 2.552439 0 Td 61.036585 Tz (2/30 ) Tj 4.616585 0 Td 59.598013 Tz (\(2006.01\) ) Tj 12.207317 0 Td 50.107169 Tz (Separation, ) Tj 3.529024 0 Td 53.902439 Tz (Sensors ) Tj 2.441463 0 Td 60.420054 Tz (and ) Tj 1.265122 0 Td 48.089431 Tz (Catalysis; ) Tj 3.085122 0 Td 56.412602 Tz (Adv. ) Tj 1.575854 0 Td 57.337398 Tz (Polym. ) Tj 2.286098 0 Td 42.910569 Tz (Sci.; ) Tj 1.487073 0 Td 51.788618 Tz (Oct. ) Tj 1.531463 0 Td 46.856369 Tz (19, ) Tj 1.043171 0 Td 54.747967 Tz (2006; ) Tj 48.214286 0 0 48.214286 0 1520.519251 Tm 6.802963 0 Td 52.716049 Tz (\(52\) ) Tj 2.094815 0 Td 55.308642 Tz (U.S. ) Tj 1.534815 0 Td 53.004115 Tz (Cl. ) Tj 1.41037 0 Td 32.079012 Tz (......................... ) Tj 5.288889 0 Td 58.534979 Tz (427/507,522/81: ) Tj 5.517037 0 Td 57.037037 Tz (522/180; ) Tj 4.334815 0 Td 50.987654 Tz (206; ) Tj 1.493333 0 Td 48.82716 Tz (191-210. ) Tj 48.571429 0 0 48.571429 0 1480 Tm 10.747059 0 Td 56.617647 Tz (427/496; ) Tj 2.923529 0 Td 57.046569 Tz (427/506; ) Tj 2.944118 0 Td 56.617647 Tz (427/508; ) Tj 2.944118 0 Td 56.188725 Tz (427/512; ) Tj 2.902941 0 Td 57.046569 Tz (427/517; ) Tj 49.047619 0 0 49.047619 0 1439.446882 Tm 10.071845 0 Td 56.067961 Tz (427/518; ) Tj 2.895146 0 Td 55.643204 Tz (427/520; ) Tj 2.915534 0 Td 56.067961 Tz (427/256; ) Tj 2.915534 0 Td 55.643204 Tz (427/287; ) Tj 2.874757 0 Td 54.708738 Tz (427/407.1; ) Tj 12.192233 0 Td 55.295675 Tz (\(Continued\) ) Tj 44.761905 0 0 44.761905 0 1396.928475 Tm 11.03617 0 Td 61.43617 Tz (427/409: ) Tj 3.194681 0 Td 59.574468 Tz (428/411.1; ) Tj 3.797872 0 Td 61.43617 Tz (428/419: ) Tj 3.17234 0 Td 54.609929 Tz (428/.457; ) Tj 3.194681 0 Td 61.43617 Tz (428/461; ) Tj 9.673404 0 Td 49.335106 Tz (inap ) Tj 66.623377 0 0 66.623377 0 1345.972933 Tm 8.690643 0 Td 40.9641 Tz (428/463: ) Tj 2.131384 0 Td 42.348928 Tz (568/67:568/68: ) Tj 3.707407 0 Td 40.025991 Tz (568/77; ) Tj 1.876218 0 Td 40.9641 Tz (526/286; ) Tj 3.122027 0 Td 104.234351 Tz (\(i. ) Tj 1.996296 0 Td 87.556855 Tz (Eli ) Tj 2.686745 0 Td 101.732727 Tz (St. ) Tj 2.041326 0 Td 74.214858 Tz (Mction ) Tj 2.716764 0 Td 37.83707 Tz (Corless: ) Tj 2.071345 0 Td 40.526316 Tz (Brian ) Tj 1.485965 0 Td 60.038986 Tz (R ) Tj 74.155844 0 0 74.155844 0 1297.920074 Tm 7.039229 0 Td 37.084063 Tz (264,426, ) Tj 1.928371 0 Td 42.70286 Tz (264446; ) Tj 1.914886 0 Td 40.748496 Tz (264448,264,458.264/405; ) Tj 8.387741 0 Td 91.024518 Tz (E. ) Tj 1.955342 0 Td 51.692936 Tz (XR ) Tj 0.997898 0 Td 26.970228 Tz (I ) Tj 0.418039 0 Td 44.950379 Tz (P ) Tj 0.485464 0 Td 29.96692 Tz (fFi ) Tj 1.051839 0 Td 60.683012 Tz (& ) Tj 0.525919 0 Td 44.500876 Tz (Dodge ) Tj 1.469877 0 Td 51.692936 Tz (LLP ) Tj 42.571429 0 0 42.571429 0 1281.132787 Tm 12.261745 0 Td 64.597315 Tz (264/494; ) Tj 3.35906 0 Td 64.597315 Tz (264/496; ) Tj 3.35906 0 Td 64.107942 Tz (585/400; ) Tj 3.35906 0 Td 62.870114 Tz (585/411:585/.435: ) Tj 8.761745 0 Td 61.334825 Tz (andry; ) Tj 2.536913 0 Td 71.029083 Tz (Edwards ) Tj 3.147651 0 Td 65.902312 Tz (Angell ) Tj 2.677852 0 Td 68.512304 Tz (Falmer ) Tj 2.677852 0 Td 105.704698 Tz (& ) Tj 0.916107 0 Td 76.733781 Tz (Lodge ) Tj 40 0 0 40 0 1236 Tm 20.475 0 Td 73.550725 Tz (585/436:585F437:585/440 ) Tj 27.857143 0 0 27.857143 0 1216.774704 Tm 33.815385 0 Td 41.880342 Tz (s ) Tj 5.133333 0 Td 41.880342 Tz (s ) Tj 8.220513 0 Td 107.692308 Tz (57 ) Tj 11.989744 0 Td 151.816239 Tz (ABSTRACT ) Tj 51.071429 0 0 51.071429 0 1185.079762 Tm 6.422378 0 Td 49.7669 Tz (\(58\) ) Tj 1.997203 0 Td 50.25641 Tz (Field ) Tj 1.742657 0 Td 55.477855 Tz (of ) Tj 0.783217 0 Td 49.417249 Tz (Classification ) Tj 4.346853 0 Td 59.285159 Tz (Search ) Tj 2.506294 0 Td 30.057662 Tz (................... ) Tj 3.994406 0 Td 51.748252 Tz (568/67, ) Tj 3.700699 0 Td 49.7669 Tz (\(57\) ) Tj 48.571429 0 0 48.571429 0 1143 Tm 10.644118 0 Td 54.411765 Tz (568/68, ) Tj 2.532353 0 Td 51.470588 Tz (77; ) Tj 1.358824 0 Td 56.188725 Tz (526/286; ) Tj 3.108824 0 Td 56.188725 Tz (522/180, ) Tj 2.923529 0 Td 52.614379 Tz (81; ) Tj 1.358824 0 Td 54.558824 Tz (428/411.1, ) Tj 44.285714 0 0 44.285714 0 1097.050888 Tm 12.803226 0 Td 62.096774 Tz (428/419, ) Tj 3.206452 0 Td 61.155914 Tz (457, ) Tj 1.670968 0 Td 62.096774 Tz (461, ) Tj 1.670968 0 Td 62.096774 Tz (463; ) Tj 1.964516 0 Td 61.626344 Tz (585/400, ) Tj 3.183871 0 Td 65.389785 Tz (411,435, ) Tj 4.877419 0 Td 75.268817 Tz (Th ) Tj 3.680645 0 Td 50.806452 Tz (ti ) Tj 2.235484 0 Td 35.752688 Tz (ti ) Tj 3.093548 0 Td 52.688172 Tz (id ) Tj 7.812903 0 Td 71.505376 Tz (d ) Tj 0.609677 0 Td 70.878136 Tz (method ) Tj 58.021978 0 0 58.021978 0 1052.981691 Tm 9.789394 0 Td 47.036774 Tz (585/436, ) Tj 2.430114 0 Td 46.677715 Tz (437, ) Tj 1.258144 0 Td 48.113952 Tz (440; ) Tj 1.499432 0 Td 47.036774 Tz (264/405, ) Tj 2.412879 0 Td 46.677715 Tz (426, ) Tj 1.309848 0 Td 46.677715 Tz (446, ) Tj 1.275379 0 Td 46.677715 Tz (448, ) Tj 3.136742 0 Td 87.61048 Tz (sets ) Tj 2.447348 0 Td 64.630682 Tz (1W ) Tj 1.568371 0 Td 149.368687 Tz (t ) Tj 3.016098 0 Td 427.998737 Tz (EN ) Tj 6.618182 0 Td 80.429293 Tz (s ) Tj 0.913447 0 Td 37.342172 Tz (S ) Tj 47.857143 0 0 47.857143 0 1026.440691 Tm 11.847761 0 Td 57.462687 Tz (264/485, ) Tj 2.967164 0 Td 55.721393 Tz (494, ) Tj 1.525373 0 Td 58.333333 Tz (495; ) Tj 1.81791 0 Td 57.027363 Tz (427/508, ) Tj 2.946269 0 Td 62.106136 Tz (512,517,518, ) Tj 6.080597 0 Td 62.686567 Tz (O ) Tj 0.919403 0 Td 57.114428 Tz (using ) Tj 1.985075 0 Td 54.560531 Tz (the ) Tj 1.880597 0 Td 119.568823 Tz (OOC ) Tj 2.653731 0 Td 50.497512 Tz (to ) Tj 1.191045 0 Td 51.368159 Tz (abricate ) Tj 2.758209 0 Td 53.9801 Tz (robust ) Tj 2.214925 0 Td 63.18408 Tz (polymer ) Tj 2.946269 0 Td 53.233831 Tz (Surface ) Tj 50.21978 0 0 50.21978 0 984.063253 Tm 13.938731 0 Td 54.7593 Tz (427/520, ) Tj 2.827571 0 Td 53.099927 Tz (256, ) Tj 1.493435 0 Td 57.129832 Tz (265,287,407.1, ) Tj 5.017943 0 Td 60.843666 Tz (409 ) Tj 2.628446 0 Td 51.440554 Tz (coatings ) Tj 2.608534 0 Td 55.588986 Tz (with ) Tj 1.473523 0 Td 50.776805 Tz (controlled ) Tj 3.126258 0 Td 51.591406 Tz (thicknesses ) Tj 3.564333 0 Td 58.315098 Tz (between ) Tj 2.688184 0 Td 36.5062 Tz (1 ) Tj 0.418162 0 Td 61.949915 Tz (and ) Tj 1.234573 0 Td 53.099927 Tz (5 ) Tj 0.477899 0 Td 76.331145 Tz (nanom ) Tj 52.436975 0 0 52.436975 0 942.064076 Tm 8.162179 0 Td 57.211538 Tz (See ) Tj 1.163301 0 Td 48.254176 Tz (application ) Tj 3.394551 0 Td 37.346421 Tz (file ) Tj 1.087019 0 Td 46.616809 Tz (for ) Tj 0.972596 0 Td 55.225027 Tz (complete ) Tj 2.822436 0 Td 49.795228 Tz (search ) Tj 1.964263 0 Td 44.100561 Tz (history. ) Tj 5.244391 0 Td 41.849181 Tz (eters. ) Tj 1.697276 0 Td 61.44943 Tz (The ) Tj 1.277724 0 Td 49.265491 Tz (coatings ) Tj 2.555449 0 Td 48.735755 Tz (are ) Tj 1.067949 0 Td 60.389957 Tz (composed ) Tj 3.051282 0 Td 57.211538 Tz (of ) Tj 0.781891 0 Td 54.03312 Tz (a ) Tj 0.533974 0 Td 60.389957 Tz (new ) Tj 1.354006 0 Td 47.676282 Tz (material ) Tj 2.479167 0 Td 55.395299 Tz (contain ) Tj 51.428571 0 0 51.428571 0 908.210773 Tm 25.297222 0 Td 50.771605 Tz (ing ) Tj 1.147222 0 Td 55.387205 Tz (polymerized ) Tj 3.908333 0 Td 62.789352 Tz (monomers ) Tj 3.247222 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 51.371742 Tz (4-vinylbenzenepropanethiol. ) Tj 49.450549 0 0 49.450549 0 865.500457 Tm 6.632889 0 Td 51.398148 Tz (\(56\) ) Tj 6.390222 0 Td 57.296296 Tz (References ) Tj 3.660222 0 Td 58.644444 Tz (Cited ) Tj 9.625778 0 Td 66.283951 Tz (The ) Tj 1.456 0 Td 60.666667 Tz (polymer ) Tj 2.790667 0 Td 51.518519 Tz (Surface ) Tj 2.446889 0 Td 52.962963 Tz (coating ) Tj 2.527778 0 Td 69.654321 Tz (may ) Tj 1.536889 0 Td 60.666667 Tz (be ) Tj 0.970667 0 Td 53.925926 Tz (applied ) Tj 2.527778 0 Td 47.185185 Tz (to ) Tj 0.889778 0 Td 53.925926 Tz (metal ) Tj 1.921111 0 Td 61.790123 Tz (and ) Tj 48.461538 0 0 48.461538 0 813.463082 Tm 11.328571 0 Td 55.886243 Tz (U.S. ) Tj 1.609524 0 Td 76.80776 Tz (PATENT ) Tj 2.992063 0 Td 87.889477 Tz (DOCUMENTS ) Tj 10.936508 0 Td 45.998677 Tz (silicon. ) Tj 2.373016 0 Td 68.783069 Tz (The ) Tj 1.444444 0 Td 63.624339 Tz (method ) Tj 2.47619 0 Td 53.306878 Tz (includes ) Tj 2.765079 0 Td 58.465608 Tz (exposing ) Tj 2.950794 0 Td 58.465608 Tz (a ) Tj 0.577778 0 Td 55.714286 Tz (metal ) Tj 1.857143 0 Td 51.205173 Tz (Substrate ) Tj 2.930159 0 Td 51.587302 Tz (to ) Tj 0.804762 0 Td 58.465608 Tz (a ) Tj 51.428571 0 0 51.428571 0 772.13834 Tm 25.316667 0 Td 48.206019 Tz (Solution ) Tj 2.605556 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 49.691358 Tz (the ) Tj 1.186111 0 Td 67.12963 Tz (monomer ) Tj 3.052778 0 Td 46.990741 Tz (in ) Tj 0.836111 0 Td 56.018519 Tz (hexanes ) Tj 2.644444 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 52.5 Tz (order ) Tj 1.808333 0 Td 46.990741 Tz (to ) Tj 0.894444 0 Td 50 Tz (deposit ) Tj 2.372222 0 Td 55.092593 Tz (a ) Tj 46.992481 0 0 46.992481 0 734.038488 Tm 8.66096 0 Td 51.623704 Tz (5,290,956 ) Tj 3.17072 0 Td 88.666667 Tz (A ) Tj 0.9576 0 Td 53.2 Tz (* ) Tj 1.21296 0 Td 54.973333 Tz (3/1994 ) Tj 2.53232 0 Td 69.16 Tz (Emmons ) Tj 2.68128 0 Td 42.56 Tz (et ) Tj 0.68096 0 Td 36.648889 Tz (al. ) Tj 1.00016 0 Td 32.192821 Tz (............. ) Tj 2.8728 0 Td 54.213333 Tz (549,478 ) Tj 3.91552 0 Td 63.84 Tz (monolayer ) Tj 3.57504 0 Td 65.613333 Tz (of ) Tj 0.87248 0 Td 54.382222 Tz (the ) Tj 1.21296 0 Td 72.96 Tz (monomer ) Tj 3.21328 0 Td 58.52 Tz (onto ) Tj 1.61728 0 Td 54.382222 Tz (the ) Tj 1.19168 0 Td 57.456 Tz (metal ) Tj 1.95776 0 Td 50.983333 Tz (surface. ) Tj 2.66 0 Td 69.751111 Tz (The ) Tj 1.44704 0 Td 75.662222 Tz (sub ) Tj 42.063492 0 0 42.063492 0 702.818043 Tm 9.675849 0 Td 57.672956 Tz (5,382.640 ) Tj 3.542264 0 Td 99.056604 Tz (A ) Tj 1.069811 0 Td 59.433962 Tz (* ) Tj 1.497736 0 Td 56.792453 Tz (1/1995 ) Tj 2.686415 0 Td 77.264151 Tz (Emmons ) Tj 2.995472 0 Td 47.54717 Tz (et ) Tj 0.760755 0 Td 40.943396 Tz (al. ) Tj 1.117358 0 Td 35.965167 Tz (............. ) Tj 3.209434 0 Td 60.566038 Tz (526,266 ) Tj 61.938776 0 0 61.938776 0 661.616205 Tm 6.571005 0 Td 39.166514 Tz (5,403,902 ) Tj 2.405601 0 Td 67.27073 Tz (A ) Tj 1.646787 0 Td 41.259381 Tz (4/1995 ) Tj 1.953542 0 Td 42.716914 Tz (Heilmann ) Tj 2.211862 0 Td 32.289951 Tz (et ) Tj 0.500494 0 Td 28.702178 Tz (al. ) Tj 6.603295 0 Td 69.96156 Tz (s ) Tj 0.597364 0 Td 69.96156 Tz (1SN ) Tj 1.937397 0 Td 72.652389 Tz (sited ) Tj 2.308731 0 Td 46.416804 Tz (with ) Tj 1.582208 0 Td 66.732565 Tz (title ) Tj 4.633608 0 Td 39.017024 Tz (1. ) Tj 1.243163 0 Td 45.744097 Tz (t ) Tj 0.839539 0 Td 39.017024 Tz (tO ) Tj 45.785714 0 0 45.785714 0 636.205809 Tm 8.889236 0 Td 52.17542 Tz (5,549,931 ) Tj 3.25429 0 Td 91.00364 Tz (A ) Tj 2.271451 0 Td 55.208875 Tz (8/1996 ) Tj 2.577223 0 Td 49.869995 Tz (Dattatraya ) Tj 3.166927 0 Td 45.50182 Tz (et ) Tj 0.677067 0 Td 38.82822 Tz (al. ) Tj 7.578783 0 Td 51.690068 Tz (graft ) Tj 1.725429 0 Td 65.522621 Tz (a ) Tj 0.546022 0 Td 53.692148 Tz (thin ) Tj 1.485179 0 Td 67.342694 Tz (po ) Tj 1.026521 0 Td 72.802912 Tz (ymer ) Tj 1.900156 0 Td 57.722309 Tz (coating ) Tj 2.620905 0 Td 59.152366 Tz (onto ) Tj 1.638066 0 Td 55.815566 Tz (the ) Tj 1.223089 0 Td 55.815566 Tz (sur ) Tj 1.24493 0 Td 52.782111 Tz (ace. ) Tj 1.638066 0 Td 25.481019 Tz (I ) Tj 0.349454 0 Td 63.702548 Tz (he ) Tj 0.939158 0 Td 61.154446 Tz (proce ) Tj 2.227769 0 Td 59.455712 Tz (ure ) Tj 46.240602 0 0 46.240602 0 596.595258 Tm 8.801789 0 Td 51.261668 Tz (5,773,581 ) Tj 3.243902 0 Td 86.504065 Tz (A ) Tj 2.205854 0 Td 36.04336 Tz (6, ) Tj 0.670407 0 Td 54.966125 Tz (1998 ) Tj 1.859837 0 Td 62.475158 Tz (Camble ) Tj 2.44374 0 Td 43.252033 Tz (et ) Tj 0.670407 0 Td 37.244806 Tz (al. ) Tj 8.239512 0 Td 62.475158 Tz (can ) Tj 1.254309 0 Td 64.878049 Tz (be ) Tj 0.929919 0 Td 56.768293 Tz (repeated ) Tj 2.87626 0 Td 48.658537 Tz (in ) Tj 0.735285 0 Td 58.390244 Tz (order ) Tj 1.838211 0 Td 52.262873 Tz (to ) Tj 0.778537 0 Td 54.065041 Tz (control ) Tj 2.422114 0 Td 56.467931 Tz (the ) Tj 1.102927 0 Td 56.06745 Tz (thickness ) Tj 3.179024 0 Td 59.471545 Tz (of ) Tj 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2154.763387 Tm 7.13125 0 Td 46.180556 Tz (vesicles; ) Tj 2.778125 0 Td 62.708333 Tz (Chem. ) Tj 2.165625 0 Td 68.229167 Tz (Commun. ) Tj 3.128125 0 Td 63.194444 Tz (The ) Tj 1.421875 0 Td 56.875 Tz (Royal ) Tj 1.96875 0 Td 52.083333 Tz (Society ) Tj 2.45 0 Td 54.6875 Tz (of ) Tj 0.83125 0 Td 56.30787 Tz (Chemistry ) Tj 3.303125 0 Td 53.229167 Tz (2000, ) Tj 34.285714 0 0 34.285714 0 2122 Tm 9.654167 0 Td 71.458333 Tz (1433-1434. ) Tj 42.857143 0 0 42.857143 0 2077 Tm 7.63 0 Td 51.527778 Tz (Lin, ) Tj 1.47 0 Td 46.666667 Tz (Z., ) Tj 1.12 0 Td 63.194444 Tz (Kim, ) Tj 1.796667 0 Td 56.388889 Tz (D. ) Tj 0.956667 0 Td 58.333333 Tz (H. ) Tj 1.073333 0 Td 70 Tz (Wu. ) Tj 1.516667 0 Td 50.555556 Tz (X., ) Tj 1.19 0 Td 59.197531 Tz (Boosahda, ) Tj 3.476667 0 Td 44.074074 Tz (L., ) Tj 1.05 0 Td 53.148148 Tz (Stone, ) Tj 2.17 0 Td 49.259259 Tz (D., ) Tj 1.19 0 Td 52.777778 Tz (Larose, ) Tj 2.52 0 Td 48.611111 Tz (L. ) Tj 0.816667 0 Td 101.111111 Tz (& ) Tj 45.714286 0 0 45.714286 0 2039.52611 Tm 7.153125 0 Td 48.307292 Tz (Russell, ) Tj 2.58125 0 Td 43.75 Tz (T. ) Tj 0.875 0 Td 34.635417 Tz (P. ) Tj 0.7 0 Td 87.5 Tz (A ) Tj 0.809375 0 Td 56.145833 Tz (Rapid ) Tj 1.990625 0 Td 56.875 Tz (Route ) Tj 1.925 0 Td 49.21875 Tz (to ) Tj 0.83125 0 Td 54.6875 Tz (Arrays ) Tj 2.23125 0 Td 56.510417 Tz (of ) Tj 0.875 0 Td 52.083333 Tz (Nanostructures ) Tj 4.6375 0 Td 47.395833 Tz (in ) Tj 0.809375 0 Td 58.333333 Tz (Thin ) Tj 42.857143 0 0 42.857143 0 2003 Tm 7.63 0 Td 54.444444 Tz (Films; ) Tj 2.17 0 Td 64.166667 Tz (Advanced ) Tj 3.313333 0 Td 54.012346 Tz (Materials ) Tj 3.103333 0 Td 53.472222 Tz (Oct. ) Tj 1.516667 0 Td 44.722222 Tz (2, ) Tj 0.77 0 Td 56.777778 Tz (2002, ) Tj 2.03 0 Td 46.666667 Tz (14, ) Tj 1.166667 0 Td 57.166667 Tz (1373-1376. ) Tj 45.714286 0 0 45.714286 0 1962.328205 Tm 7.153125 0 Td 52.256944 Tz (Jeong, ) Tj 2.0125 0 Td 72.916667 Tz (U. ) Tj 1.071875 0 Td 56.510417 Tz (Ryu, ) Tj 1.553125 0 Td 51.041667 Tz (D.Y., ) Tj 1.684375 0 Td 61.067708 Tz (Kim, ) Tj 1.61875 0 Td 34.635417 Tz (J. ) Tj 0.6125 0 Td 71.09375 Tz (K. ) Tj 1.028125 0 Td 61.067708 Tz (Kim, ) Tj 1.6625 0 Td 52.864583 Tz (D. ) Tj 0.83125 0 Td 69.270833 Tz (H. ) Tj 0.9625 0 Td 68.055556 Tz (Wu, ) Tj 1.35625 0 Td 58.333333 Tz (X. ) Tj 0.853125 0 Td 91.145833 Tz (& ) Tj 0.765625 0 Td 47.395833 Tz (Russell, ) Tj 2.384375 0 Td 47.395833 Tz (T. ) Tj 0.7875 0 Td 36.458333 Tz (P. ) Tj 45.714286 0 0 45.714286 0 1925.877193 Tm 7.175 0 Td 49.479167 Tz (Precise ) Tj 2.31875 0 Td 52.604167 Tz (Control ) Tj 2.471875 0 Td 58.333333 Tz (of ) Tj 0.7875 0 Td 60.611979 Tz (Nanopore ) Tj 3.128125 0 Td 52.864583 Tz (Size ) Tj 1.509375 0 Td 43.75 Tz (in ) Tj 0.74375 0 Td 57.421875 Tz (Thin ) Tj 1.6625 0 Td 55.598958 Tz (Film ) Tj 1.553125 0 Td 59.0625 Tz (Using ) Tj 1.990625 0 Td 54.6875 Tz (Mixtures ) Tj 2.8875 0 Td 54.6875 Tz (of ) Tj 45.714286 0 0 45.714286 0 1890.165893 Tm 7.153125 0 Td 59.791667 Tz (Asymmetric ) Tj 3.784375 0 Td 57.604167 Tz (Block ) Tj 1.8375 0 Td 60.763889 Tz (Copolymer ) Tj 3.390625 0 Td 58.333333 Tz (and ) Tj 1.26875 0 Td 60.460069 Tz (Homopolymer; ) Tj 4.50625 0 Td 57.8125 Tz (Macromolecules ) Tj 41.428571 0 0 41.428571 0 1851 Tm 7.893103 0 Td 61.350575 Tz (Dec. ) Tj 1.713793 0 Td 46.264368 Tz (2, ) Tj 0.796552 0 Td 58.735632 Tz (2003, ) Tj 2.003448 0 Td 53.639847 Tz (36, ) Tj 1.303448 0 Td 61.350575 Tz (10126-10 ) Tj 3.065517 0 Td 53.304598 Tz (129. ) Tj 45.714286 0 0 45.714286 0 1808.441176 Tm 7.13125 0 Td 56.510417 Tz (Wei, ) Tj 1.575 0 Td 43.75 Tz (Y.; ) Tj 1.115625 0 Td 51.953125 Tz (Qiu, ) Tj 1.53125 0 Td 51.041667 Tz (K.-Y. ) Tj 1.8375 0 Td 83.854167 Tz (A ) Tj 0.7875 0 Td 57.604167 Tz (Novel ) Tj 2.0125 0 Td 53.004808 Tz (Nonsurfactant ) Tj 4.41875 0 Td 57.604167 Tz (Route ) Tj 1.96875 0 Td 47.395833 Tz (to ) Tj 0.896875 0 Td 58.697917 Tz (Nanoporous ) Tj 45.714286 0 0 45.714286 0 1773.243081 Tm 7.153125 0 Td 51.041667 Tz (Materials ) Tj 2.909375 0 Td 58.333333 Tz (and ) Tj 1.26875 0 Td 37.673611 Tz (Its ) Tj 0.896875 0 Td 49.583333 Tz (Biological ) Tj 3.10625 0 Td 49.639423 Tz (Applications; ) Tj 4.06875 0 Td 49.21875 Tz (Series ) Tj 1.946875 0 Td 58.333333 Tz (on ) Tj 0.875 0 Td 58.333333 Tz (Chemical ) Tj 2.996875 0 Td 65.625 Tz (Engi ) Tj 45.714286 0 0 45.714286 0 1734.906921 Tm 7.153125 0 Td 49.21875 Tz (neering, ) Tj 2.515625 0 Td 59.0625 Tz (Nanoporous ) Tj 3.653125 0 Td 48.854167 Tz (Materials; ) Tj 3.10625 0 Td 53.958333 Tz (2004, ) Tj 1.75 0 Td 44.661458 Tz (vol. ) Tj 1.203125 0 Td 45.572917 Tz (4; ) Tj 0.678125 0 Td 55.902778 Tz (Ch. ) Tj 1.18125 0 Td 51.041667 Tz (28; ) Tj 1.05 0 Td 54.6875 Tz (873-892; ) Tj 2.8 0 Td 71.09375 Tz (Impe ) Tj 45.714286 0 0 45.714286 0 1698.247748 Tm 7.153125 0 Td 40.104167 Tz (rial ) Tj 1.159375 0 Td 53.645833 Tz (College ) Tj 2.471875 0 Td 45.572917 Tz (Press. ) Tj 45.714286 0 0 45.714286 0 1654.069091 Tm 7.175 0 Td 50.434028 Tz (Desai, ) Tj 1.925 0 Td 48.854167 Tz (T.A.; ) Tj 1.684375 0 Td 52.256944 Tz (Hansford, ) Tj 2.996875 0 Td 44.479167 Tz (D.J.; ) Tj 1.509375 0 Td 51.041667 Tz (Kulinsky, ) Tj 2.909375 0 Td 43.75 Tz (L.; ) Tj 0.940625 0 Td 52.083333 Tz (Nashat, ) Tj 2.31875 0 Td 52.5 Tz (A.H.; ) Tj 1.79375 0 Td 47.395833 Tz (Rasi, ) Tj 1.53125 0 Td 51.041667 Tz (G.; ) Tj 1.028125 0 Td 53.472222 Tz (Tu, ) Tj 45.714286 0 0 45.714286 0 1619.173397 Tm 7.153125 0 Td 35.243056 Tz (J.; ) Tj 0.765625 0 Td 61.25 Tz (Wang, ) Tj 1.946875 0 Td 43.75 Tz (Y., ) Tj 0.940625 0 Td 55.902778 Tz (Zhang, ) Tj 2.165625 0 Td 55.902778 Tz (M., ) Tj 1.203125 0 Td 43.75 Tz (Ferrari. ) Tj 2.275 0 Td 54.6875 Tz (M.; ) Tj 1.159375 0 Td 54.024621 Tz (Nanoporousanit-fouling ) Tj 7.284375 0 Td 45.833333 Tz (silicon ) Tj 45.714286 0 0 45.714286 0 1579.440926 Tm 7.153125 0 Td 58.333333 Tz (mebranes ) Tj 3.0625 0 Td 47.395833 Tz (for ) Tj 1.09375 0 Td 51.851852 Tz (biosensor ) Tj 3.040625 0 Td 47.395833 Tz (applications; ) Tj 4.025 0 Td 52.5 Tz (Biosensors ) Tj 3.390625 0 Td 87.5 Tz (& ) Tj 0.896875 0 Td 49.21875 Tz (Bioelectronics ) Tj 41.428571 0 0 41.428571 0 1542 Tm 7.893103 0 Td 60.344828 Tz (2000, ) Tj 2.1 0 Td 50.957854 Tz (15, ) Tj 1.062069 0 Td 60.344828 Tz (454-462. ) Tj 45.714286 0 0 45.714286 0 2869.85751 Tm 28.48125 0 Td 49.674479 Tz (Poulain, ) Tj 2.690625 0 Td 47.395833 Tz (N.; ) Tj 1.18125 0 Td 56.510417 Tz (Nakache, ) Tj 3.0625 0 Td 41.319444 Tz (E.; ) Tj 1.09375 0 Td 46.666667 Tz (Pina, ) Tj 1.70625 0 Td 46.180556 Tz (A.; ) Tj 1.18125 0 Td 53.877315 Tz (Levesque, ) Tj 3.19375 0 Td 48.307292 Tz (G.J. ) Tj 1.465625 0 Td 51.883013 Tz (Nanoparticles ) Tj 45.714286 0 0 45.714286 0 2832.517618 Tm 28.459375 0 Td 59.244792 Tz (from ) Tj 1.6625 0 Td 50 Tz (Vesicle ) Tj 2.384375 0 Td 51.041667 Tz (Polymerization: ) Tj 4.85625 0 Td 50.358073 Tz (Characterization ) Tj 5.096875 0 Td 58.333333 Tz (and ) Tj 1.334375 0 Td 50.520833 Tz (Kinetic ) Tj 2.40625 0 Td 52.256944 Tz (Study; ) Tj 45.714286 0 0 45.714286 0 2794.378238 Tm 28.459375 0 Td 51.041667 Tz (Journal ) Tj 2.31875 0 Td 58.333333 Tz (of ) Tj 0.809375 0 Td 59.375 Tz (Polymer ) Tj 2.625 0 Td 54.166667 Tz (Science ) Tj 2.5375 0 Td 51.770833 Tz (1996, ) Tj 1.70625 0 Td 51.041667 Tz (34, ) Tj 1.115625 0 Td 53.776042 Tz (729-737. ) Tj 45.714286 0 0 45.714286 0 2759.161209 Tm 28.48125 0 Td 52.5 Tz (Hotz, ) Tj 1.859375 0 Td 37.673611 Tz (J.; ) Tj 1.00625 0 Td 52.256944 Tz (Meier, ) Tj 2.165625 0 Td 65.625 Tz (W. ) Tj 1.115625 0 Td 52.971814 Tz (Vesicle-Templated ) Tj 5.73125 0 Td 58.854167 Tz (Polymer ) Tj 2.8 0 Td 58.940972 Tz (Hollow ) Tj 2.471875 0 Td 51.041667 Tz (Spheres; ) Tj 45.714286 0 0 45.714286 0 2719.978587 Tm 28.459375 0 Td 60.15625 Tz (Langmuir ) Tj 3.0625 0 Td 50.130208 Tz (Feb. ) Tj 1.421875 0 Td 43.75 Tz (3, ) Tj 0.7875 0 Td 51.770833 Tz (1998, ) Tj 1.8375 0 Td 44.965278 Tz (14, ) Tj 1.071875 0 Td 53.958333 Tz (1031-1036. ) Tj 45.714286 0 0 45.714286 0 2681.422007 Tm 28.4375 0 Td 52.604167 Tz (Nardin, ) Tj 2.384375 0 Td 52.864583 Tz (C. ) Tj 0.83125 0 Td 44.479167 Tz (Hirt, ) Tj 1.465625 0 Td 41.319444 Tz (T.; ) Tj 0.9625 0 Td 51.5625 Tz (Leukel, ) Tj 2.31875 0 Td 35.243056 Tz (J.; ) Tj 0.809375 0 Td 52.256944 Tz (Meier, ) Tj 1.990625 0 Td 67.447917 Tz (W. ) Tj 1.00625 0 Td 55.681818 Tz (Polymerized ) Tj 3.784375 0 Td 83.854167 Tz (ABA ) Tj 1.640625 0 Td 51.953125 Tz (Triblock ) Tj 45.714286 0 0 45.714286 0 2645.642202 Tm 28.459375 0 Td 61.168981 Tz (Copolymer ) Tj 3.434375 0 Td 46.990741 Tz (Vesicles; ) Tj 2.778125 0 Td 55.497685 Tz (Langmuir, ) Tj 3.19375 0 Td 55.598958 Tz (Nov. ) Tj 1.553125 0 Td 49.826389 Tz (20, ) Tj 1.1375 0 Td 52.5 Tz (1999, ) Tj 1.859375 0 Td 44.965278 Tz (16, ) Tj 1.071875 0 Td 53.958333 Tz (1035-1041. ) Tj 45.714286 0 0 45.714286 0 2605.707768 Tm 28.48125 0 Td 49.826389 Tz (Kurja, ) Tj 1.96875 0 Td 36.458333 Tz (J.; ) Tj 0.875 0 Td 50 Tz (Noelte, ) Tj 2.31875 0 Td 50 Tz (R.J.M.; ) Tj 2.31875 0 Td 57.421875 Tz (Maxwell, ) Tj 2.975 0 Td 43.020833 Tz (I.A.; ) Tj 1.465625 0 Td 60.416667 Tz (German, ) Tj 2.734375 0 Td 43.75 Tz (A.I. ) Tj 1.3125 0 Td 51.953125 Tz (Free ) Tj 1.44375 0 Td 52.604167 Tz (Radical ) Tj 45.714286 0 0 45.714286 0 2574.066116 Tm 28.48125 0 Td 52.604167 Tz (Polymerization ) Tj 4.659375 0 Td 56.510417 Tz (of ) Tj 0.765625 0 Td 53.645833 Tz (Styrene ) Tj 2.49375 0 Td 43.75 Tz (in ) Tj 0.765625 0 Td 57.928241 Tz (Dioctadecyldimethylammonium ) Tj 9.66875 0 Td 70.486111 Tz (Bro ) Tj 45.714286 0 0 45.714286 0 2532.47695 Tm 28.459375 0 Td 61.067708 Tz (mide ) Tj 1.596875 0 Td 47.395833 Tz (Vesicles; ) Tj 2.778125 0 Td 54.231771 Tz (Polymer, ) Tj 2.865625 0 Td 51.770833 Tz (1993, ) Tj 1.75 0 Td 48.611111 Tz (34, ) Tj 1.115625 0 Td 54.6875 Tz (2045-2049. ) Tj 45.714286 0 0 45.714286 0 2494.79786 Tm 28.459375 0 Td 58.333333 Tz (McKelvey, ) Tj 3.28125 0 Td 52.5 Tz (C.A.; ) Tj 1.728125 0 Td 49.21875 Tz (Kaler, ) Tj 1.96875 0 Td 51.770833 Tz (E.W.; ) Tj 1.684375 0 Td 51.041667 Tz (Zasadzinski, ) Tj 3.828125 0 Td 44.479167 Tz (J.A.; ) Tj 1.4875 0 Td 52.864583 Tz (Coldren; ) Tj 2.66875 0 Td 52.5 Tz (Jung, ) Tj 1.75 0 Td 51.041667 Tz (H.T. ) Tj 45.714286 0 0 45.714286 0 2460.508197 Tm 28.459375 0 Td 55.052083 Tz (Templating ) Tj 3.478125 0 Td 58.940972 Tz (Hollow ) Tj 2.296875 0 Td 54.282407 Tz (Polymeric ) Tj 3.084375 0 Td 54.6875 Tz (Spheres ) Tj 2.45 0 Td 58.333333 Tz (from ) Tj 1.53125 0 Td 52.135417 Tz (Catanionic ) Tj 3.325 0 Td 53.030303 Tz (Equilibrium ) Tj 45.714286 0 0 45.714286 0 2420.713768 Tm 28.4375 0 Td 47.800926 Tz (Vesicles: ) Tj 2.8 0 Td 51.851852 Tz (Synthesis ) Tj 2.996875 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 48.897059 Tz (Characterization; ) Tj 5.228125 0 Td 55.497685 Tz (Langmuir, ) Tj 3.215625 0 Td 51.041667 Tz (Sep. ) Tj 1.4875 0 Td 48.611111 Tz (28, ) Tj 1.09375 0 Td 53.229167 Tz (2000, ) Tj 41.428571 0 0 41.428571 0 2383 Tm 31.475862 0 Td 50.957854 Tz (16, ) Tj 1.110345 0 Td 61.149425 Tz (8285-8290. ) Tj 45.714286 0 0 45.714286 0 2344.691238 Tm 28.459375 0 Td 51.770833 Tz (Jung, ) Tj 2.05625 0 Td 55.902778 Tz (M.: ) Tj 1.575 0 Td 51.5625 Tz (Hubert, ) Tj 2.7125 0 Td 56.25 Tz (D.H.W.; ) Tj 2.953125 0 Td 59.895833 Tz (Bomans, ) Tj 3.01875 0 Td 49.21875 Tz (P.H. ) Tj 1.246875 0 Td 47.395833 Tz (H.; ) Tj 1.4 0 Td 48.206019 Tz (Frederik, ) Tj 3.171875 0 Td 49.583333 Tz (P.M.; ) Tj 45.714286 0 0 45.714286 0 2307.101695 Tm 28.459375 0 Td 52.662037 Tz (Meuldijk, ) Tj 2.975 0 Td 36.458333 Tz (J.; ) Tj 0.809375 0 Td 60.763889 Tz (Van ) Tj 1.26875 0 Td 53.958333 Tz (Herk, ) Tj 1.771875 0 Td 55.416667 Tz (A.M.; ) Tj 1.859375 0 Td 46.940104 Tz (Fischer, ) Tj 2.428125 0 Td 54.6875 Tz (H. ) Tj 0.809375 0 Td 60.416667 Tz (German, ) Tj 2.690625 0 Td 43.75 Tz (A.I. ) Tj 1.246875 0 Td 75.347222 Tz (New ) Tj 1.44375 0 Td 55.729167 Tz (Vesicle ) Tj 45.714286 0 0 45.714286 0 2272.02133 Tm 28.48125 0 Td 58.854167 Tz (Polymer ) Tj 2.75625 0 Td 52.604167 Tz (Hybrid: ) Tj 2.49375 0 Td 51.041667 Tz (the ) Tj 1.203125 0 Td 52.662037 Tz (Parachute ) Tj 3.10625 0 Td 48.517628 Tz (Architecture; ) Tj 4.134375 0 Td 59.244792 Tz (Langmuir ) Tj 3.19375 0 Td 51.041667 Tz (1997, ) Tj 1.88125 0 Td 46.180556 Tz (13, ) Tj 34.285714 0 0 34.285714 0 2238 Tm 37.945833 0 Td 73.402778 Tz (6877-688O. ) Tj 45.714286 0 0 45.714286 0 2195.482252 Tm 28.459375 0 Td 54.6875 Tz (McIntosh, ) Tj 3.084375 0 Td 47.395833 Tz (T. ) Tj 0.765625 0 Td 35.243056 Tz (J., ) Tj 0.809375 0 Td 57.118056 Tz (Simon, ) Tj 2.253125 0 Td 56.510417 Tz (S.A. ) Tj 1.509375 0 Td 91.145833 Tz (& ) Tj 0.765625 0 Td 59.791667 Tz (MacDonald, ) Tj 3.784375 0 Td 51.041667 Tz (R. ) Tj 0.7875 0 Td 52.864583 Tz (C. ) Tj 0.809375 0 Td 63.194444 Tz (The ) Tj 1.290625 0 Td 52.560764 Tz (Organization ) Tj 45.714286 0 0 45.714286 0 2158.820144 Tm 28.459375 0 Td 56.510417 Tz (of ) Tj 0.74375 0 Td 55.092593 Tz (n-Alkanes ) Tj 3.128125 0 Td 43.75 Tz (in ) Tj 0.721875 0 Td 51.041667 Tz (Lipid ) Tj 1.70625 0 Td 47.395833 Tz (Bilayers; ) Tj 2.778125 0 Td 54.6875 Tz (Biochimica ) Tj 3.4125 0 Td 45.572917 Tz (et ) Tj 0.7 0 Td 54.322917 Tz (Biophysica ) Tj 3.346875 0 Td 56.510417 Tz (Acta ) Tj 1.553125 0 Td 51.041667 Tz (1980, ) Tj 41.428571 0 0 41.428571 0 2121 Tm 31.427586 0 Td 57.327586 Tz 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47.69292 Tz (present ) Tj 2.150119 0 Td 46.96367 Tz (invention ) Tj 2.719809 0 Td 42.004773 Tz (relates ) Tj 1.911217 0 Td 44.411297 Tz (to ) Tj 0.698329 0 Td 49.005569 Tz (a ) Tj 0.496181 0 Td 60.236012 Tz (new ) Tj 1.212888 0 Td 56.006364 Tz (polymer ) Tj 2.444153 0 Td 53.599841 Tz (used ) Tj 1.45179 0 Td 42.879873 Tz (in ) Tj 0.679952 0 Td 46.96367 Tz (the ) Tj 54.693878 0 0 54.693878 0 1587.449173 Tm 5.960448 0 Td 49.670398 Tz (production ) Tj 3.181343 0 Td 53.327114 Tz (of ) Tj 0.731343 0 Td 48.756219 Tz (a ) Tj 0.475373 0 Td 49.191542 Tz (polymerization ) Tj 4.314925 0 Td 45.328047 Tz (coating. ) Tj 2.358582 0 Td 58.913765 Tz (The ) Tj 1.225 0 Td 49.844527 Tz (polymerization ) Tj 51.558442 0 0 51.558442 0 1541.944581 Tm 6.342317 0 Td 51.259446 Tz (coating ) Tj 2.30806 0 Td 37.174643 Tz (is ) Tj 0.659446 0 Td 55.761965 Tz (used ) Tj 1.493451 0 Td 45.256087 Tz (to ) Tj 0.717632 0 Td 51.721243 Tz (coat ) Tj 1.396474 0 Td 48.950462 Tz (metals, ) Tj 2.230479 0 Td 60.34145 Tz (and ) Tj 1.24131 0 Td 50.428212 Tz (other ) Tj 1.66801 0 Td 49.076406 Tz (substances, ) Tj 3.432997 0 Td 46.872376 Tz (in ) Tj 0.737028 0 Td 52.367758 Tz (order ) Tj 51.836735 0 0 51.836735 0 1502.573611 Tm 6.269685 0 Td 48.228346 Tz (to ) Tj 0.752362 0 Td 53.28084 Tz (provide ) Tj 2.372835 0 Td 49.192913 Tz (protection ) Tj 3.144488 0 Td 57.07021 Tz (from ) Tj 1.562598 0 Td 50.371829 Tz (corrosion ) Tj 2.932283 0 Td 57.874016 Tz (and ) Tj 1.234646 0 Td 45.305416 Tz (insulation. ) Tj 42.142857 0 0 42.142857 0 1424.556876 Tm 11.105085 0 Td 103.220339 Tz (BACKGROUND ) Tj 6.40678 0 Td 94.915254 Tz (OF ) Tj 1.305085 0 Td 97.551789 Tz (THE ) Tj 1.99322 0 Td 90.52103 Tz (INVENTION ) Tj 54.428571 0 0 54.428571 0 1334.926934 Tm 6.724409 0 Td 49.431321 Tz (Surface ) Tj 2.406824 0 Td 47.462817 Tz (coatings ) Tj 2.608924 0 Td 48.993876 Tz (play ) Tj 1.506562 0 Td 55.11811 Tz (a ) Tj 0.67979 0 Td 53.893263 Tz (major ) Tj 1.910761 0 Td 44.4007 Tz (role ) Tj 1.414698 0 Td 42.869641 Tz (in ) Tj 0.863517 0 Td 52.055993 Tz (our ) Tj 1.249344 0 Td 39.297171 Tz (lives. ) Tj 1.745407 0 Td 58.945757 Tz (They ) Tj 54.642857 0 0 54.642857 0 1292.43599 Tm 5.984314 0 Td 48.366013 Tz (include ) Tj 2.177778 0 Td 43.137255 Tz (paints, ) Tj 2.013072 0 Td 46.666667 Tz (adhesives, ) Tj 2.983007 0 Td 54.901961 Tz (and ) Tj 1.189542 0 Td 42.362624 Tz (sealants, ) Tj 2.470588 0 Td 63.442266 Tz (among ) Tj 2.086275 0 Td 62.527233 Tz (many ) Tj 1.665359 0 Td 43.572985 Tz (others. ) Tj 53 0 0 53 0 1251.057143 Tm 6.169811 0 Td 59.748428 Tz (They ) Tj 1.566038 0 Td 48.218029 Tz (are ) Tj 1 0 Td 48.427673 Tz (often ) Tj 1.566038 0 Td 54.245283 Tz (used ) Tj 1.45283 0 Td 46.121593 Tz (for ) Tj 0.943396 0 Td 49.371069 Tz (decoration ) Tj 3.09434 0 Td 56.603774 Tz (and ) Tj 1.113208 0 Td 48.113208 Tz (protection ) Tj 3.018868 0 Td 55.031447 Tz (of ) Tj 0.735849 0 Td 45.073375 Tz (surfaces. ) Tj 53.214286 0 0 53.214286 0 1211.616891 Tm 6.144966 0 Td 56.375839 Tz (These ) Tj 1.916779 0 Td 48.545861 Tz (coatings ) Tj 2.593289 0 Td 44.891872 Tz (typically ) Tj 2.668456 0 Td 42.058166 Tz (utilize ) Tj 1.973154 0 Td 46.979866 Tz (properties ) Tj 3.044295 0 Td 57.941834 Tz (of ) Tj 0.826846 0 Td 53.243848 Tz (adhered ) Tj 2.461745 0 Td 46.353468 Tz (films ) Tj 51.746032 0 0 51.746032 0 1166.649208 Tm 6.3 0 Td 53.949387 Tz (with ) Tj 1.468712 0 Td 53.949387 Tz (bulk ) Tj 1.449387 0 Td 48.044479 Tz (thicknesses. ) Tj 3.671779 0 Td 57.97546 Tz (With ) Tj 1.565337 0 Td 49.386503 Tz (reference ) Tj 2.879448 0 Td 43.481595 Tz (to ) Tj 0.753681 0 Td 47.852761 Tz (metals, ) Tj 2.183742 0 Td 50.817996 Tz (corrosion ) Tj 2.918098 0 Td 40.260736 Tz (is ) Tj 53 0 0 53 0 1125.210909 Tm 6.169811 0 Td 46.202225 Tz (deterioration ) Tj 3.754717 0 Td 55.031447 Tz (of ) Tj 0.735849 0 Td 45.073375 Tz (essential ) Tj 2.566038 0 Td 47.169811 Tz (properties ) Tj 3 0 Td 44.025157 Tz (in ) Tj 0.679245 0 Td 53.459119 Tz (a ) Tj 0.490566 0 Td 47.562893 Tz (material ) Tj 2.471698 0 Td 55.555556 Tz (due ) Tj 1.150943 0 Td 44.025157 Tz (to ) Tj 0.716981 0 Td 57.389937 Tz (reac ) Tj 54.571429 0 0 54.571429 0 1082.608802 Tm 5.973822 0 Td 44.589878 Tz (tions ) Tj 1.502618 0 Td 49.629145 Tz (with ) Tj 1.374346 0 Td 34.613147 Tz (its ) Tj 0.769634 0 Td 50.138162 Tz (environment. ) Tj 3.774869 0 Td 45.811518 Tz (In ) Tj 0.71466 0 Td 48.86562 Tz (metals ) Tj 1.924084 0 Td 54.973822 Tz (and ) Tj 1.15445 0 Td 49.47644 Tz (metal ) Tj 1.649215 0 Td 42.321117 Tz (alloys, ) Tj 1.942408 0 Td 55.584642 Tz (corro ) Tj 51.648352 0 0 51.648352 0 1042.722429 Tm 6.331277 0 Td 49.210993 Tz (Sion ) Tj 1.355319 0 Td 52.706856 Tz (begins ) Tj 2.032979 0 Td 52.437943 Tz (with ) Tj 1.432766 0 Td 49.479905 Tz (the ) Tj 1.064894 0 Td 45.177305 Tz (loss ) Tj 1.258511 0 Td 53.244681 Tz (of ) Tj 0.716383 0 Td 58.085106 Tz (an ) Tj 0.851915 0 Td 48.404255 Tz (electron ) Tj 2.49766 0 Td 58.085106 Tz (and ) Tj 1.181064 0 Td 40.336879 Tz (is ) Tj 0.638936 0 Td 51.631206 Tz (described ) Tj 2.923617 0 Td 50.01773 Tz (as ) Tj 0.735745 0 Td 61.312057 Tz (an ) Tj 54.897959 0 0 54.897959 0 1002.151122 Tm 5.93829 0 Td 47.967782 Tz (electrochemical ) Tj 4.44461 0 Td 49.008674 Tz (process ) Tj 2.204089 0 Td 44.671623 Tz (\(Jones, ) Tj 2.040149 0 Td 53.128872 Tz (Denny, ) Tj 2.113011 0 Td 47.360595 Tz (1996, ) Tj 1.639405 0 Td 46.146221 Tz (Principles ) Tj 2.914498 0 Td 59.706733 Tz (and ) Tj 54.642857 0 0 54.642857 0 957.589901 Tm 5.966013 0 Td 49.411765 Tz (Prevention ) Tj 3.202614 0 Td 59.477124 Tz (of ) Tj 0.786928 0 Td 48.496732 Tz (Corrosion, ) Tj 3.184314 0 Td 57.95207 Tz (2nd ) Tj 1.281046 0 Td 42.701525 Tz (edition, ) Tj 2.324183 0 Td 57.342048 Tz (Upper ) Tj 1.939869 0 Td 51.851852 Tz (Saddle ) Tj 2.122876 0 Td 44.22658 Tz (River, ) Tj 54.693878 0 0 54.693878 0 918.292254 Tm 5.978731 0 Td 42.052239 Tz (N.J., ) Tj 1.444403 0 Td 46.089863 Tz (Prentice ) Tj 2.376866 0 Td 43.271144 Tz (Hall, ) Tj 1.444403 0 Td 64.754353 Tz (ISBN ) Tj 1.663806 0 Td 49.975124 Tz (0-13-359993-0\). ) Tj 4.64403 0 Td 47.994403 Tz (Existing ) Tj 2.395149 0 Td 45.37037 Tz (coatings, ) Tj 54.444444 0 0 54.444444 0 878.233843 Tm 6.02449 0 Td 51.27551 Tz (Such ) Tj 1.359184 0 Td 47.44898 Tz (as ) Tj 0.697959 0 Td 42.857143 Tz (traditional ) Tj 2.938776 0 Td 45.408163 Tz (paints ) Tj 1.763265 0 Td 56.122449 Tz (and ) Tj 1.102041 0 Td 55.539359 Tz (polymer ) Tj 2.406122 0 Td 48.214286 Tz (coatings ) Tj 2.42449 0 Td 44.557823 Tz (typically ) Tj 2.516327 0 Td 54.336735 Tz (have ) Tj 54.603175 0 0 54.603175 0 833.219543 Tm 5.970349 0 Td 47.48062 Tz (thickness ) Tj 2.856977 0 Td 53.797238 Tz (measured ) Tj 2.856977 0 Td 42.732558 Tz (in ) Tj 0.769186 0 Td 46.547965 Tz (tens ) Tj 1.355233 0 Td 54.94186 Tz (of ) Tj 0.860756 0 Td 51.889535 Tz (microns ) Tj 2.435756 0 Td 42.732558 Tz (to ) Tj 0.805814 0 Td 49.34593 Tz (ensure ) Tj 2.014535 0 Td 52.652616 Tz (complete ) Tj 54.603175 0 0 54.603175 0 794.388024 Tm 5.988663 0 Td 51.126453 Tz (coverage ) Tj 2.600581 0 Td 54.94186 Tz (of ) Tj 0.732558 0 Td 46.802326 Tz (the ) Tj 1.025581 0 Td 49.447674 Tz (metal ) Tj 1.66657 0 Td 47.093023 Tz (surface ) Tj 2.106105 0 Td 54.94186 Tz (and ) Tj 1.135465 0 Td 50.744913 Tz (adequate ) Tj 2.600581 0 Td 50.744913 Tz (adhesion ) Tj 2.563953 0 Td 55.959302 Tz (proper ) Tj 54.603175 0 0 54.603175 0 753.323194 Tm 5.970349 0 Td 37.238372 Tz (ties. ) Tj 1.428488 0 Td 62.063953 Tz (Due ) Tj 1.355233 0 Td 44.258721 Tz (to ) Tj 0.805814 0 Td 46.802326 Tz (the ) Tj 1.098837 0 Td 51.584302 Tz (importance ) Tj 3.351453 0 Td 53.415698 Tz (of ) Tj 0.824128 0 Td 45.445736 Tz (coatings, ) Tj 2.710465 0 Td 43.565011 Tz (significant ) Tj 3.113372 0 Td 42.296512 Tz (efforts ) Tj 43.015873 0 0 43.015873 0 715.739409 Tm 7.578598 0 Td 68.773063 Tz (have ) Tj 1.976015 0 Td 67.804428 Tz (been ) Tj 1.976015 0 Td 64.760148 Tz (devoted ) Tj 3.068635 0 Td 52.306273 Tz (to ) Tj 0.976384 0 Td 56.396064 Tz (fabricate ) Tj 3.394096 0 Td 69.741697 Tz (them ) Tj 2.045756 0 Td 63.929889 Tz (with ) Tj 1.859779 0 Td 59.879235 Tz (thicknesses ) Tj 4.323985 0 Td 53.274908 Tz (less ) Tj 43.214286 0 0 43.214286 0 673.719363 Tm 7.543802 0 Td 62.672176 Tz (than ) Tj 1.828099 0 Td 70.707071 Tz (100 ) Tj 1.480992 0 Td 62.672176 Tz (micrometers. ) Tj 4.766942 0 Td 89.990817 Tz (Common ) Tj 3.517355 0 Td 53.99449 Tz (thin ) Tj 1.596694 0 Td 56.887052 Tz (film ) Tj 1.642975 0 Td 56.098172 Tz (fabrication ) Tj 3.980165 0 Td 82.92011 Tz (meth ) Tj 54.693878 0 0 54.693878 0 629.385071 Tm 5.978731 0 Td 52.819237 Tz (ods ) Tj 1.133582 0 Td 47.885572 Tz (include ) Tj 2.19403 0 Td 46.978648 Tz (spin-coating ) Tj 3.547015 0 Td 54.850746 Tz (and ) Tj 1.151866 0 Td 55.721393 Tz (polymer ) Tj 2.468284 0 Td 46.470771 Tz (brushes. ) Tj 2.413433 0 Td 49.010158 Tz (Spin-coating ) Tj 54.603175 0 0 54.603175 0 585.638142 Tm 6.006977 0 Td 43.168605 Tz (\(Weill, ) Tj 1.959593 0 Td 54.94186 Tz (A. ) Tj 0.842442 0 Td 88.517442 Tz (& ) Tj 0.750872 0 Td 53.415698 Tz (Dechenaux, ) Tj 3.424709 0 Td 40.697674 Tz (E., ) Tj 0.952326 0 Td 48.837209 Tz (1998. ) Tj 1.611628 0 Td 62.063953 Tz (The ) Tj 1.281977 0 Td 47.056686 Tz (spin-coating ) Tj 3.534593 0 Td 49.273256 Tz (process ) Tj 54.489796 0 0 54.489796 0 544.769508 Tm 5.982772 0 Td 57.775003 Tz (mechanism ) Tj 3.340075 0 Td 44.569288 Tz (related ) Tj 2.092135 0 Td 44.350811 Tz (to ) Tj 0.734082 0 Td 55.493134 Tz (polymer ) Tj 2.49588 0 Td 46.262484 Tz (solution ) Tj 2.40412 0 Td 44.489842 Tz (properties. ) Tj 3.193258 0 Td 54.182272 Tz (Polymer ) Tj 54.464286 0 0 54.464286 0 502.801508 Tm 6.003934 0 Td 51.465474 Tz (Engineering ) Tj 3.65377 0 Td 60.182149 Tz (and ) Tj 1.303607 0 Td 49.836066 Tz (Science ) Tj 2.386885 0 Td 44.881603 Tz (28, ) Tj 1.101639 0 Td 53.169399 Tz (945-948\) ) Tj 2.79082 0 Td 53.041894 Tz (can ) Tj 1.230164 0 Td 43.224044 Tz (reliably ) Tj 2.386885 0 Td 45.901639 Tz (create ) Tj 54.603175 0 0 54.603175 0 459.141113 Tm 5.988663 0 Td 45.784884 Tz (films ) Tj 1.739826 0 Td 50.363372 Tz (with ) Tj 1.611628 0 Td 47.172304 Tz (thicknesses ) Tj 3.497965 0 Td 62.572674 Tz (down ) Tj 1.886337 0 Td 41.206395 Tz (to ) Tj 0.87907 0 Td 59.011628 Tz (200 ) Tj 1.428488 0 Td 70.203488 Tz (nm ) Tj 1.227035 0 Td 51.889535 Tz (while ) Tj 1.886337 0 Td 55.813953 Tz (polymer ) Tj 52.857143 0 0 52.857143 0 419.07601 Tm 6.167568 0 Td 52.252252 Tz (brushes ) Tj 2.289189 0 Td 49.399399 Tz (are ) Tj 1.021622 0 Td 47.822823 Tz (useful ) Tj 1.854054 0 Td 47.297297 Tz (for ) Tj 0.927027 0 Td 56.756757 Tz (growing ) Tj 2.478378 0 Td 47.297297 Tz (films ) Tj 1.532432 0 Td 45.720721 Tz (that ) Tj 1.191892 0 Td 49.399399 Tz (are ) Tj 0.964865 0 Td 53.603604 Tz (about ) Tj 1.797297 0 Td 54.129129 Tz (10-500 ) Tj 2.062162 0 Td 51.501502 Tz (nm. ) Tj 54.404762 0 0 54.404762 0 377.464634 Tm 5.992123 0 Td 47.177243 Tz (thick ) Tj 1.507221 0 Td 48.504741 Tz (\(Dyer, ) Tj 1.893217 0 Td 45.339168 Tz (D.J., ) Tj 1.507221 0 Td 50.853392 Tz (Feng, ) Tj 1.654267 0 Td 32.676878 Tz (J., ) Tj 0.73523 0 Td 50.929978 Tz (Schmidt, ) Tj 2.591685 0 Td 41.86725 Tz (R., ) Tj 0.900656 0 Td 58.818381 Tz (Wong, ) Tj 1.856455 0 Td 47.483589 Tz (V. ) Tj 0.716849 0 Td 65.864333 Tz (N. ) Tj 0.937418 0 Td 52.691466 Tz (Zhao, ) Tj 1.672648 0 Td 44.420131 Tz (T. ) Tj 52.857143 0 0 52.857143 0 338.017094 Tm 6.186486 0 Td 88.288288 Tz (& ) Tj 0.7 0 Td 49.924925 Tz (Yagci, ) Tj 1.967568 0 Td 42.042042 Tz (Y., ) Tj 0.983784 0 Td 52.342342 Tz (2004, ) Tj 1.816216 0 Td 53.866366 Tz (Photoinduced ) Tj 4.067568 0 Td 51.126126 Tz (polymerization ) Tj 4.540541 0 Td 55.968468 Tz (from ) Tj 1.589189 0 Td 73.573574 Tz (dim ) Tj 54.857143 0 0 54.857143 0 297.300236 Tm 5.960938 0 Td 49.334491 Tz (ethylamino-terminated ) Tj 6.453125 0 Td 47.743056 Tz (self-assembled ) Tj 4.283854 0 Td 52.256944 Tz (monolayers ) Tj 3.354167 0 Td 56.206597 Tz (on ) Tj 0.875 0 Td 46.180556 Tz (gold. ) Tj 54.897959 0 0 54.897959 0 250.312281 Tm 5.956506 0 Td 53.562577 Tz (Macromolecules ) Tj 4.626766 0 Td 51.610905 Tz (37,7072-7074\). ) Tj 4.462825 0 Td 56.923792 Tz (Such ) Tj 1.49368 0 Td 51.610905 Tz (bulky ) Tj 1.675836 0 Td 46.551012 Tz (thickness ) Tj 2.65948 0 Td 36.431227 Tz (is ) Tj 0.5829 0 Td 48.574969 Tz (not ) Tj 54.571429 0 0 54.571429 0 212.062871 Tm 5.973822 0 Td 44.114795 Tz (practical ) Tj 2.492147 0 Td 61.84555 Tz (when ) Tj 1.612565 0 Td 47.338569 Tz (coatings ) Tj 2.382199 0 Td 47.847586 Tz (are ) Tj 1.007853 0 Td 52.937755 Tz (needed ) Tj 2.015707 0 Td 42.757417 Tz (in ) Tj 0.623037 0 Td 49.629145 Tz (confined ) Tj 2.492147 0 Td 49.883653 Tz (spaces ) Tj 1.905759 0 Td 55.991856 Tz (and ) Tj 1.117801 0 Td 46.829552 Tz (the ) Tj 53 0 0 53 0 171.397797 Tm 6.169811 0 Td 52.672956 Tz (chemical ) Tj 2.716981 0 Td 56.918239 Tz (components ) Tj 3.622642 0 Td 56.603774 Tz (of ) Tj 0.773585 0 Td 53.459119 Tz (such ) Tj 1.471698 0 Td 49.13522 Tz (coatings ) Tj 2.54717 0 Td 67.085954 Tz (may ) Tj 1.415094 0 Td 49.056604 Tz (leach ) Tj 1.679245 0 Td 49.266247 Tz (out ) Tj 1.075472 0 Td 58.176101 Tz (of ) Tj 0.773585 0 Td 49.266247 Tz (the ) Tj 30 0 0 30 0 2755 Tm 41.833333 0 Td 72.222222 Tz (5 ) Tj 30 0 0 30 0 2547 Tm 41.666667 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.633333 0 Td 75 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.566667 0 Td 80.555556 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.6 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.566667 0 Td 80.555556 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.566667 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.566667 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.6 0 Td 83.333333 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.6 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.633333 0 Td 80.555556 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.633333 0 Td 75 Tz (65 ) Tj 51.428571 0 0 51.428571 0 2969 Tm 33.775 0 Td 74.537037 Tz (2 ) Tj 53.142857 0 0 53.142857 0 2915.850962 Tm 24.481183 0 Td 49.731183 Tz (coating ) Tj 2.22043 0 Td 44.69086 Tz (into ) Tj 1.223118 0 Td 48.088411 Tz (the ) Tj 0.978495 0 Td 51.224612 Tz (environment. ) Tj 3.801075 0 Td 50.440562 Tz (Accordingly, ) Tj 3.801075 0 Td 47.043011 Tz (there ) Tj 1.543011 0 Td 37.634409 Tz (is ) Tj 0.602151 0 Td 50.179211 Tz (a ) Tj 0.47043 0 Td 54.883513 Tz (need ) Tj 1.467742 0 Td 45.997611 Tz (for ) Tj 53.214286 0 0 53.214286 0 2874.584788 Tm 24.448322 0 Td 50.894855 Tz (nanothin ) Tj 2.70604 0 Td 46.353468 Tz (insulating ) Tj 3.044295 0 Td 48.545861 Tz (robust ) Tj 1.973154 0 Td 48.93736 Tz (coatings ) Tj 2.612081 0 Td 43.847875 Tz (to ) Tj 0.789262 0 Td 49.66443 Tz (address ) Tj 2.367785 0 Td 48.85906 Tz (these ) Tj 1.710067 0 Td 46.457867 Tz (issues ) Tj 52.857143 0 0 52.857143 0 2834.932897 Tm 24.613514 0 Td 56.756757 Tz (and ) Tj 1.172973 0 Td 51.801802 Tz (provide ) Tj 2.327027 0 Td 53.603604 Tz (a ) Tj 0.52973 0 Td 48.873874 Tz (superior ) Tj 2.478378 0 Td 49.049049 Tz (corrosion ) Tj 2.837838 0 Td 46.150696 Tz (protection. ) Tj 42.142857 0 0 42.142857 0 2757.629845 Tm 35.094915 0 Td 107.909605 Tz (SUMMARY ) Tj 4.722034 0 Td 94.915254 Tz (OF ) Tj 1.305085 0 Td 97.551789 Tz (THE ) Tj 2.064407 0 Td 89.202762 Tz (INVENTION ) Tj 54.603175 0 0 54.603175 0 2668.492958 Tm 24.50407 0 Td 50.363372 Tz (This ) Tj 1.428488 0 Td 47.141473 Tz (invention ) Tj 2.728779 0 Td 47.141473 Tz (describes ) Tj 2.728779 0 Td 51.889535 Tz (a ) Tj 0.512791 0 Td 61.046512 Tz (new ) Tj 1.318605 0 Td 56.468023 Tz (method ) Tj 2.234302 0 Td 46.802326 Tz (for ) Tj 0.952326 0 Td 49.515504 Tz (preparing ) Tj 2.838663 0 Td 43.49564 Tz (soft ) Tj 42.857143 0 0 42.857143 0 2632.957233 Tm 30.356667 0 Td 63.194444 Tz (nanothin ) Tj 3.29 0 Td 58.333333 Tz (films ) Tj 1.96 0 Td 64.166667 Tz (with ) Tj 1.796667 0 Td 60.10101 Tz (thicknesses ) Tj 4.153333 0 Td 70 Tz (between ) Tj 3.22 0 Td 42.777778 Tz (1 ) Tj 0.606667 0 Td 89.444444 Tz (nm ) Tj 1.283333 0 Td 72.592593 Tz (and ) Tj 1.516667 0 Td 70 Tz (5 ) Tj 0.676667 0 Td 72.592593 Tz (nm. ) Tj 1.493333 0 Td 79.722222 Tz (As ) Tj 54.642857 0 0 54.642857 0 2585.357977 Tm 23.79085 0 Td 47.41533 Tz (thicknesses ) Tj 3.403922 0 Td 46.895425 Tz (increase ) Tj 2.50719 0 Td 54.901961 Tz (above ) Tj 1.95817 0 Td 33.551198 Tz (1 ) Tj 0.585621 0 Td 70.152505 Tz (nm ) Tj 1.152941 0 Td 45.751634 Tz (the ) Tj 1.134641 0 Td 46.090535 Tz (materials ) Tj 2.983007 0 Td 45.446623 Tz (properties ) Tj 51.785714 0 0 51.785714 0 2544.887199 Tm 25.122759 0 Td 56.858238 Tz (change ) Tj 2.336552 0 Td 56.321839 Tz (from ) Tj 1.66069 0 Td 59.003831 Tz (two ) Tj 1.371034 0 Td 52.957158 Tz (dimensional ) Tj 3.804138 0 Td 45.057471 Tz (to ) Tj 0.811034 0 Td 48.91954 Tz (three ) Tj 1.737931 0 Td 50.957854 Tz (dimensional. ) Tj 4.016552 0 Td 53.425287 Tz (Films ) Tj 42.987013 0 0 42.987013 0 2508.9437 Tm 30.241692 0 Td 64.942095 Tz (with ) Tj 1.907553 0 Td 59.919436 Tz (thicknesses ) Tj 4.280363 0 Td 69.234642 Tz (between ) Tj 3.349849 0 Td 38.7714 Tz (1 ) Tj 0.697885 0 Td 87.23565 Tz (nm ) Tj 1.419033 0 Td 69.78852 Tz (and ) Tj 1.674924 0 Td 67.84995 Tz (10 ) Tj 1.163142 0 Td 87.23565 Tz (nm ) Tj 1.372508 0 Td 60.74186 Tz (are ) Tj 1.39577 0 Td 73.66566 Tz (of ) Tj 1.116616 0 Td 53.310675 Tz (interest ) Tj 54.571429 0 0 54.571429 0 2461.020101 Tm 23.82199 0 Td 52.356021 Tz (because ) Tj 2.382199 0 Td 48.86562 Tz (they ) Tj 1.410995 0 Td 46.829552 Tz (are ) Tj 1.062827 0 Td 50.222998 Tz (extremely ) Tj 2.931937 0 Td 44.284468 Tz (thin ) Tj 1.301047 0 Td 50.901687 Tz (\(on ) Tj 1.099476 0 Td 51.919721 Tz (a ) Tj 0.549738 0 Td 51.241032 Tz (molecular ) Tj 2.950262 0 Td 40.575916 Tz (level\), ) Tj 1.905759 0 Td 49.883653 Tz (but ) Tj 53.214286 0 0 53.214286 0 2419.312048 Tm 24.42953 0 Td 44.369873 Tz (retain ) Tj 1.785235 0 Td 47.606264 Tz (three ) Tj 1.634899 0 Td 51.250763 Tz (dimensional ) Tj 3.57047 0 Td 45.271507 Tz (properties. ) Tj 3.175839 0 Td 61.595824 Tz (The ) Tj 1.277852 0 Td 58.985831 Tz (method ) Tj 2.273826 0 Td 47.762864 Tz (also ) Tj 1.35302 0 Td 43.400447 Tz (results ) Tj 42.97619 0 0 42.97619 0 2383.961588 Tm 30.272576 0 Td 54.293629 Tz (in ) Tj 0.907479 0 Td 60.757156 Tz (the ) Tj 1.349584 0 Td 56.408965 Tz (fabrication ) Tj 3.978947 0 Td 71.745152 Tz (of ) Tj 0.954017 0 Td 69.806094 Tz (a ) Tj 0.698061 0 Td 76.269621 Tz (new ) Tj 1.698615 0 Td 58.171745 Tz (material ) Tj 3.071468 0 Td 54.293629 Tz (that ) Tj 1.559003 0 Td 65.927978 Tz (can ) Tj 1.442659 0 Td 65.152355 Tz (cover ) Tj 2.163989 0 Td 67.867036 Tz (an ) Tj 1.093629 0 Td 55.586334 Tz (entire ) Tj 54.444444 0 0 54.444444 0 2336.523136 Tm 23.895918 0 Td 44.387755 Tz (Surface. ) Tj 2.442857 0 Td 56.632653 Tz (Even ) Tj 1.634694 0 Td 52.55102 Tz (though ) Tj 2.185714 0 Td 35.714286 Tz (its ) Tj 0.9 0 Td 47.278912 Tz (thickness ) Tj 2.828571 0 Td 38.265306 Tz (is ) Tj 0.716327 0 Td 50.680272 Tz (extremely ) Tj 3.012245 0 Td 45.918367 Tz (small, ) Tj 1.928571 0 Td 47.959184 Tz (the ) Tj 54.464286 0 0 54.464286 0 2298.066167 Tm 23.887213 0 Td 48.52459 Tz (coating ) Tj 2.295082 0 Td 49.981785 Tz (has ) Tj 1.156721 0 Td 45.901639 Tz (excellent ) Tj 2.735738 0 Td 44.677596 Tz (insulating ) Tj 2.900984 0 Td 44.232489 Tz (properties. ) Tj 3.249836 0 Td 42.84153 Tz (In ) Tj 0.752787 0 Td 45.027322 Tz (theory, ) Tj 2.148197 0 Td 53.551913 Tz (such ) Tj 53.015873 0 0 53.015873 0 2253.723485 Tm 24.53982 0 Td 47.155689 Tz (films ) Tj 1.65988 0 Td 52.185629 Tz (could ) Tj 1.810778 0 Td 56.586826 Tz (be ) Tj 0.943114 0 Td 47.155689 Tz (useful ) Tj 1.961677 0 Td 48.203593 Tz (for ) Tj 1.056287 0 Td 47.155689 Tz (applications ) Tj 3.678144 0 Td 45.583832 Tz (in ) Tj 0.792216 0 Td 52.657186 Tz (chemical ) Tj 2.791617 0 Td 46.762725 Tz (sensors, ) Tj 50.357143 0 0 50.357143 0 2212.611382 Tm 25.835461 0 Td 49.438534 Tz (nano-insulators, ) Tj 4.924823 0 Td 61.78093 Tz (and ) Tj 1.310638 0 Td 55.529288 Tz (molecular ) Tj 3.157447 0 Td 46.611505 Tz (electronics. ) Tj 54.642857 0 0 54.642857 0 2168.57598 Tm 24.504575 0 Td 57.674787 Tz (Embodiments ) Tj 3.934641 0 Td 48.801743 Tz (of ) Tj 0.677124 0 Td 44.734931 Tz (the ) Tj 0.933333 0 Td 47.494553 Tz (present ) Tj 2.104575 0 Td 47.446139 Tz (invention ) Tj 2.671895 0 Td 47.494553 Tz (include ) Tj 2.104575 0 Td 48.801743 Tz (a ) Tj 0.439216 0 Td 60.239651 Tz (compound ) Tj 54.761905 0 0 54.761905 0 2129.350063 Tm 23.757391 0 Td 56.304348 Tz (of ) Tj 0.949565 0 Td 48.478261 Tz (4-vinylbenezenepropanethiol, ) Tj 8.546087 0 Td 51.73913 Tz (a ) Tj 0.730435 0 Td 54.782609 Tz (polymer ) Tj 2.684348 0 Td 43.75 Tz (thereof, ) Tj 2.483478 0 Td 56.811594 Tz (and ) Tj 43.142857 0 0 43.142857 0 2090.936085 Tm 30.155629 0 Td 69.536424 Tz (methods ) Tj 3.31457 0 Td 69.536424 Tz (of ) Tj 1.135762 0 Td 63.097866 Tz (use ) Tj 1.529801 0 Td 54.083885 Tz (thereof. ) Tj 3.059603 0 Td 63.097866 Tz (Disclosed ) Tj 3.754967 0 Td 60.522443 Tz (herein ) Tj 2.596026 0 Td 46.357616 Tz (is ) Tj 0.950331 0 Td 61.810155 Tz (a ) Tj 0.788079 0 Td 72.111847 Tz (method ) Tj 2.990066 0 Td 67.604857 Tz (of ) Tj 53.428571 0 0 53.428571 0 2046.636047 Tm 24.350267 0 Td 58.229352 Tz (making ) Tj 2.283422 0 Td 49.465241 Tz (4-vinylbenezenepropanethiol. ) Tj 8.47861 0 Td 54.590018 Tz (Also ) Tj 1.516043 0 Td 48.177857 Tz (disclosed ) Tj 2.770053 0 Td 49.390969 Tz (herein ) Tj 52.987013 0 0 52.987013 0 2004.103356 Tm 24.553186 0 Td 37.745098 Tz (is ) Tj 0.754902 0 Td 53.472222 Tz (a ) Tj 0.679412 0 Td 57.666122 Tz (method ) Tj 2.377941 0 Td 56.617647 Tz (of ) Tj 0.88701 0 Td 51.89951 Tz (applying ) Tj 2.774265 0 Td 45.60866 Tz (that ) Tj 1.377696 0 Td 62.122141 Tz (compound ) Tj 3.264951 0 Td 48.754085 Tz (to ) Tj 0.868137 0 Td 50.326797 Tz (a ) Tj 0.622794 0 Td 48.229847 Tz (metal. ) Tj 2.019363 0 Td 55.831291 Tz (That ) Tj 54.761905 0 0 54.761905 0 1963.159353 Tm 23.757391 0 Td 56.811594 Tz (method ) Tj 2.173043 0 Td 47.173913 Tz (includes ) Tj 2.373913 0 Td 49.371981 Tz (providing ) Tj 2.775652 0 Td 49.146538 Tz (4-vinylbenezenepropanethiol ) Tj 8.071304 0 Td 47.173913 Tz (as ) Tj 0.712174 0 Td 51.73913 Tz (a ) Tj 54.428571 0 0 54.428571 0 1919.554202 Tm 23.902887 0 Td 45.931759 Tz (Solution ) Tj 2.370079 0 Td 42.869641 Tz (in ) Tj 0.67979 0 Td 53.587052 Tz (an ) Tj 0.790026 0 Td 48.993876 Tz (organic ) Tj 2.223097 0 Td 44.017935 Tz (solvent, ) Tj 2.278215 0 Td 49.674346 Tz (providing ) Tj 2.811024 0 Td 52.055993 Tz (a ) Tj 0.47769 0 Td 46.442111 Tz (metal, ) Tj 1.855643 0 Td 48.118985 Tz (placing ) Tj 2.167979 0 Td 47.97317 Tz (the ) Tj 54.642857 0 0 54.642857 0 1878.836165 Tm 23.79085 0 Td 51.24183 Tz (metal ) Tj 1.720261 0 Td 45.751634 Tz (in ) Tj 0.750327 0 Td 46.768337 Tz (the ) Tj 1.061438 0 Td 45.751634 Tz (solution ) Tj 2.415686 0 Td 54.901961 Tz (of ) Tj 0.786928 0 Td 49.153679 Tz (4-vinylbenzenepropanethiol ) Tj 7.869281 0 Td 48.801743 Tz (so ) Tj 0.823529 0 Td 43.464052 Tz (that ) Tj 54.415584 0 0 54.415584 0 1834.304878 Tm 23.890215 0 Td 47.984619 Tz (the ) Tj 0.992363 0 Td 45.942721 Tz (Solution ) Tj 2.370644 0 Td 35.222753 Tz (is ) Tj 0.588067 0 Td 41.348449 Tz (in ) Tj 0.624821 0 Td 47.25537 Tz (contact ) Tj 2.113365 0 Td 50.536993 Tz (with ) Tj 1.341527 0 Td 46.96367 Tz (the ) Tj 1.01074 0 Td 49.618138 Tz (metal ) Tj 1.635561 0 Td 43.645585 Tz (surface, ) Tj 2.260382 0 Td 55.131265 Tz (and ) Tj 1.139379 0 Td 51.302705 Tz (exposing ) Tj 51.428571 0 0 51.428571 0 1794.024155 Tm 25.277778 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 53.240741 Tz (mixture ) Tj 2.411111 0 Td 46.990741 Tz (to ) Tj 0.777778 0 Td 45.075758 Tz (ultraviolet ) Tj 3.169444 0 Td 45.694444 Tz (radiation. ) Tj 2.955556 0 Td 48.611111 Tz (In ) Tj 0.777778 0 Td 47.222222 Tz (certain ) Tj 2.158333 0 Td 56.983025 Tz (embodiments, ) Tj 53.214286 0 0 53.214286 0 1752.095808 Tm 24.448322 0 Td 53.243848 Tz (exposing ) Tj 2.687248 0 Td 48.023863 Tz (the ) Tj 1.052349 0 Td 51.006711 Tz (mixture ) Tj 2.311409 0 Td 45.41387 Tz (to ) Tj 0.732886 0 Td 43.563148 Tz (ultraviolet ) Tj 3.044295 0 Td 45.935869 Tz (radiation ) Tj 2.649664 0 Td 45.637584 Tz (further ) Tj 2.085906 0 Td 48.154362 Tz (includes ) Tj 54.444444 0 0 54.444444 0 1711.199023 Tm 23.895918 0 Td 51.27551 Tz (exposing ) Tj 2.644898 0 Td 46.938776 Tz (the ) Tj 1.046939 0 Td 50.728863 Tz (mixture ) Tj 2.314286 0 Td 41.326531 Tz (to ) Tj 0.697959 0 Td 42.857143 Tz (ultraviolet ) Tj 2.993878 0 Td 45.238095 Tz (radiation ) Tj 2.626531 0 Td 52.040816 Tz (having ) Tj 2.020408 0 Td 55.102041 Tz (a ) Tj 0.514286 0 Td 68.112245 Tz (wave ) Tj 51.571429 0 0 51.571429 0 1669.899117 Tm 25.227147 0 Td 50.092336 Tz (length ) Tj 2.036011 0 Td 58.171745 Tz (of ) Tj 0.833795 0 Td 58.171745 Tz (from ) Tj 1.648199 0 Td 54.293629 Tz (about ) Tj 1.861496 0 Td 59.249 Tz (200 ) Tj 1.33795 0 Td 54.939982 Tz (nanometers ) Tj 3.529086 0 Td 45.244691 Tz (to ) Tj 0.775623 0 Td 54.939982 Tz (about ) Tj 1.842105 0 Td 62.480763 Tz (300 ) Tj 1.376731 0 Td 72.391505 Tz (nanom ) Tj 44.395604 0 0 44.395604 0 1631.928121 Tm 29.304703 0 Td 51.806931 Tz (eters ) Tj 1.779455 0 Td 55.060506 Tz (for ) Tj 1.126238 0 Td 63.820132 Tz (a ) Tj 0.563119 0 Td 58.188944 Tz (duration ) Tj 2.995792 0 Td 63.820132 Tz (of ) Tj 0.855941 0 Td 67.574257 Tz (from ) Tj 1.80198 0 Td 63.820132 Tz (about ) Tj 2.162376 0 Td 63.820132 Tz (10 ) Tj 0.94604 0 Td 62.747525 Tz (minutes ) Tj 2.838119 0 Td 50.680693 Tz (to ) Tj 0.810891 0 Td 63.069307 Tz (about ) Tj 2.139851 0 Td 37.541254 Tz (1 ) Tj 0.47302 0 Td 57.062706 Tz (hour. ) Tj 50.31746 0 0 50.31746 0 1585.799751 Tm 25.87571 0 Td 48.028391 Tz (In ) Tj 0.8347 0 Td 51.671924 Tz (other ) Tj 1.729022 0 Td 58.241325 Tz (embodiments, ) Tj 4.451735 0 Td 48.580442 Tz (the ) Tj 1.132808 0 Td 46.071121 Tz (ultraviolet ) Tj 3.259306 0 Td 48.580442 Tz (radiation ) Tj 2.86183 0 Td 54.100946 Tz (has ) Tj 1.192429 0 Td 59.621451 Tz (a ) Tj 0.576341 0 Td 74.526814 Tz (wave ) Tj 54.428571 0 0 54.428571 0 1542.508621 Tm 23.902887 0 Td 47.462817 Tz (length ) Tj 1.892388 0 Td 55.11811 Tz (of ) Tj 0.734908 0 Td 52.055993 Tz (about ) Tj 1.727034 0 Td 48.993876 Tz (255. ) Tj 1.396325 0 Td 47.462817 Tz (In ) Tj 0.716535 0 Td 45.056868 Tz (certain ) Tj 2.076115 0 Td 53.331875 Tz (embodiments, ) Tj 4.060367 0 Td 45.931759 Tz (the ) Tj 1.010499 0 Td 50.831146 Tz (metal ) Tj 1.727034 0 Td 64.304462 Tz (may ) Tj 53.015873 0 0 53.015873 0 1504.206388 Tm 24.520958 0 Td 59.730539 Tz (be ) Tj 0.886527 0 Td 48.952096 Tz (copper, ) Tj 2.301198 0 Td 47.155689 Tz (gold, ) Tj 1.65988 0 Td 49.600798 Tz (platinum, ) Tj 2.923653 0 Td 51.871257 Tz (or ) Tj 0.811078 0 Td 42.754491 Tz (iron. ) Tj 1.49012 0 Td 56.137725 Tz (Another ) Tj 2.546407 0 Td 59.101796 Tz (embodiment ) Tj 3.753593 0 Td 56.586826 Tz (of ) Tj 53 0 0 53 0 1461.929134 Tm 24.509434 0 Td 50.314465 Tz (the ) Tj 1.188679 0 Td 58.70021 Tz (method ) Tj 2.415094 0 Td 56.603774 Tz (of ) Tj 0.886792 0 Td 51.493711 Tz (applying ) Tj 2.754717 0 Td 53.459119 Tz (a ) Tj 0.622642 0 Td 61.713836 Tz (compound ) Tj 3.264151 0 Td 45.597484 Tz (to ) Tj 0.830189 0 Td 53.459119 Tz (a ) Tj 0.622642 0 Td 47.69392 Tz (metal, ) Tj 2.056604 0 Td 48.742138 Tz (includes ) Tj 54.761905 0 0 54.761905 0 1423.276066 Tm 23.73913 0 Td 49.371981 Tz (providing ) Tj 2.848696 0 Td 48.132045 Tz (4-vinylbenzenepropanethiol, ) Tj 8.016522 0 Td 49.033816 Tz (providing ) Tj 2.830435 0 Td 48.695652 Tz (a ) Tj 0.493043 0 Td 49.304348 Tz (metal ) Tj 1.716522 0 Td 44.130435 Tz (in ) Tj 54.693878 0 0 54.693878 0 1380.010856 Tm 23.78694 0 Td 49.626866 Tz (hexane, ) Tj 2.303731 0 Td 48.320896 Tz (placing ) Tj 2.212313 0 Td 46.72471 Tz (the ) Tj 1.042164 0 Td 49.107826 Tz (4-vinylbenzenepropanethiol ) Tj 7.898507 0 Td 42.661692 Tz (in ) Tj 0.731343 0 Td 45.708955 Tz (the ) Tj 1.042164 0 Td 67.039801 Tz (hex ) Tj 54.52381 0 0 54.52381 0 1335.1313 Tm 23.861135 0 Td 52.983988 Tz (ane ) Tj 1.21048 0 Td 48.908297 Tz (with ) Tj 1.430568 0 Td 46.870451 Tz (the ) Tj 1.118777 0 Td 48.908297 Tz (metal ) Tj 1.724017 0 Td 44.323144 Tz (in ) Tj 0.751965 0 Td 50.131004 Tz (order ) Tj 1.705677 0 Td 41.266376 Tz (to ) Tj 0.751965 0 Td 49.344978 Tz (prepare ) Tj 2.292576 0 Td 51.965066 Tz (a ) Tj 0.568559 0 Td 46.997817 Tz (mixture, ) Tj 2.512664 0 Td 52.474527 Tz (adding ) Tj 2.10917 0 Td 55.021834 Tz (a ) Tj 54.428571 0 0 54.428571 0 1294.369325 Tm 23.884514 0 Td 50.306212 Tz (thermal ) Tj 2.296588 0 Td 44.4007 Tz (free ) Tj 1.249344 0 Td 43.744532 Tz (radical ) Tj 2.020997 0 Td 40.82823 Tz (initiator ) Tj 2.333333 0 Td 52.821522 Tz (such ) Tj 1.433071 0 Td 47.462817 Tz (as ) Tj 0.734908 0 Td 51.618548 Tz (benzoyl ) Tj 2.333333 0 Td 50.524934 Tz (peroxide ) Tj 2.608924 0 Td 39.807524 Tz (to ) Tj 0.698163 0 Td 46.952464 Tz (the ) Tj 54.571429 0 0 54.571429 0 1252.386473 Tm 23.840314 0 Td 47.338569 Tz (mixture, ) Tj 2.437173 0 Td 54.973822 Tz (and ) Tj 1.136126 0 Td 47.949389 Tz (incubating ) Tj 3.02356 0 Td 45.811518 Tz (the ) Tj 0.971204 0 Td 50.61082 Tz (mixture ) Tj 2.235602 0 Td 42.757417 Tz (at ) Tj 0.67801 0 Td 52.683246 Tz (from ) Tj 1.410995 0 Td 51.308901 Tz (about ) Tj 1.685864 0 Td 58.027923 Tz (50 ) Tj 0.806283 0 Td 49.30192 Tz (degrees ) Tj 53.015873 0 0 53.015873 0 1211.067146 Tm 24.53982 0 Td 49.850299 Tz (Celsius ) Tj 2.225749 0 Td 44.011976 Tz (to ) Tj 0.679042 0 Td 52.814371 Tz (about ) Tj 1.716467 0 Td 61.302395 Tz (90 ) Tj 0.848802 0 Td 50.748503 Tz (degrees ) Tj 2.301198 0 Td 46.762725 Tz (Celsius. ) Tj 2.433234 0 Td 45.583832 Tz (In ) Tj 0.679042 0 Td 45.808383 Tz (certain ) Tj 2.093713 0 Td 54.752994 Tz (embodiments, ) Tj 52.987013 0 0 52.987013 0 1169.513141 Tm 24.553186 0 Td 49.697712 Tz (incubating ) Tj 3.151716 0 Td 48.229847 Tz (the ) Tj 1.075735 0 Td 51.674837 Tz (mixture ) Tj 2.340196 0 Td 37.745098 Tz (is ) Tj 0.641667 0 Td 55.831291 Tz (from ) Tj 1.528676 0 Td 52.843137 Tz (about ) Tj 1.811765 0 Td 53.472222 Tz (15 ) Tj 0.81152 0 Td 53.022876 Tz (minutes ) Tj 2.415686 0 Td 45.60866 Tz (to ) Tj 0.717157 0 Td 52.843137 Tz (about ) Tj 1.755147 0 Td 56.617647 Tz (24 ) Tj 50.31746 0 0 50.31746 0 1128.913965 Tm 25.835962 0 Td 50.788644 Tz (hours. ) Tj 2.126498 0 Td 44.716088 Tz (In ) Tj 0.775079 0 Td 48.264984 Tz (certain ) Tj 2.245741 0 Td 58.51735 Tz (embodiments, ) Tj 4.431861 0 Td 50.788644 Tz (the ) Tj 1.152681 0 Td 53.470032 Tz (thermal ) Tj 2.484227 0 Td 48.028391 Tz (free ) Tj 1.391167 0 Td 47.791798 Tz (radical ) Tj 2.245741 0 Td 56.309148 Tz (ini ) Tj 53.214286 0 0 53.214286 0 1087.438961 Tm 24.42953 0 Td 42.281879 Tz (tiator ) Tj 1.879195 0 Td 36.017897 Tz (is ) Tj 0.789262 0 Td 52.796421 Tz (benzoyl ) Tj 2.574497 0 Td 48.371862 Tz (peroxide. ) Tj 2.987919 0 Td 38.836689 Tz (Still ) Tj 1.503356 0 Td 51.454139 Tz (another ) Tj 2.461745 0 Td 58.881432 Tz (embodiment ) Tj 3.908725 0 Td 45.935869 Tz (for ) Tj 54.642857 0 0 54.642857 0 1047.276675 Tm 23.80915 0 Td 49.945534 Tz (applying ) Tj 2.616993 0 Td 51.851852 Tz (a ) Tj 0.54902 0 Td 60.620915 Tz (compound ) Tj 3.129412 0 Td 44.22658 Tz (to ) Tj 0.786928 0 Td 49.411765 Tz (metal ) Tj 1.775163 0 Td 47.276688 Tz (includes ) Tj 2.488889 0 Td 49.140644 Tz (providing ) Tj 2.891503 0 Td 52.287582 Tz (4-vinyl ) Tj 55 0 0 55 0 1008.125313 Tm 23.636364 0 Td 48.787879 Tz (benzenepropanethiol, ) Tj 6.472727 0 Td 51.893939 Tz (exposing ) Tj 3.072727 0 Td 47.474747 Tz (the ) Tj 1.490909 0 Td 52.049911 Tz (4-vinylbenzenepro ) Tj 52.987013 0 0 52.987013 0 963.152795 Tm 24.534314 0 Td 48.579339 Tz (panethiol ) Tj 2.830882 0 Td 44.035948 Tz (to ) Tj 0.717157 0 Td 44.035948 Tz (air ) Tj 0.943627 0 Td 44.035948 Tz (at ) Tj 0.698284 0 Td 61.335784 Tz (room ) Tj 1.660784 0 Td 51.470588 Tz (temperature ) Tj 3.566912 0 Td 46.132898 Tz (for ) Tj 1.019118 0 Td 55.831291 Tz (from ) Tj 1.528676 0 Td 53.472222 Tz (about ) Tj 1.755147 0 Td 61.335784 Tz (30 ) Tj 0.905882 0 Td 74.441721 Tz (min ) Tj 42.040816 0 0 42.040816 0 925.325581 Tm 30.92233 0 Td 61.44822 Tz (utes ) Tj 3.139806 0 Td 61.44822 Tz (to ) Tj 2.45 0 Td 67.394822 Tz (about ) Tj 3.686893 0 Td 75.323625 Tz (24 ) Tj 2.616505 0 Td 60.787487 Tz (hours, ) Tj 3.924757 0 Td 57.979369 Tz (diluting ) Tj 4.448058 0 Td 63.430421 Tz (the ) Tj 54.693878 0 0 54.693878 0 882.233533 Tm 23.78694 0 Td 49.107826 Tz (4-vinylbenzenepropanethiol ) Tj 7.843657 0 Td 55.866501 Tz (and ) Tj 1.206716 0 Td 35.55141 Tz (its ) Tj 0.841045 0 Td 50.787728 Tz (oligomers ) Tj 2.943657 0 Td 42.661692 Tz (in ) Tj 0.694776 0 Td 54.850746 Tz (an ) Tj 0.859328 0 Td 48.756219 Tz (organic ) Tj 54.415584 0 0 54.415584 0 836.55811 Tm 23.926969 0 Td 46.81782 Tz (solvent ) Tj 2.150119 0 Td 42.879873 Tz (to ) Tj 0.735084 0 Td 52.068417 Tz (about ) Tj 1.800955 0 Td 68.914081 Tz (1% ) Tj 1.029117 0 Td 53.599841 Tz (w/w, ) Tj 1.506921 0 Td 55.131265 Tz (and ) Tj 1.212888 0 Td 47.78043 Tz (contacting ) Tj 3.050597 0 Td 46.96367 Tz (the ) Tj 1.029117 0 Td 50.230708 Tz (metal ) Tj 1.727446 0 Td 50.536993 Tz (with ) Tj 1.433413 0 Td 44.921771 Tz (the ) Tj 54.693878 0 0 54.693878 0 797.969484 Tm 23.805224 0 Td 44.947139 Tz (Solution ) Tj 2.322015 0 Td 54.850746 Tz (of ) Tj 0.731343 0 Td 48.990624 Tz (4-vinylbenzenepropanethiol ) Tj 7.788806 0 Td 54.850746 Tz (and ) Tj 1.151866 0 Td 36.567164 Tz (its ) Tj 0.786194 0 Td 48.451493 Tz (oligomers. ) Tj 3.071642 0 Td 47.232587 Tz (In ) Tj 54.693878 0 0 54.693878 0 752.302462 Tm 23.78694 0 Td 43.967662 Tz (certain ) Tj 2.011194 0 Td 53.327114 Tz (embodiments, ) Tj 3.967537 0 Td 46.72471 Tz (the ) Tj 0.987313 0 Td 56.374378 Tz (method ) Tj 2.175746 0 Td 44.838308 Tz (further ) Tj 1.974627 0 Td 47.232587 Tz (includes ) Tj 2.413433 0 Td 48.146766 Tz (incubating ) Tj 54.642857 0 0 54.642857 0 713.854722 Tm 23.79085 0 Td 47.78504 Tz (the ) Tj 1.061438 0 Td 50.631808 Tz (metal ) Tj 1.738562 0 Td 44.22658 Tz (in ) Tj 0.732026 0 Td 46.768337 Tz (the ) Tj 1.043137 0 Td 46.132898 Tz (solution ) Tj 2.415686 0 Td 56.427015 Tz (of ) Tj 0.786928 0 Td 49.036367 Tz (4-vinylbenzenepropanethiol ) Tj 7.887582 0 Td 45.751634 Tz (for ) Tj 42.987013 0 0 42.987013 0 675.989432 Tm 30.264955 0 Td 68.819235 Tz (from ) Tj 2.000604 0 Td 65.135952 Tz (about ) Tj 2.326284 0 Td 65.91138 Tz (10 ) Tj 1.139879 0 Td 64.249748 Tz (seconds ) Tj 3.047432 0 Td 54.27996 Tz (to ) Tj 0.977039 0 Td 65.135952 Tz (about ) Tj 2.256495 0 Td 73.66566 Tz (40 ) Tj 1.163142 0 Td 59.44948 Tz (hours. ) Tj 2.512387 0 Td 56.21853 Tz (In ) Tj 1.000302 0 Td 55.941591 Tz (certain ) Tj 2.651964 0 Td 62.03424 Tz (other ) Tj 54.444444 0 0 54.444444 0 629.56568 Tm 23.895918 0 Td 53.571429 Tz (embodiments, ) Tj 4.004082 0 Td 48.367347 Tz (incubating ) Tj 2.993878 0 Td 46.938776 Tz (the ) Tj 1.010204 0 Td 49.591837 Tz (metal ) Tj 1.634694 0 Td 42.857143 Tz (in ) Tj 0.62449 0 Td 50 Tz (the ) Tj 1.010204 0 Td 45.535714 Tz (solution ) Tj 2.314286 0 Td 52.040816 Tz (of ) Tj 0.697959 0 Td 52.478134 Tz (4-vinyl ) Tj 53.174603 0 0 53.174603 0 588.877928 Tm 24.447761 0 Td 51.468971 Tz (benzenepropanethiol ) Tj 6.074328 0 Td 47.014925 Tz (for ) Tj 1.034328 0 Td 54.850746 Tz (from ) Tj 1.54209 0 Td 52.029851 Tz (about ) Tj 1.824179 0 Td 51.716418 Tz (10 ) Tj 0.808657 0 Td 52.835821 Tz (seconds ) Tj 2.42597 0 Td 43.880597 Tz (to ) Tj 0.733433 0 Td 52.656716 Tz (about ) Tj 1.748955 0 Td 59.552239 Tz (30 ) Tj 41.428571 0 0 41.428571 0 552 Tm 31.403448 0 Td 63.362069 Tz (minutes. ) Tj 54.603175 0 0 54.603175 0 502.901535 Tm 24.485756 0 Td 54.178779 Tz (Also ) Tj 1.520058 0 Td 47.141473 Tz (disclosed ) Tj 2.728779 0 Td 47.819767 Tz (herein ) Tj 1.922965 0 Td 36.627907 Tz (is ) Tj 0.622674 0 Td 54.94186 Tz (a ) Tj 0.549419 0 Td 56.976744 Tz (method ) Tj 2.234302 0 Td 54.94186 Tz (of ) Tj 0.769186 0 Td 57.485465 Tz (making ) Tj 2.234302 0 Td 53.415698 Tz (4-vinylben ) Tj 54.761905 0 0 54.761905 0 461.753538 Tm 23.757391 0 Td 47.800512 Tz (Zenepropanethiol. ) Tj 5.021739 0 Td 60.869565 Tz (The ) Tj 1.296522 0 Td 56.811594 Tz (method ) Tj 2.227826 0 Td 47.173913 Tz (includes ) Tj 2.428696 0 Td 49.710145 Tz (providing ) Tj 2.921739 0 Td 60 Tz (1-bromo ) Tj 54.52381 0 0 54.52381 0 422.017305 Tm 23.861135 0 Td 50.054585 Tz (3-phenylpropane, ) Tj 5.153712 0 Td 52.474527 Tz (adding ) Tj 2.200873 0 Td 43.813683 Tz (acetic ) Tj 1.925764 0 Td 50.606502 Tz (anhydride ) Tj 3.062882 0 Td 56.040757 Tz (and ) Tj 1.338865 0 Td 58.842795 Tz (aluminum ) Tj 53.142857 0 0 53.142857 0 377.43408 Tm 24.481183 0 Td 45.997611 Tz (chloride, ) Tj 2.69086 0 Td 49.865591 Tz (incubating ) Tj 3.180108 0 Td 47.043011 Tz (the ) Tj 1.072581 0 Td 51.075269 Tz (mixture ) Tj 2.333333 0 Td 43.90681 Tz (at ) Tj 0.733871 0 Td 54.883513 Tz (from ) Tj 1.543011 0 Td 52.688172 Tz (about ) Tj 1.75 0 Td 62.724014 Tz (-20 ) Tj 1.317204 0 Td 42.33871 Tz (to ) Tj 0.715054 0 Td 53.315412 Tz (about ) Tj 51.666667 0 0 51.666667 0 336.987229 Tm 25.180645 0 Td 62.903226 Tz (20 ) Tj 0.909677 0 Td 52.534562 Tz (degrees ) Tj 2.380645 0 Td 51.152074 Tz (Celsius ) Tj 2.341935 0 Td 48.387097 Tz (for ) Tj 1.045161 0 Td 57.258065 Tz (from ) Tj 1.567742 0 Td 54.193548 Tz (about ) Tj 1.877419 0 Td 38.709677 Tz (1 ) Tj 0.483871 0 Td 56.451613 Tz (hour ) Tj 1.548387 0 Td 45.16129 Tz (to ) Tj 0.716129 0 Td 54.193548 Tz (about ) Tj 1.877419 0 Td 54.83871 Tz (12 ) Tj 0.851613 0 Td 48.924731 Tz (hours, ) Tj 54.857143 0 0 54.857143 0 298.683544 Tm 23.716146 0 Td 43.547454 Tz (isolating ) Tj 2.460938 0 Td 47.59838 Tz (the ) Tj 1.002604 0 Td 43.885031 Tz (resulting ) Tj 2.497396 0 Td 50.332755 Tz (p-\(3-bromopropyl\)acetophenone, ) Tj 9.205729 0 Td 66.840278 Tz (add ) Tj 54.761905 0 0 54.761905 0 255.859857 Tm 23.757391 0 Td 48.695652 Tz (ing ) Tj 1.095652 0 Td 54.782609 Tz (sodium ) Tj 2.191304 0 Td 50.355731 Tz (borohydride ) Tj 3.524348 0 Td 44.130435 Tz (to ) Tj 0.748696 0 Td 46.666667 Tz (the ) Tj 1.004348 0 Td 52.226087 Tz (p-\(3-bromopropyl\)acetophe ) Tj 54.428571 0 0 54.428571 0 210.465602 Tm 23.902887 0 Td 55.88364 Tz (none ) Tj 1.506562 0 Td 45.548994 Tz (solution ) Tj 2.388451 0 Td 41.338583 Tz (in ) Tj 0.67979 0 Td 50.354817 Tz (methanol, ) Tj 2.902887 0 Td 48.075241 Tz (incubating ) Tj 3.049869 0 Td 46.952464 Tz (the ) Tj 1.028871 0 Td 50.306212 Tz (mixture ) Tj 2.259843 0 Td 41.338583 Tz (at ) Tj 0.643045 0 Td 51.44357 Tz (about ) Tj 1.708661 0 Td 55.11811 Tz (0 ) Tj 54.603175 0 0 54.603175 0 170.816993 Tm 23.826453 0 Td 49.273256 Tz (degrees ) Tj 2.3625 0 Td 48.401163 Tz (Celsius ) Tj 2.344186 0 Td 45.784884 Tz (for ) Tj 1.080523 0 Td 51.27907 Tz (about ) Tj 1.831395 0 Td 54.94186 Tz (2 ) Tj 0.640988 0 Td 45.784884 Tz (hours, ) Tj 1.996221 0 Td 43.410853 Tz (isolating ) Tj 2.655523 0 Td 46.802326 Tz (the ) Tj 1.153779 0 Td 44.089147 Tz (resulting ) Tj ET Q endstream endobj 300 0 obj << /Length 1 >> stream q endstream endobj 301 0 obj << /Length 47795 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.325 0 Td 83.522727 Tz (US ) Tj 1.240909 0 Td 58.038721 Tz (7,829,155 ) Tj 3.388636 0 Td 68.939394 Tz (B1 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.454054 0 Td 72.522523 Tz (3 ) Tj 51.428571 0 0 51.428571 0 2920.362187 Tm 6.358333 0 Td 54.475309 Tz (p-\(3-bromopropyl\)-O-methylbenzenemethanol, ) Tj 13.922222 0 Td 55.092593 Tz (adding ) Tj 2.177778 0 Td 56.712963 Tz (tolu ) Tj 51.428571 0 0 51.428571 0 2875.718713 Tm 6.358333 0 Td 50.231481 Tz (ensulfonic ) Tj 3.247222 0 Td 50.231481 Tz (acid ) Tj 1.4 0 Td 46.990741 Tz (to ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 48.611111 Tz (solution ) Tj 2.547222 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 57.449495 Tz (p-\(3-bromopropyl\)-O-me ) Tj 51.428571 0 0 51.428571 0 2834.311321 Tm 6.338889 0 Td 54.751462 Tz (thylbenzenemethanol ) Tj 6.416667 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 47.395833 Tz (toluene, ) Tj 2.469444 0 Td 48.971193 Tz (refluxing ) Tj 2.780556 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 53.703704 Tz (mixture ) Tj 2.411111 0 Td 55.740741 Tz (under ) Tj 51.428571 0 0 51.428571 0 2792.399494 Tm 6.358333 0 Td 44.722222 Tz (inert ) Tj 1.613889 0 Td 56.064815 Tz (atmosphere ) Tj 3.655556 0 Td 47.530864 Tz (for ) Tj 1.088889 0 Td 54.444444 Tz (about ) Tj 1.905556 0 Td 61.574074 Tz (4 ) Tj 0.622222 0 Td 50.231481 Tz (hours, ) Tj 2.080556 0 Td 46.8107 Tz (isolating ) Tj 2.780556 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 47.530864 Tz (resulting ) Tj 51.428571 0 0 51.428571 0 2753.172781 Tm 6.358333 0 Td 52.62963 Tz (p-\(3-Bromopropyl\)styrene, ) Tj 8.088889 0 Td 55.092593 Tz (adding ) Tj 2.197222 0 Td 49.016204 Tz (thiourea ) Tj 2.566667 0 Td 45.37037 Tz (to ) Tj 0.758333 0 Td 47.530864 Tz (the ) Tj 1.05 0 Td 58.333333 Tz (p-\(3-Bro ) Tj 51.428571 0 0 51.428571 0 2709.863691 Tm 6.358333 0 Td 52.423747 Tz (mopropyl\)styrene, ) Tj 5.541667 0 Td 50.231481 Tz (gently ) Tj 2.002778 0 Td 48.971193 Tz (refluxing ) Tj 2.8 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 53.703704 Tz (mixture ) Tj 2.469444 0 Td 47.530864 Tz (for ) Tj 0.991667 0 Td 55.092593 Tz (about ) Tj 1.905556 0 Td 53.472222 Tz (16 ) Tj 51.428571 0 0 51.428571 0 2668.952381 Tm 6.338889 0 Td 50.231481 Tz (hours, ) Tj 2.080556 0 Td 56.17284 Tz (adding ) Tj 2.294444 0 Td 58.873457 Tz (sodium ) Tj 2.411111 0 Td 52.5 Tz (hydroxide, ) Tj 3.422222 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 50.231481 Tz (gently ) Tj 2.119444 0 Td 48.611111 Tz (refluxing ) Tj 2.897222 0 Td 50.771605 Tz (the ) Tj 40 0 0 40 0 2630 Tm 8.225 0 Td 68.452381 Tz (mixture ) Tj 3.1 0 Td 62.5 Tz (for ) Tj 1.3 0 Td 70.833333 Tz (about ) Tj 2.325 0 Td 79.166667 Tz (4 ) Tj 0.675 0 Td 64.583333 Tz (hours. ) Tj 51.428571 0 0 51.428571 0 2584.016561 Tm 7.097222 0 Td 52.662037 Tz (This ) Tj 1.477778 0 Td 50.05144 Tz (invention ) Tj 2.916667 0 Td 49.691358 Tz (describes ) Tj 2.877778 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 52.256944 Tz (nanothin ) Tj 2.722222 0 Td 57.87037 Tz (polymer ) Tj 2.644444 0 Td 50.462963 Tz (coating ) Tj 2.313889 0 Td 66.975309 Tz (pro ) Tj 51.428571 0 0 51.428571 0 2542.319461 Tm 6.358333 0 Td 58.333333 Tz (duced ) Tj 1.905556 0 Td 58.333333 Tz (by ) Tj 0.875 0 Td 46.990741 Tz (either ) Tj 1.808333 0 Td 45.37037 Tz (graft-to ) Tj 2.372222 0 Td 50.231481 Tz (or ) Tj 0.738889 0 Td 46.018519 Tz (graft ) Tj 1.555556 0 Td 56.712963 Tz (from ) Tj 1.594444 0 Td 53.472222 Tz (methods. ) Tj 2.741667 0 Td 55.555556 Tz (Organic ) Tj 2.547222 0 Td 73.45679 Tz (mol ) Tj 51.428571 0 0 51.428571 0 2500.604061 Tm 6.358333 0 Td 50.231481 Tz (ecules ) Tj 2.177778 0 Td 51.203704 Tz (containing ) Tj 3.402778 0 Td 53.472222 Tz (both ) Tj 1.633333 0 Td 44.722222 Tz (thiol ) Tj 1.672222 0 Td 59.41358 Tz (and ) Tj 1.458333 0 Td 53.20216 Tz (vinylbenzene ) Tj 4.2 0 Td 48.611111 Tz (functional ) Tj 51.428571 0 0 51.428571 0 2464 Tm 6.358333 0 Td 51.388889 Tz (groups, ) Tj 2.683333 0 Td 51.851852 Tz (exemplified ) Tj 3.947222 0 Td 59.953704 Tz (by ) Tj 1.283333 0 Td 57.037037 Tz (newly ) Tj 2.255556 0 Td 51.557239 Tz (synthesized ) Tj 3.908333 0 Td 56.388889 Tz (4-vinylben ) Tj 51.428571 0 0 51.428571 0 2417.566038 Tm 6.358333 0 Td 50.898693 Tz (Zenepropanethiol, ) Tj 5.327778 0 Td 56.712963 Tz (form ) Tj 1.516667 0 Td 50.771605 Tz (robust ) Tj 1.944444 0 Td 51.388889 Tz (coating ) Tj 2.275 0 Td 58.333333 Tz (on ) Tj 0.855556 0 Td 54.282407 Tz (Such ) Tj 1.458333 0 Td 52.5 Tz (metal ) Tj 1.711111 0 Td 49.421296 Tz (Surfaces ) Tj 51.428571 0 0 51.428571 0 2374.728643 Tm 6.358333 0 Td 50.231481 Tz (as ) Tj 0.777778 0 Td 55.092593 Tz (gold ) Tj 1.497222 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 56.17284 Tz (copper ) Tj 2.197222 0 Td 52.662037 Tz (with ) Tj 1.477778 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 49.259259 Tz (controlled ) Tj 3.15 0 Td 49.691358 Tz (thickness ) Tj 2.897222 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 52.662037 Tz (1-10 ) Tj 51.428571 0 0 51.428571 0 2336.633803 Tm 6.358333 0 Td 74.537037 Tz (nm ) Tj 1.05 0 Td 49.151235 Tz (range. ) Tj 1.886111 0 Td 58.333333 Tz (These ) Tj 1.866667 0 Td 49.826389 Tz (coatings ) Tj 2.488889 0 Td 53.703704 Tz (provide ) Tj 2.352778 0 Td 55.497685 Tz (complete ) Tj 2.8 0 Td 53.877315 Tz (coverage ) Tj 2.683333 0 Td 55.092593 Tz (of ) Tj 0.738889 0 Td 53.148148 Tz (metal ) Tj 48.571429 0 0 48.571429 0 2292 Tm 6.752941 0 Td 49.754902 Tz (Surface, ) Tj 2.491176 0 Td 52.614379 Tz (act ) Tj 1.029412 0 Td 54.901961 Tz (as ) Tj 0.802941 0 Td 49.754902 Tz (insulators ) Tj 3.129412 0 Td 48.039216 Tz (in ) Tj 0.741176 0 Td 53.986928 Tz (electrochemical ) Tj 5.002941 0 Td 49.411765 Tz (reactions, ) Tj 3.088235 0 Td 62.908497 Tz (and ) Tj 1.255882 0 Td 52.614379 Tz (are ) Tj 51.428571 0 0 51.428571 0 2252.803493 Tm 6.358333 0 Td 53.703704 Tz (capable ) Tj 2.430556 0 Td 55.092593 Tz (of ) Tj 0.758333 0 Td 51.527778 Tz (preventing ) Tj 3.266667 0 Td 48.287037 Tz (corrosion. ) Tj 38.571429 0 0 38.571429 0 2177 Tm 10.992593 0 Td 90.740741 Tz (BRIEF ) Tj 3.007407 0 Td 94.668911 Tz (DESCRIPTION ) Tj 6.533333 0 Td 101.54321 Tz (OF ) Tj 1.451852 0 Td 105.144033 Tz (THE ) Tj 2.177778 0 Td 105.864198 Tz (DRAWINGS ) Tj 51.428571 0 0 51.428571 0 2088.588235 Tm 7.116667 0 Td 54.282407 Tz (FIG. ) Tj 1.594444 0 Td 48.611111 Tz (1 ) Tj 0.544444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 56.481481 Tz (drawing ) Tj 2.586111 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 48.611111 Tz (the ) Tj 1.088889 0 Td 54.282407 Tz (chemical ) Tj 2.858333 0 Td 47.170782 Tz (structure ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 55.555556 Tz (4-vinyl ) Tj 51.428571 0 0 51.428571 0 2052 Tm 6.338889 0 Td 52.013889 Tz (benzenepropanethiol. ) Tj 51.428571 0 0 51.428571 0 2006.76338 Tm 7.116667 0 Td 54.282407 Tz (FIG. ) Tj 1.633333 0 Td 58.333333 Tz (2 ) Tj 0.641667 0 Td 38.888889 Tz (is ) Tj 0.758333 0 Td 51.851852 Tz (a ) Tj 0.622222 0 Td 50.411523 Tz (flowchart ) Tj 3.013889 0 Td 57.407407 Tz (showing ) Tj 2.722222 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 47.962963 Tz (steps ) Tj 1.711111 0 Td 61.574074 Tz (of ) Tj 0.933333 0 Td 48.971193 Tz (synthesis ) Tj 2.955556 0 Td 43.75 Tz (to ) Tj 51.428571 0 0 51.428571 0 1966.993031 Tm 6.358333 0 Td 52.314815 Tz (prepare ) Tj 2.313889 0 Td 52.350427 Tz (4-vinylbenzenepropanethiol ) Tj 8.322222 0 Td 58.333333 Tz (from ) Tj 1.555556 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 62.87037 Tz (shown ) Tj 2.061111 0 Td 45.37037 Tz (starting ) Tj 40 0 0 40 0 1928 Tm 8.175 0 Td 60.416667 Tz (materials. ) Tj 58.571429 0 0 58.571429 0 1882.981919 Tm 6.231707 0 Td 48.373984 Tz (FIG. ) Tj 1.519512 0 Td 54.065041 Tz (3 ) Tj 0.7 0 Td 34.146341 Tz (is ) Tj 0.75122 0 Td 51.219512 Tz (an ) Tj 1.007317 0 Td 64.498645 Tz ("H-NMR ) Tj 2.680488 0 Td 43.089431 Tz (spectra ) Tj 2.134146 0 Td 54.065041 Tz (of ) Tj 0.904878 0 Td 48.876136 Tz (4-vinylbenzenepro ) Tj 51.428571 0 0 51.428571 0 1840.616967 Tm 6.358333 0 Td 50.05144 Tz (panethiol ) Tj 3.052778 0 Td 58.333333 Tz (showing ) Tj 2.8 0 Td 49.691358 Tz (the ) Tj 1.244444 0 Td 50.925926 Tz (content ) Tj 2.469444 0 Td 58.333333 Tz (of ) Tj 0.952778 0 Td 48.611111 Tz (the ) Tj 1.225 0 Td 54.208754 Tz (composition ) Tj 3.947222 0 Td 59.62963 Tz (which ) Tj 51.428571 0 0 51.428571 0 1798.280576 Tm 6.358333 0 Td 44.907407 Tz (results ) Tj 2.061111 0 Td 57.523148 Tz (from ) Tj 1.536111 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 47.314815 Tz (steps ) Tj 1.594444 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 48.611111 Tz (synthesis ) Tj 2.761111 0 Td 54.282407 Tz (provided ) Tj 2.741667 0 Td 47.222222 Tz (herein. ) Tj 2.119444 0 Td 66.435185 Tz (As ) Tj 0.933333 0 Td 64.166667 Tz (shown ) Tj 58.571429 0 0 58.571429 0 1753 Tm 5.565854 0 Td 42.276423 Tz (therein ) Tj 1.963415 0 Td 65.447154 Tz ("H-NMR ) Tj 2.47561 0 Td 49.085366 Tz (\(270 ) Tj 1.314634 0 Td 61.178862 Tz (MHz, ) Tj 1.621951 0 Td 64.308943 Tz (CDC1\) ) Tj 2.1 0 Td 45.528455 Tz (& ) Tj 0.478049 0 Td 43.394309 Tz (1.35 ) Tj 1.195122 0 Td 30.352304 Tz (\(t, ) Tj 0.734146 0 Td 49.322493 Tz (1H, ) Tj 1.041463 0 Td 48.373984 Tz (SH\), ) Tj 1.365854 0 Td 41.260163 Tz (1.91 ) Tj 51.428571 0 0 51.428571 0 1712 Tm 6.377778 0 Td 59.953704 Tz (\(m,2H, ) Tj 2.294444 0 Td 60.277778 Tz (CH2\), ) Tj 1.963889 0 Td 48.611111 Tz (2.51 ) Tj 1.4 0 Td 61.033951 Tz (\(m,2H, ) Tj 2.333333 0 Td 59.62963 Tz (CH2\), ) Tj 1.944444 0 Td 49.421296 Tz (2.71 ) Tj 1.419444 0 Td 32.407407 Tz (\(t, ) Tj 0.738889 0 Td 59.41358 Tz (2H, ) Tj 1.225 0 Td 58.981481 Tz (CH2\), ) Tj 1.925 0 Td 52.662037 Tz (5.18 ) Tj 1.419444 0 Td 42.12963 Tz (\(d. ) Tj 51.428571 0 0 51.428571 0 1670 Tm 6.416667 0 Td 35.648148 Tz (1 ) Tj 0.505556 0 Td 55.092593 Tz (H, ) Tj 0.875 0 Td 59.143519 Tz (CH\), ) Tj 1.613889 0 Td 51.851852 Tz (5.69 ) Tj 1.458333 0 Td 39.969136 Tz (\(d. ) Tj 0.991667 0 Td 57.253086 Tz (1H, ) Tj 1.205556 0 Td 59.953704 Tz (CH\), ) Tj 1.613889 0 Td 52.662037 Tz (6.68 ) Tj 1.477778 0 Td 45.37037 Tz (\(dd. ) Tj 1.341667 0 Td 56.17284 Tz (1H, ) Tj 1.225 0 Td 58.333333 Tz (CH\), ) Tj 1.613889 0 Td 51.041667 Tz (7.13 ) Tj 1.458333 0 Td 39.969136 Tz (\(d. ) Tj 0.972222 0 Td 57.253086 Tz (2H, ) Tj 52.857143 0 0 52.857143 0 1628 Tm 6.186486 0 Td 51.501502 Tz (arom\), ) Tj 2.062162 0 Td 50.45045 Tz (7.32 ) Tj 1.418919 0 Td 39.93994 Tz (\(d. ) Tj 0.927027 0 Td 57.807808 Tz (2H, ) Tj 1.210811 0 Td 51.501502 Tz (arom\). ) Tj 51.428571 0 0 51.428571 0 1590.18543 Tm 7.116667 0 Td 54.282407 Tz (FIG. ) Tj 1.497222 0 Td 64.814815 Tz (4 ) Tj 0.563889 0 Td 40.509259 Tz (is ) Tj 0.680556 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 54.444444 Tz (graph ) Tj 1.847222 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 58.333333 Tz (polymer ) Tj 2.625 0 Td 47.800926 Tz (grafting ) Tj 2.508333 0 Td 56.712963 Tz (from ) Tj 1.575 0 Td 54.282407 Tz (gold ) Tj 1.497222 0 Td 50 Tz (Surface ) Tj 51.428571 0 0 51.428571 0 1547.340451 Tm 6.377778 0 Td 57.87037 Tz (showing ) Tj 2.547222 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 49.826389 Tz (increase ) Tj 2.547222 0 Td 43.75 Tz (in ) Tj 0.661111 0 Td 50.411523 Tz (thickness ) Tj 2.877778 0 Td 53.472222 Tz (of ) Tj 0.719444 0 Td 50.771605 Tz (the ) Tj 1.030556 0 Td 52.546296 Tz (polymerization ) Tj 4.569444 0 Td 59.953704 Tz (coat ) Tj 51.428571 0 0 51.428571 0 1504.736211 Tm 6.358333 0 Td 50.771605 Tz (ing ) Tj 1.069444 0 Td 50.231481 Tz (as ) Tj 0.738889 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 50.87963 Tz (incubation ) Tj 3.208333 0 Td 54.282407 Tz (time ) Tj 1.438889 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 54.282407 Tz (exposure ) Tj 2.761111 0 Td 45.37037 Tz (to ) Tj 0.719444 0 Td 45.075758 Tz (ultraviolet ) Tj 3.111111 0 Td 48.611111 Tz (radiation ) Tj 51.428571 0 0 51.428571 0 1462.669136 Tm 6.358333 0 Td 46.990741 Tz (increases. ) Tj 3.091667 0 Td 63.734568 Tz (The ) Tj 1.4 0 Td 54.768519 Tz (wavelength ) Tj 3.538889 0 Td 61.574074 Tz (of ) Tj 0.913889 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 45.37037 Tz (ultraviolet ) Tj 3.286111 0 Td 46.8107 Tz (radiation ) Tj 2.8 0 Td 56.712963 Tz (used ) Tj 38.571429 0 0 38.571429 0 1428 Tm 8.451852 0 Td 83.539095 Tz (was ) Tj 1.788889 0 Td 77.777778 Tz (255 ) Tj 1.737037 0 Td 77.777778 Tz (nm. ) Tj 58.571429 0 0 58.571429 0 1382.727038 Tm 6.231707 0 Td 48.373984 Tz (FIG. ) Tj 1.314634 0 Td 59.756098 Tz (5 ) Tj 0.546341 0 Td 34.146341 Tz (is ) Tj 0.580488 0 Td 51.219512 Tz (an ) Tj 0.836585 0 Td 64.9729 Tz ("H-NMR ) Tj 2.509756 0 Td 43.089431 Tz (spectra ) Tj 1.980488 0 Td 51.219512 Tz (of ) Tj 0.717073 0 Td 42.682927 Tz (the ) Tj 0.939024 0 Td 48.632668 Tz (polymerized ) Tj 3.363415 0 Td 45.528455 Tz (coating ) Tj 51.428571 0 0 51.428571 0 1340.53715 Tm 6.358333 0 Td 50.411523 Tz (disclosed ) Tj 2.936111 0 Td 47.222222 Tz (herein. ) Tj 2.255556 0 Td 52.546296 Tz (Polymerization ) Tj 4.705556 0 Td 47.395833 Tz (resulted ) Tj 2.527778 0 Td 56.712963 Tz (from ) Tj 1.613889 0 Td 55.092593 Tz (exposure ) Tj 2.858333 0 Td 46.990741 Tz (to ) Tj 51.428571 0 0 51.428571 0 1295 Tm 6.338889 0 Td 45.664983 Tz (ultraviolet ) Tj 3.247222 0 Td 46.8107 Tz (radiation ) Tj 2.741667 0 Td 55.092593 Tz (\(255 ) Tj 1.555556 0 Td 64.814815 Tz (nm\) ) Tj 1.380556 0 Td 47.530864 Tz (for ) Tj 1.030556 0 Td 63.194444 Tz (20 ) Tj 0.913889 0 Td 49.691358 Tz (hours. ) Tj 2.002778 0 Td 64.814815 Tz (The ) Tj 1.341667 0 Td 51.851852 Tz (decrease ) Tj 2.702778 0 Td 50.231481 Tz (in ) Tj 51.428571 0 0 51.428571 0 1256.138232 Tm 6.338889 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 47.314815 Tz (vinyl ) Tj 1.613889 0 Td 52.391975 Tz (proton ) Tj 2.061111 0 Td 58.333333 Tz (peak ) Tj 1.536111 0 Td 51.041667 Tz (area ) Tj 1.380556 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 49.421296 Tz (increase ) Tj 2.527778 0 Td 46.990741 Tz (in ) Tj 0.719444 0 Td 59.143519 Tz (peak ) Tj 1.555556 0 Td 51.041667 Tz (area ) Tj 1.4 0 Td 52.662037 Tz (near ) Tj 1.438889 0 Td 47.530864 Tz (2.5 ) Tj 51.428571 0 0 51.428571 0 1216.22756 Tm 6.358333 0 Td 71.296296 Tz (ppm ) Tj 1.672222 0 Td 51.041667 Tz (Supports ) Tj 2.819444 0 Td 49.691358 Tz (the ) Tj 1.244444 0 Td 53.472222 Tz (occurrence ) Tj 3.558333 0 Td 58.333333 Tz (of ) Tj 0.972222 0 Td 52.314815 Tz (polymerization ) Tj 4.783333 0 Td 58.333333 Tz (between ) Tj 51.428571 0 0 51.428571 0 1174.841424 Tm 6.358333 0 Td 49.259259 Tz (vinyl ) Tj 1.672222 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 44.074074 Tz (thiol ) Tj 1.497222 0 Td 51.388889 Tz (groups. ) Tj 51.428571 0 0 51.428571 0 1132.205955 Tm 7.116667 0 Td 54.282407 Tz (FIG. ) Tj 1.477778 0 Td 58.333333 Tz (6 ) Tj 0.486111 0 Td 53.20216 Tz (demonstrates ) Tj 3.966667 0 Td 49.691358 Tz (the ) Tj 1.030556 0 Td 43.981481 Tz (ability ) Tj 1.983333 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 0.991667 0 Td 52.777778 Tz (polymerization ) Tj 4.569444 0 Td 59.953704 Tz (coat ) Tj 51.428571 0 0 51.428571 0 1088.450667 Tm 6.358333 0 Td 50.771605 Tz (ing ) Tj 1.225 0 Td 48.611111 Tz (to ) Tj 0.933333 0 Td 46.585648 Tz (insulate ) Tj 2.527778 0 Td 50.771605 Tz (the ) Tj 1.244444 0 Td 53.148148 Tz (metal ) Tj 1.925 0 Td 46.585648 Tz (Surface. ) Tj 2.586111 0 Td 66.111111 Tz (Shown ) Tj 2.294444 0 Td 49.907407 Tz (there ) Tj 1.808333 0 Td 49.691358 Tz (are ) Tj 1.186111 0 Td 48.070988 Tz (cyclic ) Tj 51.428571 0 0 51.428571 0 1051.306778 Tm 6.358333 0 Td 60.327635 Tz (Voltammograms ) Tj 4.938889 0 Td 52.5 Tz (using ) Tj 1.769444 0 Td 54.73251 Tz (potassium ) Tj 3.188889 0 Td 46.866097 Tz (ferricyanide. ) Tj 3.888889 0 Td 66.759259 Tz (Shown ) Tj 2.236111 0 Td 48.611111 Tz (there ) Tj 51.428571 0 0 51.428571 0 1007.169427 Tm 6.358333 0 Td 38.888889 Tz (is ) Tj 0.719444 0 Td 58.333333 Tz (a ) Tj 0.583333 0 Td 56.388889 Tz (comparison ) Tj 3.636111 0 Td 57.87037 Tz (between ) Tj 2.702778 0 Td 55.092593 Tz (an ) Tj 0.933333 0 Td 50.05144 Tz (untreated ) Tj 2.936111 0 Td 55.092593 Tz (gold ) Tj 1.555556 0 Td 47.395833 Tz (Surface, ) Tj 2.527778 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 55.902778 Tz (gold ) Tj 51.428571 0 0 51.428571 0 967.16 Tm 6.377778 0 Td 49.537037 Tz (Surface ) Tj 2.255556 0 Td 55.632716 Tz (having ) Tj 2.177778 0 Td 58.333333 Tz (a ) Tj 0.622222 0 Td 44.290123 Tz (1.3 ) Tj 1.069444 0 Td 72.916667 Tz (nm ) Tj 1.088889 0 Td 52.546296 Tz (polymerization ) Tj 4.647222 0 Td 47.800926 Tz (coating, ) Tj 2.488889 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 55.092593 Tz (gold ) Tj 51.428571 0 0 51.428571 0 925.420272 Tm 6.377778 0 Td 49.537037 Tz (Surface ) Tj 2.275 0 Td 55.092593 Tz (having ) Tj 2.177778 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 50.771605 Tz (3.2 ) Tj 1.147222 0 Td 74.537037 Tz (nm ) Tj 1.108333 0 Td 52.777778 Tz (polymerization ) Tj 4.666667 0 Td 47.395833 Tz (coating. ) Tj 2.488889 0 Td 63.734568 Tz (The ) Tj 1.380556 0 Td 55.092593 Tz (redox ) Tj 51.428571 0 0 51.428571 0 882.514019 Tm 6.358333 0 Td 54.6875 Tz (mediator ) Tj 2.761111 0 Td 62.654321 Tz (was ) Tj 1.4 0 Td 35.648148 Tz (1 ) Tj 0.486111 0 Td 98.842593 Tz (mM ) Tj 1.361111 0 Td 54.012346 Tz (potassium ) Tj 3.169444 0 Td 48.341049 Tz (ferricyanide ) Tj 3.675 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 68.595679 Tz (1MKC1. ) Tj 40 0 0 40 0 846 Tm 9.15 0 Td 69.791667 Tz (FIG. ) Tj 1.975 0 Td 79.166667 Tz (7 ) Tj 0.775 0 Td 68.055556 Tz (demonstrates ) Tj 5.2 0 Td 62.5 Tz (the ) Tj 1.4 0 Td 73.958333 Tz (enhanced ) Tj 3.825 0 Td 60.833333 Tz (insulation ) Tj 3.95 0 Td 65.909091 Tz (characteris ) Tj 51.428571 0 0 51.428571 0 799.312039 Tm 6.338889 0 Td 42.939815 Tz (tics ) Tj 1.263889 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 52.314815 Tz (polymerization ) Tj 4.627778 0 Td 51.388889 Tz (coating ) Tj 2.372222 0 Td 50.411523 Tz (disclosed ) Tj 2.916667 0 Td 50.771605 Tz (herein ) Tj 2.041667 0 Td 50.231481 Tz (as ) Tj 0.836111 0 Td 83.179012 Tz (com ) Tj 51.428571 0 0 51.428571 0 757.940781 Tm 6.358333 0 Td 53.796296 Tz (pared ) Tj 1.983333 0 Td 48.611111 Tz (to ) Tj 0.972222 0 Td 50.771605 Tz (the ) Tj 1.302778 0 Td 47.314815 Tz (insulation ) Tj 3.247222 0 Td 50.231481 Tz (capacity ) Tj 2.838889 0 Td 55.092593 Tz (of ) Tj 1.011111 0 Td 57.253086 Tz (monolayer ) Tj 3.461111 0 Td 58.333333 Tz (of ) Tj 1.011111 0 Td 68.055556 Tz (dode ) Tj 51.428571 0 0 51.428571 0 717.629389 Tm 6.358333 0 Td 46.990741 Tz (canethiol. ) Tj 3.130556 0 Td 55.092593 Tz (FIG. ) Tj 1.633333 0 Td 71.296296 Tz (7A ) Tj 1.147222 0 Td 37.268519 Tz (is ) Tj 0.719444 0 Td 51.851852 Tz (a ) Tj 0.602778 0 Td 47.530864 Tz (cyclic ) Tj 2.002778 0 Td 61.033951 Tz (Voltammogram ) Tj 4.666667 0 Td 49.259259 Tz (prior ) Tj 1.691667 0 Td 45.37037 Tz (to ) Tj 0.816667 0 Td 59.41358 Tz (any ) Tj 51.428571 0 0 51.428571 0 675.336095 Tm 6.358333 0 Td 50.987654 Tz (electrochemical ) Tj 4.763889 0 Td 45.694444 Tz (stripping. ) Tj 2.916667 0 Td 53.472222 Tz (FIG. ) Tj 1.438889 0 Td 69.675926 Tz (7B ) Tj 0.991667 0 Td 38.888889 Tz (is ) Tj 0.583333 0 Td 58.333333 Tz (a ) Tj 0.486111 0 Td 47.530864 Tz (cyclic ) Tj 1.847222 0 Td 61.844136 Tz (Voltammogram ) Tj 51.428571 0 0 51.428571 0 635.466276 Tm 6.358333 0 Td 45.37037 Tz (after ) Tj 1.516667 0 Td 61.574074 Tz (50 ) Tj 0.933333 0 Td 47.530864 Tz (stripping ) Tj 2.741667 0 Td 46.759259 Tz (cycles. ) Tj 51.428571 0 0 51.428571 0 591.654194 Tm 7.116667 0 Td 54.282407 Tz (FIG. ) Tj 1.497222 0 Td 64.814815 Tz (8 ) Tj 0.602778 0 Td 37.268519 Tz (is ) Tj 0.641667 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 47.314815 Tz (table ) Tj 1.633333 0 Td 57.87037 Tz (showing ) Tj 2.625 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 49.691358 Tz (thickness ) Tj 2.877778 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 53.009259 Tz (polymerization ) Tj 51.428571 0 0 51.428571 0 552.020464 Tm 6.358333 0 Td 50.231481 Tz (coatings ) Tj 2.586111 0 Td 46.018519 Tz (after ) Tj 1.555556 0 Td 54.768519 Tz (mechanical ) Tj 3.5 0 Td 47.530864 Tz (stripping ) Tj 2.741667 0 Td 53.472222 Tz (or ) Tj 0.816667 0 Td 50.854701 Tz (manipulation. ) Tj 51.428571 0 0 51.428571 0 506.371429 Tm 7.116667 0 Td 54.282407 Tz (FIG. ) Tj 1.536111 0 Td 64.814815 Tz (9 ) Tj 0.680556 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 46.666667 Tz (table ) Tj 1.652778 0 Td 58.333333 Tz (showing ) Tj 2.683333 0 Td 51.851852 Tz (the ) Tj 1.166667 0 Td 50.771605 Tz (increased ) Tj 2.975 0 Td 50.05144 Tz (thickness ) Tj 2.955556 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 48.611111 Tz (the ) Tj 51.428571 0 0 51.428571 0 469.53202 Tm 6.358333 0 Td 52.314815 Tz (polymerization ) Tj 4.686111 0 Td 50.925926 Tz (coating ) Tj 2.430556 0 Td 46.527778 Tz (\(thiol-styrene ) Tj 4.180556 0 Td 58.333333 Tz (polymer ) Tj 2.722222 0 Td 46.018519 Tz (film\) ) Tj 1.652778 0 Td 51.851852 Tz (as ) Tj 0.913889 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 424.602871 Tm 6.358333 0 Td 50.87963 Tz (incubation ) Tj 3.247222 0 Td 51.851852 Tz (period ) Tj 2.041667 0 Td 56.712963 Tz (of ) Tj 0.738889 0 Td 52.932099 Tz (the ) Tj 1.108333 0 Td 47.530864 Tz (Substrate ) Tj 2.741667 0 Td 49.151235 Tz (\(gold\) ) Tj 1.925 0 Td 55.092593 Tz (being ) Tj 1.808333 0 Td 57.973251 Tz (Submersed ) Tj 3.305556 0 Td 48.611111 Tz (in ) Tj 51.428571 0 0 51.428571 0 384.870073 Tm 6.338889 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 35.648148 Tz (1 ) Tj 0.486111 0 Td 98.842593 Tz (mM ) Tj 1.4 0 Td 51.976496 Tz (4-vinylbenzenepropanethiol ) Tj 8.322222 0 Td 48.287037 Tz (increased. ) Tj 51.428571 0 0 51.428571 0 341.369393 Tm 7.116667 0 Td 54.282407 Tz (FIG. ) Tj 1.536111 0 Td 58.333333 Tz (10 ) Tj 0.913889 0 Td 40.509259 Tz (is ) Tj 0.661111 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 47.314815 Tz (table ) Tj 1.613889 0 Td 53.347578 Tz (demonstrating ) Tj 4.375 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 43.209877 Tz (stability ) Tj 2.527778 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 64.814815 Tz (poly ) Tj 51.428571 0 0 51.428571 0 297.712195 Tm 6.358333 0 Td 51.527778 Tz (merization ) Tj 3.325 0 Td 51.388889 Tz (coating ) Tj 2.372222 0 Td 54.12037 Tz (Subsequent ) Tj 3.441667 0 Td 46.990741 Tz (to ) Tj 0.777778 0 Td 51.49177 Tz (treatment ) Tj 3.013889 0 Td 51.851852 Tz (with ) Tj 1.458333 0 Td 51.851852 Tz (the ) Tj 1.186111 0 Td 64.166667 Tz (named ) Tj 40 0 0 40 0 261 Tm 8.175 0 Td 70.3125 Tz (chemical ) Tj 3.625 0 Td 62.5 Tz (for ) Tj 1.3 0 Td 81.25 Tz (30 ) Tj 1.2 0 Td 65.625 Tz (minutes. ) Tj 51.428571 0 0 51.428571 0 213.722772 Tm 7.116667 0 Td 54.282407 Tz (FIG. ) Tj 1.827778 0 Td 56.712963 Tz (11 ) Tj 1.205556 0 Td 58.981481 Tz (shows ) Tj 2.275 0 Td 47.530864 Tz (cyclic ) Tj 2.216667 0 Td 60.078348 Tz (voltammograms ) Tj 5.191667 0 Td 58.333333 Tz (of ) Tj 1.088889 0 Td 53.652263 Tz (electrode ) Tj 51.428571 0 0 51.428571 0 170.157833 Tm 6.358333 0 Td 60.648148 Tz (mounted ) Tj 2.702778 0 Td 51.851852 Tz (nanothin ) Tj 2.644444 0 Td 44.830247 Tz (films, ) Tj 1.769444 0 Td 57.685185 Tz (which ) Tj 1.866667 0 Td 49.691358 Tz (are ) Tj 1.011111 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 63.518519 Tz (named ) Tj 2.002778 0 Td 53.009259 Tz (polymerization ) Tj 30 0 0 30 0 2547 Tm 41.666667 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.666667 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.6 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.6 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.6 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.566667 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.566667 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.6 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.6 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.633333 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.633333 0 Td 75 Tz (65 ) Tj 51.428571 0 0 51.428571 0 2969 Tm 33.775 0 Td 77.777778 Tz (4 ) Tj 51.428571 0 0 51.428571 0 2919.062572 Tm 25.297222 0 Td 48.251029 Tz (coatings, ) Tj 2.741667 0 Td 43.981481 Tz (dithiol ) Tj 2.022222 0 Td 49.583333 Tz (multilayer ) Tj 3.052778 0 Td 59.41358 Tz (and ) Tj 1.186111 0 Td 58.333333 Tz (polymer ) Tj 2.527778 0 Td 47.800926 Tz (film ) Tj 1.283333 0 Td 52.067901 Tz (\(polymerization ) Tj 51.428571 0 0 51.428571 0 2876.063492 Tm 25.297222 0 Td 50.925926 Tz (coating ) Tj 2.352778 0 Td 50.05144 Tz (disclosed ) Tj 2.916667 0 Td 45.775463 Tz (herein\), ) Tj 2.430556 0 Td 46.990741 Tz (to ) Tj 0.797222 0 Td 60.763889 Tz (show ) Tj 1.691667 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 47.638889 Tz (insulating ) Tj 3.033333 0 Td 46.843434 Tz (properties. ) Tj 51.428571 0 0 51.428571 0 2834.031008 Tm 25.316667 0 Td 68.055556 Tz (By ) Tj 1.127778 0 Td 48.361823 Tz (ellipsometry, ) Tj 4.063889 0 Td 48.611111 Tz (the ) Tj 1.205556 0 Td 49.691358 Tz (thickness ) Tj 2.994444 0 Td 58.333333 Tz (of ) Tj 0.913889 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 44.444444 Tz (dithiol ) Tj 2.216667 0 Td 49.907407 Tz (multilayer ) Tj 3.286111 0 Td 38.888889 Tz (is ) Tj 58.571429 0 0 58.571429 0 2789.386282 Tm 22.212195 0 Td 50.081301 Tz (46.0+9.8A. ) Tj 3.12439 0 Td 55.96206 Tz (The ) Tj 1.143902 0 Td 43.631436 Tz (thickness ) Tj 2.492683 0 Td 49.796748 Tz (of ) Tj 0.665854 0 Td 43.631436 Tz (the ) Tj 0.887805 0 Td 52.03252 Tz (polymer ) Tj 2.304878 0 Td 41.260163 Tz (film ) Tj 1.160976 0 Td 32.723577 Tz (is ) Tj 0.529268 0 Td 47.306911 Tz (45.2+0.6 ) Tj 2.407317 0 Td 49.796748 Tz (A. ) Tj 40 0 0 40 0 2755 Tm 32.525 0 Td 81.944444 Tz (The ) Tj 1.725 0 Td 68.333333 Tz (redox ) Tj 2.375 0 Td 72.222222 Tz (marker ) Tj 2.775 0 Td 50 Tz (is ) Tj 0.925 0 Td 45.833333 Tz (1 ) Tj 0.65 0 Td 125 Tz (mM ) Tj 1.75 0 Td 68.382353 Tz (ferrocenemethanol ) Tj 7.2 0 Td 60.416667 Tz (in ) Tj 0.975 0 Td 56.944444 Tz (0.1 ) Tj 1.4 0 Td 110.416667 Tz (MPBS ) Tj 51.428571 0 0 51.428571 0 2709.740741 Tm 25.297222 0 Td 43.75 Tz (at ) Tj 0.7 0 Td 61.574074 Tz (pH-7.0 ) Tj 2.391667 0 Td 59.41358 Tz (and ) Tj 1.302778 0 Td 38.888889 Tz (1 ) Tj 0.525 0 Td 97.222222 Tz (mM ) Tj 1.341667 0 Td 59.41358 Tz (MgCl2. ) Tj 38.571429 0 0 38.571429 0 2634 Tm 35.181481 0 Td 97.762346 Tz (DETAILED ) Tj 4.977778 0 Td 94.276094 Tz (DESCRIPTION ) Tj 6.533333 0 Td 99.382716 Tz (OF ) Tj 1.4 0 Td 106.584362 Tz (THE ) Tj 2.177778 0 Td 98.902606 Tz (INVENTION ) Tj 51.428571 0 0 51.428571 0 2544.562423 Tm 26.016667 0 Td 63.734568 Tz (The ) Tj 1.244444 0 Td 50.411523 Tz (invention ) Tj 2.819444 0 Td 50.411523 Tz (disclosed ) Tj 2.819444 0 Td 50.231481 Tz (herein ) Tj 1.944444 0 Td 38.888889 Tz (is ) Tj 0.602778 0 Td 55.092593 Tz (a ) Tj 0.427778 0 Td 64.00463 Tz (compound ) Tj 3.208333 0 Td 47.800926 Tz (referred ) Tj 2.391667 0 Td 45.37037 Tz (to ) Tj 0.661111 0 Td 51.851852 Tz (as ) Tj 51.428571 0 0 51.428571 0 2509.770379 Tm 25.297222 0 Td 51.251715 Tz (4-vinylbenzenepropanethiol. ) Tj 8.575 0 Td 52.225783 Tz (4-vinylbenzenepropanethiol ) Tj 8.4 0 Td 40.509259 Tz (is ) Tj 51.428571 0 0 51.428571 0 2465.3269 Tm 25.297222 0 Td 53.703704 Tz (capable ) Tj 2.411111 0 Td 55.092593 Tz (of ) Tj 0.719444 0 Td 54.282407 Tz (polymerizing ) Tj 4.083333 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 51.851852 Tz (order ) Tj 1.672222 0 Td 46.990741 Tz (to ) Tj 0.758333 0 Td 48.070988 Tz (create ) Tj 1.866667 0 Td 58.333333 Tz (a ) Tj 0.505556 0 Td 58.333333 Tz (polymer ) Tj 2.605556 0 Td 50.462963 Tz (coating ) Tj 51.428571 0 0 51.428571 0 2421.39823 Tm 25.277778 0 Td 54.552469 Tz (having ) Tj 2.177778 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 50.05144 Tz (thickness ) Tj 2.936111 0 Td 55.092593 Tz (of ) Tj 0.797222 0 Td 44.560185 Tz (less ) Tj 1.263889 0 Td 51.851852 Tz (than ) Tj 1.536111 0 Td 55.092593 Tz (10 ) Tj 0.875 0 Td 59.41358 Tz (nm. ) Tj 1.283333 0 Td 62.654321 Tz (The ) Tj 1.322222 0 Td 58.333333 Tz (polymer ) Tj 2.644444 0 Td 50.462963 Tz (coating ) Tj 40 0 0 40 0 2385 Tm 32.55 0 Td 69.166667 Tz (slows ) Tj 2.25 0 Td 65.277778 Tz (corrosion ) Tj 3.725 0 Td 72.916667 Tz (of ) Tj 0.975 0 Td 66.666667 Tz (metals ) Tj 2.6 0 Td 76.388889 Tz (and ) Tj 1.5 0 Td 61.458333 Tz (acts ) Tj 1.65 0 Td 64.583333 Tz (as ) Tj 0.975 0 Td 72.916667 Tz (an ) Tj 1.075 0 Td 61.111111 Tz (insulator ) Tj 3.425 0 Td 76.388889 Tz (and ) Tj 1.575 0 Td 56.770833 Tz (resister ) Tj 51.428571 0 0 51.428571 0 2336.597898 Tm 25.297222 0 Td 45.37037 Tz (in ) Tj 0.933333 0 Td 51.203704 Tz (electrochemical ) Tj 4.977778 0 Td 49.259259 Tz (processes. ) Tj 3.344444 0 Td 55.902778 Tz (Also ) Tj 1.730556 0 Td 50.411523 Tz (disclosed ) Tj 3.072222 0 Td 51.311728 Tz (herein ) Tj 2.236111 0 Td 37.268519 Tz (is ) Tj 0.855556 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 2299.349515 Tm 25.297222 0 Td 60.493827 Tz (method ) Tj 2.45 0 Td 56.712963 Tz (of ) Tj 0.816667 0 Td 53.472222 Tz (applying ) Tj 2.8 0 Td 52.225783 Tz (4-vinylbenzenepropanethiol ) Tj 8.4 0 Td 45.37037 Tz (to ) Tj 0.816667 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 53.148148 Tz (metal ) Tj 51.428571 0 0 51.428571 0 2257.12 Tm 25.316667 0 Td 45.37037 Tz (substrate. ) Tj 2.955556 0 Td 71.296296 Tz (When ) Tj 1.963889 0 Td 52.10114 Tz (4-vinylbenzenepropanethiol ) Tj 8.361111 0 Td 38.888889 Tz (is ) Tj 0.7 0 Td 50.925926 Tz (applied ) Tj 2.372222 0 Td 45.37037 Tz (to ) Tj 0.777778 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 2214.211823 Tm 25.297222 0 Td 49.151235 Tz (metal. ) Tj 1.983333 0 Td 55.092593 Tz (Such ) Tj 1.516667 0 Td 50.231481 Tz (as ) Tj 0.816667 0 Td 49.537037 Tz (copper, ) Tj 2.294444 0 Td 49.259259 Tz (gold, ) Tj 1.652778 0 Td 51.49177 Tz (platinum, ) Tj 2.955556 0 Td 53.472222 Tz (or ) Tj 0.797222 0 Td 44.722222 Tz (iron, ) Tj 1.516667 0 Td 51.851852 Tz (the ) Tj 1.088889 0 Td 47.314815 Tz (beneficial ) Tj 51.428571 0 0 51.428571 0 2172.534665 Tm 25.297222 0 Td 48.287037 Tz (properties ) Tj 3.033333 0 Td 51.49177 Tz (described ) Tj 2.897222 0 Td 57.037037 Tz (above ) Tj 1.827778 0 Td 49.691358 Tz (are ) Tj 1.011111 0 Td 46.990741 Tz (present. ) Tj 2.411111 0 Td 44.965278 Tz (Finally, ) Tj 2.294444 0 Td 47.800926 Tz (also ) Tj 1.302778 0 Td 50.05144 Tz (disclosed ) Tj 51.428571 0 0 51.428571 0 2132.211823 Tm 25.277778 0 Td 50.771605 Tz (herein ) Tj 2.138889 0 Td 38.888889 Tz (is ) Tj 0.738889 0 Td 58.333333 Tz (a ) Tj 0.661111 0 Td 59.953704 Tz (method ) Tj 2.430556 0 Td 58.333333 Tz (of ) Tj 0.933333 0 Td 59.41358 Tz (making ) Tj 2.430556 0 Td 52.225783 Tz (4-vinylbenzenepropanethiol ) Tj 51.428571 0 0 51.428571 0 2088.485149 Tm 25.277778 0 Td 59.62963 Tz (which ) Tj 1.983333 0 Td 44.907407 Tz (results ) Tj 2.080556 0 Td 46.990741 Tz (in ) Tj 0.758333 0 Td 56.712963 Tz (an ) Tj 0.855556 0 Td 55.902778 Tz (abundant ) Tj 2.858333 0 Td 61.033951 Tz (amount ) Tj 2.372222 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 55.092593 Tz (a ) Tj 0.505556 0 Td 53.472222 Tz (high ) Tj 1.497222 0 Td 47.685185 Tz (quality ) Tj 2.177778 0 Td 66.435185 Tz (prod ) Tj 34.285714 0 0 34.285714 0 2052 Tm 37.916667 0 Td 66.840278 Tz (uct. ) Tj 51.428571 0 0 51.428571 0 2004.803109 Tm 26.036111 0 Td 66.759259 Tz (Shown ) Tj 2.177778 0 Td 46.990741 Tz (in ) Tj 0.777778 0 Td 55.092593 Tz (FIG. ) Tj 1.575 0 Td 42.12963 Tz (1, ) Tj 0.719444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 54.6875 Tz (chemical ) Tj 2.819444 0 Td 47.530864 Tz (structure ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 56.388889 Tz (4-vinylben ) Tj 51.428571 0 0 51.428571 0 1964.576694 Tm 25.297222 0 Td 50.708061 Tz (Zenepropanethiol. ) Tj 5.327778 0 Td 64.814815 Tz (As ) Tj 0.933333 0 Td 62.222222 Tz (shown ) Tj 2.022222 0 Td 45.775463 Tz (therein, ) Tj 2.352778 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 58.333333 Tz (2 ) Tj 0.525 0 Td 48.935185 Tz (functional ) Tj 3.091667 0 Td 50.925926 Tz (groups, ) Tj 51.428571 0 0 51.428571 0 1924.348865 Tm 25.277778 0 Td 44.074074 Tz (thiol ) Tj 1.536111 0 Td 59.41358 Tz (and ) Tj 1.283333 0 Td 53.472222 Tz (vinylbenzene ) Tj 4.063889 0 Td 45.694444 Tz (\(styrene\), ) Tj 2.916667 0 Td 53.703704 Tz (provide ) Tj 2.45 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 46.234568 Tz (characteristics ) Tj 51.428571 0 0 51.428571 0 1880.463734 Tm 25.297222 0 Td 52.211934 Tz (necessary ) Tj 2.936111 0 Td 45.37037 Tz (to ) Tj 0.661111 0 Td 52.5 Tz (allow ) Tj 1.730556 0 Td 52.777778 Tz (binding ) Tj 2.333333 0 Td 45.37037 Tz (to ) Tj 0.661111 0 Td 58.333333 Tz (a ) Tj 0.466667 0 Td 53.148148 Tz (metal ) Tj 1.730556 0 Td 46.585648 Tz (Surface, ) Tj 2.352778 0 Td 50.771605 Tz (the ) Tj 1.011111 0 Td 53.292181 Tz (formation ) Tj 2.994444 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 1840.338983 Tm 25.297222 0 Td 58.333333 Tz (polymer ) Tj 2.663889 0 Td 48.148148 Tz (chains, ) Tj 2.216667 0 Td 60.493827 Tz (and ) Tj 1.302778 0 Td 48.611111 Tz (cross-linking ) Tj 4.005556 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 51.203704 Tz (those ) Tj 1.730556 0 Td 58.796296 Tz (polymer ) Tj 2.663889 0 Td 48.148148 Tz (chains. ) Tj 51.428571 0 0 51.428571 0 1798.561974 Tm 25.297222 0 Td 66.435185 Tz (As ) Tj 0.991667 0 Td 47.685185 Tz (further ) Tj 2.158333 0 Td 51.49177 Tz (described ) Tj 2.955556 0 Td 47.222222 Tz (herein, ) Tj 2.158333 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 47.530864 Tz (resulting ) Tj 2.702778 0 Td 59.259259 Tz (polymer ) Tj 2.625 0 Td 50.925926 Tz (coating ) Tj 2.313889 0 Td 40.509259 Tz (is ) Tj 51.428571 0 0 51.428571 0 1754.719434 Tm 25.297222 0 Td 52.662037 Tz (very ) Tj 1.477778 0 Td 42.12963 Tz (thin, ) Tj 1.438889 0 Td 55.092593 Tz (having ) Tj 2.158333 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 49.691358 Tz (thickness ) Tj 2.858333 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 56.712963 Tz (from ) Tj 1.555556 0 Td 53.796296 Tz (about ) Tj 1.866667 0 Td 35.648148 Tz (1 ) Tj 0.505556 0 Td 71.296296 Tz (nm ) Tj 1.05 0 Td 45.37037 Tz (to ) Tj 0.719444 0 Td 55.092593 Tz (about ) Tj 1.886111 0 Td 53.472222 Tz (10 ) Tj 40 0 0 40 0 1720 Tm 32.575 0 Td 75 Tz (nm. ) Tj 1.55 0 Td 63.541667 Tz (Suitable ) Tj 3.225 0 Td 61.979167 Tz (metallic ) Tj 3.175 0 Td 63.020833 Tz (surfaces ) Tj 3.175 0 Td 66.071429 Tz (include ) Tj 2.975 0 Td 65.972222 Tz (metals ) Tj 2.575 0 Td 57.291667 Tz (that ) Tj 1.55 0 Td 73.958333 Tz (form ) Tj 1.925 0 Td 75 Tz (bonds ) Tj 51.428571 0 0 51.428571 0 1674.383838 Tm 25.277778 0 Td 54.282407 Tz (with ) Tj 1.594444 0 Td 44.722222 Tz (thiol ) Tj 1.633333 0 Td 50.925926 Tz (groups, ) Tj 2.45 0 Td 47.685185 Tz (further ) Tj 2.275 0 Td 56.712963 Tz (examples ) Tj 3.013889 0 Td 48.206019 Tz (include, ) Tj 2.605556 0 Td 49.259259 Tz (gold, ) Tj 1.788889 0 Td 50 Tz (copper, ) Tj 52.857143 0 0 52.857143 0 1629.368675 Tm 24.594595 0 Td 49.74975 Tz (platinum, ) Tj 2.856757 0 Td 43.513514 Tz (iron, ) Tj 1.475676 0 Td 39.189189 Tz (silica, ) Tj 1.778378 0 Td 57.807808 Tz (and ) Tj 1.172973 0 Td 48.348348 Tz (the ) Tj 1.002703 0 Td 40.36036 Tz (like. ) Tj 1.4 0 Td 45.720721 Tz (In ) Tj 0.718919 0 Td 45.495495 Tz (certain ) Tj 2.043243 0 Td 57.616708 Tz (embodiments ) Tj 3.972973 0 Td 56.756757 Tz (of ) Tj 51.428571 0 0 51.428571 0 1589.675406 Tm 25.277778 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 50.925926 Tz (present ) Tj 2.372222 0 Td 47.962963 Tz (invention, ) Tj 3.15 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 50.411523 Tz (thickness ) Tj 2.994444 0 Td 56.712963 Tz (of ) Tj 0.855556 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 47.170782 Tz (resulting ) Tj 2.8 0 Td 58.796296 Tz (polymer ) Tj 51.428571 0 0 51.428571 0 1545.79845 Tm 25.297222 0 Td 51.388889 Tz (coating ) Tj 2.313889 0 Td 68.055556 Tz (may ) Tj 1.4 0 Td 56.712963 Tz (be ) Tj 0.836111 0 Td 57.523148 Tz (from ) Tj 1.555556 0 Td 55.092593 Tz (about ) Tj 1.866667 0 Td 35.648148 Tz (1 ) Tj 0.486111 0 Td 71.296296 Tz (nm ) Tj 1.069444 0 Td 43.75 Tz (to ) Tj 0.680556 0 Td 54.444444 Tz (about ) Tj 1.788889 0 Td 58.333333 Tz (5 ) Tj 0.563889 0 Td 57.253086 Tz (nm. ) Tj 1.263889 0 Td 34.027778 Tz (It ) Tj 0.563889 0 Td 38.888889 Tz (is ) Tj 0.622222 0 Td 51.446759 Tz (believed ) Tj 51.428571 0 0 51.428571 0 1506.769231 Tm 25.277778 0 Td 46.990741 Tz (that ) Tj 1.244444 0 Td 51.851852 Tz (the ) Tj 1.05 0 Td 59.259259 Tz (polymer ) Tj 2.625 0 Td 50.925926 Tz (coating ) Tj 2.294444 0 Td 38.888889 Tz (is ) Tj 0.641667 0 Td 49.907407 Tz (covalently ) Tj 3.15 0 Td 51.041667 Tz (attached ) Tj 2.586111 0 Td 46.990741 Tz (to ) Tj 0.738889 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 50 Tz (Surface ) Tj 51.428571 0 0 51.428571 0 1463.362283 Tm 25.297222 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 48.070988 Tz (metal. ) Tj 2.022222 0 Td 46.585648 Tz (Further, ) Tj 2.508333 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 58.796296 Tz (polymer ) Tj 2.663889 0 Td 51.388889 Tz (coating ) Tj 2.391667 0 Td 51.49177 Tz (described ) Tj 2.994444 0 Td 51.311728 Tz (herein ) Tj 51.428571 0 0 51.428571 0 1422.126341 Tm 25.277778 0 Td 54.012346 Tz (has ) Tj 1.127778 0 Td 48.611111 Tz (greater ) Tj 2.158333 0 Td 54.282407 Tz (chemical ) Tj 2.741667 0 Td 59.41358 Tz (and ) Tj 1.225 0 Td 54.768519 Tz (mechanical ) Tj 3.441667 0 Td 42.489712 Tz (stability ) Tj 2.469444 0 Td 51.851852 Tz (than ) Tj 1.4 0 Td 50.555556 Tz (other ) Tj 1.633333 0 Td 53.472222 Tz (self ) Tj 51.428571 0 0 51.428571 0 1380.575412 Tm 25.297222 0 Td 56.17284 Tz (assembled ) Tj 3.305556 0 Td 48.611111 Tz (alkyl ) Tj 1.75 0 Td 44.074074 Tz (thiol ) Tj 1.672222 0 Td 52.73569 Tz (monolayers. ) Tj 3.791667 0 Td 66.435185 Tz (As ) Tj 1.108333 0 Td 61.574074 Tz (shown ) Tj 2.158333 0 Td 52.391975 Tz (below, ) Tj 2.177778 0 Td 50.555556 Tz (these ) Tj 51.428571 0 0 51.428571 0 1341.885572 Tm 25.297222 0 Td 58.333333 Tz (polymer ) Tj 2.702778 0 Td 49.826389 Tz (coatings ) Tj 2.663889 0 Td 56.712963 Tz (have ) Tj 1.613889 0 Td 51.131687 Tz (increased ) Tj 3.033333 0 Td 47.638889 Tz (insulating ) Tj 3.130556 0 Td 43.981481 Tz (ability ) Tj 2.119444 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 1297.679335 Tm 25.297222 0 Td 43.981481 Tz (ability ) Tj 1.963889 0 Td 46.990741 Tz (to ) Tj 0.719444 0 Td 54.282407 Tz (slow ) Tj 1.458333 0 Td 50.771605 Tz (corrosion ) Tj 2.877778 0 Td 55.092593 Tz (of ) Tj 0.738889 0 Td 48.611111 Tz (metals. ) Tj 2.138889 0 Td 90.740741 Tz (A ) Tj 0.7 0 Td 59.953704 Tz (method ) Tj 2.255556 0 Td 48.611111 Tz (for ) Tj 0.972222 0 Td 50.501543 Tz (synthesizing ) Tj 51.428571 0 0 51.428571 0 1258.506112 Tm 25.297222 0 Td 52.10114 Tz (4-vinylbenzenepropanethiol ) Tj 8.380556 0 Td 40.509259 Tz (is ) Tj 0.738889 0 Td 49.826389 Tz (outlined ) Tj 2.644444 0 Td 42.12963 Tz (in ) Tj 0.816667 0 Td 58.738426 Tz (Examples ) Tj 3.15 0 Td 48.611111 Tz (1-4 ) Tj 1.127778 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 1213.074341 Tm 25.277778 0 Td 43.75 Tz (this ) Tj 1.244444 0 Td 55.812757 Tz (document. ) Tj 3.169444 0 Td 50.771605 Tz (All ) Tj 1.069444 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 45.37037 Tz (starting ) Tj 2.372222 0 Td 48.251029 Tz (materials ) Tj 2.8 0 Td 51.49177 Tz (described ) Tj 2.936111 0 Td 49.074074 Tz (therein ) Tj 51.428571 0 0 51.428571 0 1174.155112 Tm 25.297222 0 Td 49.691358 Tz (are ) Tj 1.030556 0 Td 54.552469 Tz (widely ) Tj 2.1 0 Td 55.632716 Tz (commercially ) Tj 4.141667 0 Td 46.018519 Tz (available. ) Tj 2.936111 0 Td 56.17284 Tz (For ) Tj 1.127778 0 Td 54.6875 Tz (example, ) Tj 2.838889 0 Td 54.768519 Tz (1-bromo-3- ) Tj 51.428571 0 0 51.428571 0 1132.626667 Tm 25.297222 0 Td 55.591168 Tz (phenylpropane ) Tj 4.530556 0 Td 60.493827 Tz (was ) Tj 1.302778 0 Td 54.372428 Tz (purchased ) Tj 3.169444 0 Td 55.902778 Tz (from ) Tj 1.555556 0 Td 54.12037 Tz (Alfa-Aesar ) Tj 3.402778 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 61.574074 Tz (was ) Tj 1.341667 0 Td 50.771605 Tz (not ) Tj 51.428571 0 0 51.428571 0 1092.147208 Tm 25.297222 0 Td 47.685185 Tz (further ) Tj 2.275 0 Td 44.290123 Tz (purified. ) Tj 2.702778 0 Td 63.734568 Tz (The ) Tj 1.438889 0 Td 47.314815 Tz (steps ) Tj 1.730556 0 Td 59.953704 Tz (of ) Tj 0.913889 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 49.331276 Tz (synthesis ) Tj 2.955556 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 56.388889 Tz (4-vinylben ) Tj 51.428571 0 0 51.428571 0 1048.150769 Tm 25.297222 0 Td 51.851852 Tz (Zenepropanethiol ) Tj 5.172222 0 Td 50.771605 Tz (are ) Tj 1.088889 0 Td 47.685185 Tz (further ) Tj 2.158333 0 Td 49.826389 Tz (outlined ) Tj 2.586111 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 54.282407 Tz (FIG. ) Tj 1.497222 0 Td 42.12963 Tz (2. ) Tj 57.142857 0 0 57.142857 0 1004.532982 Tm 23.415 0 Td 46.990741 Tz (Referring ) Tj 2.6775 0 Td 40.833333 Tz (to ) Tj 0.7 0 Td 48.854167 Tz (FIG. ) Tj 1.33 0 Td 40.833333 Tz (3, ) Tj 0.6825 0 Td 42.583333 Tz (there ) Tj 1.47 0 Td 33.541667 Tz (is ) Tj 0.5775 0 Td 56.583333 Tz (shown ) Tj 1.855 0 Td 44.722222 Tz (the ) Tj 1.225 0 Td 65 Tz (H-1-NMR ) Tj 2.8875 0 Td 46.180556 Tz (Septra ) Tj 51.428571 0 0 51.428571 0 965.382353 Tm 25.297222 0 Td 49.691358 Tz (for ) Tj 1.127778 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 51.976496 Tz (4-vinylbenzenepropanethiol ) Tj 8.419444 0 Td 57.685185 Tz (which ) Tj 2.022222 0 Td 60.493827 Tz (was ) Tj 1.341667 0 Td 53.472222 Tz (prepared ) Tj 2.819444 0 Td 50.231481 Tz (as ) Tj 40 0 0 40 0 927 Tm 32.525 0 Td 66.666667 Tz (described ) Tj 3.8 0 Td 60.714286 Tz (herein. ) Tj 51.428571 0 0 51.428571 0 877.151515 Tm 26.036111 0 Td 52.932099 Tz (Disclosed ) Tj 3.013889 0 Td 51.311728 Tz (herein ) Tj 2.022222 0 Td 49.691358 Tz (are ) Tj 1.069444 0 Td 47.685185 Tz (several ) Tj 2.216667 0 Td 57.87037 Tz (methods ) Tj 2.625 0 Td 48.611111 Tz (for ) Tj 0.991667 0 Td 53.877315 Tz (applying ) Tj 2.722222 0 Td 58.333333 Tz (a ) Tj 0.505556 0 Td 64.814815 Tz (poly ) Tj 51.428571 0 0 51.428571 0 834.087282 Tm 25.297222 0 Td 65.895062 Tz (mer ) Tj 1.341667 0 Td 50.462963 Tz (coating ) Tj 2.294444 0 Td 46.990741 Tz (to ) Tj 0.758333 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 49.151235 Tz (metal. ) Tj 1.983333 0 Td 66.975309 Tz (One ) Tj 1.4 0 Td 55.092593 Tz (Such ) Tj 1.536111 0 Td 60.493827 Tz (method ) Tj 2.333333 0 Td 52.932099 Tz (allows ) Tj 2.1 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 50 Tz (Surface ) Tj 51.428571 0 0 51.428571 0 798.49505 Tm 25.297222 0 Td 52.314815 Tz (polymerization ) Tj 4.705556 0 Td 59.953704 Tz (of ) Tj 1.030556 0 Td 35.648148 Tz (1 ) Tj 0.661111 0 Td 97.222222 Tz (mM ) Tj 1.516667 0 Td 51.611797 Tz (4-vinyl-benzenepropanethiol ) Tj 8.730556 0 Td 47.530864 Tz (for ) Tj 51.428571 0 0 51.428571 0 750.652862 Tm 25.297222 0 Td 54.282407 Tz (gold ) Tj 1.438889 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 52.777778 Tz (hexane, ) Tj 2.391667 0 Td 57.685185 Tz (which ) Tj 1.905556 0 Td 44.907407 Tz (results ) Tj 2.061111 0 Td 43.75 Tz (in ) Tj 0.661111 0 Td 58.333333 Tz (a ) Tj 0.486111 0 Td 49.259259 Tz (controlled ) Tj 3.091667 0 Td 50.05144 Tz (thickness ) Tj 2.858333 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 44.560185 Tz (less ) Tj 57.142857 0 0 57.142857 0 709.804348 Tm 22.75 0 Td 47.395833 Tz (than ) Tj 1.4 0 Td 49.583333 Tz (5 ) Tj 0.595 0 Td 51.527778 Tz (nm, ) Tj 1.19 0 Td 46.666667 Tz (as ) Tj 0.8225 0 Td 56 Tz (shown ) Tj 1.9075 0 Td 43.75 Tz (in ) Tj 0.77 0 Td 49.583333 Tz (FIG. ) Tj 1.435 0 Td 39.375 Tz (4. ) Tj 0.7525 0 Td 53.083333 Tz (Based ) Tj 1.855 0 Td 53.958333 Tz (upon ) Tj 1.5225 0 Td 44.722222 Tz (the ) Tj 1.1025 0 Td 66.597222 Tz ('H-NMR ) Tj 51.428571 0 0 51.428571 0 669.801061 Tm 25.316667 0 Td 48.148148 Tz (spectra ) Tj 2.313889 0 Td 62.222222 Tz (shown ) Tj 2.197222 0 Td 43.75 Tz (in ) Tj 0.836111 0 Td 55.092593 Tz (FIG. ) Tj 1.594444 0 Td 46.990741 Tz (5, ) Tj 0.875 0 Td 42.777778 Tz (thiol ) Tj 1.594444 0 Td 58.333333 Tz (and ) Tj 1.380556 0 Td 47.962963 Tz (vinyl ) Tj 1.75 0 Td 48.611111 Tz (functional ) Tj 3.208333 0 Td 55.740741 Tz (group ) Tj 51.428571 0 0 51.428571 0 629.438095 Tm 25.297222 0 Td 52.314815 Tz (polymerization ) Tj 4.588889 0 Td 43.981481 Tz (results ) Tj 2.002778 0 Td 46.018519 Tz (after ) Tj 1.516667 0 Td 59.953704 Tz (20 ) Tj 0.836111 0 Td 54.444444 Tz (hours ) Tj 1.769444 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 54.6875 Tz (exposure ) Tj 2.780556 0 Td 45.37037 Tz (to ) Tj 0.7 0 Td 51.851852 Tz (ultravio ) Tj 51.428571 0 0 51.428571 0 586.160096 Tm 25.297222 0 Td 41.049383 Tz (let ) Tj 0.894444 0 Td 45.37037 Tz (radiation. ) Tj 2.955556 0 Td 52.314815 Tz (Polymerization ) Tj 4.530556 0 Td 54.012346 Tz (has ) Tj 1.147222 0 Td 56.712963 Tz (been ) Tj 1.536111 0 Td 54.012346 Tz (demonstrated ) Tj 4.063889 0 Td 45.37037 Tz (to ) Tj 0.719444 0 Td 55.092593 Tz (occur ) Tj 51.428571 0 0 51.428571 0 544.053528 Tm 25.277778 0 Td 54.282407 Tz (with ) Tj 1.458333 0 Td 52.662037 Tz (both ) Tj 1.438889 0 Td 45.075758 Tz (ultraviolet ) Tj 3.130556 0 Td 44.074074 Tz (light ) Tj 1.438889 0 Td 43.75 Tz (at ) Tj 0.680556 0 Td 59.41358 Tz (255 ) Tj 1.263889 0 Td 59.41358 Tz (nm, ) Tj 1.186111 0 Td 60.493827 Tz (and ) Tj 1.205556 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 54.012346 Tz (use ) Tj 1.069444 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 51.49177 Tz (thermally ) Tj 51.428571 0 0 51.428571 0 504.205811 Tm 25.297222 0 Td 44.290123 Tz (initiated ) Tj 2.586111 0 Td 52.314815 Tz (\(70-80 ) Tj 2.391667 0 Td 53.472222 Tz (C. ) Tj 0.816667 0 Td 50.87963 Tz (conditions ) Tj 3.266667 0 Td 51.851852 Tz (using ) Tj 1.730556 0 Td 54.62963 Tz (benzoyl ) Tj 2.45 0 Td 53.877315 Tz (peroxide ) Tj 2.722222 0 Td 51.851852 Tz (as ) Tj 0.797222 0 Td 59.953704 Tz (an ) Tj 51.428571 0 0 51.428571 0 462.392405 Tm 25.297222 0 Td 40.185185 Tz (initiator. ) Tj 2.761111 0 Td 64.814815 Tz (The ) Tj 1.516667 0 Td 44.074074 Tz (ultra ) Tj 1.652778 0 Td 46.990741 Tz (thin ) Tj 1.497222 0 Td 52.314815 Tz (polymerization ) Tj 4.783333 0 Td 50.462963 Tz (coating ) Tj 2.469444 0 Td 52.211934 Tz (described ) Tj 51.428571 0 0 51.428571 0 420.193211 Tm 25.277778 0 Td 51.311728 Tz (herein ) Tj 2.197222 0 Td 52.932099 Tz (demonstrates ) Tj 4.2 0 Td 48.611111 Tz (the ) Tj 1.225 0 Td 43.981481 Tz (ability ) Tj 2.236111 0 Td 42.12963 Tz (to ) Tj 0.875 0 Td 53.240741 Tz (provide ) Tj 2.605556 0 Td 45.37037 Tz (insulation. ) Tj 3.363889 0 Td 64.814815 Tz (As ) Tj 48.571429 0 0 48.571429 0 378 Tm 26.805882 0 Td 65.196078 Tz (shown ) Tj 2.182353 0 Td 46.323529 Tz (in ) Tj 0.782353 0 Td 58.333333 Tz (FIG. ) Tj 1.647059 0 Td 44.607843 Tz (6, ) Tj 0.761765 0 Td 51.470588 Tz (the ) Tj 1.111765 0 Td 46.666667 Tz (electrical ) Tj 3.005882 0 Td 52.45098 Tz (current ) Tj 2.388235 0 Td 48.039216 Tz (in ) Tj 0.802941 0 Td 51.470588 Tz (the ) Tj 1.132353 0 Td 57.647059 Tz (redox ) Tj 1.955882 0 Td 57.046569 Tz (mediator ) Tj 51.428571 0 0 51.428571 0 339.461538 Tm 25.316667 0 Td 48.206019 Tz (Solution ) Tj 2.644444 0 Td 38.888889 Tz (is ) Tj 0.816667 0 Td 49.151235 Tz (nearly ) Tj 2.119444 0 Td 45.730453 Tz (identical ) Tj 2.780556 0 Td 46.990741 Tz (to ) Tj 0.894444 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 57.685185 Tz (background ) Tj 3.772222 0 Td 44.830247 Tz (electrolyte, ) Tj 51.428571 0 0 51.428571 0 294.635468 Tm 25.277778 0 Td 59.62963 Tz (which ) Tj 1.983333 0 Td 38.888889 Tz (is ) Tj 0.661111 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 44.486532 Tz (theoritical ) Tj 3.15 0 Td 51.203704 Tz (value ) Tj 1.711111 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 53.796296 Tz (completely ) Tj 3.441667 0 Td 48.251029 Tz (insulated ) Tj 2.8 0 Td 44.074074 Tz (film. ) Tj 51.428571 0 0 51.428571 0 254.269136 Tm 25.297222 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 53.148148 Tz (redox ) Tj 1.788889 0 Td 53.877315 Tz (mediator ) Tj 2.722222 0 Td 61.574074 Tz (was ) Tj 1.341667 0 Td 35.648148 Tz (1 ) Tj 0.486111 0 Td 97.222222 Tz (mM ) Tj 1.302778 0 Td 54.372428 Tz (potassium ) Tj 3.130556 0 Td 48.611111 Tz (ferricyanide ) Tj 3.655556 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 79.398148 Tz (1M ) Tj 48.571429 0 0 48.571429 0 212 Tm 26.805882 0 Td 59.191176 Tz (KC1. ) Tj 1.647059 0 Td 70.343137 Tz (As ) Tj 1.070588 0 Td 65.882353 Tz (shown ) Tj 2.223529 0 Td 49.754902 Tz (in ) Tj 0.844118 0 Td 61.078431 Tz (FIGS. ) Tj 2.079412 0 Td 78.921569 Tz (7A ) Tj 1.152941 0 Td 62.908497 Tz (and ) Tj 1.358824 0 Td 60.620915 Tz (7B, ) Tj 1.338235 0 Td 67.769608 Tz (when ) Tj 1.852941 0 Td 54.444444 Tz (electrochemical ) Tj 51.428571 0 0 51.428571 0 174.412137 Tm 25.316667 0 Td 47.530864 Tz (stripping ) Tj 2.916667 0 Td 61.574074 Tz (was ) Tj 1.419444 0 Td 53.796296 Tz (performed, ) Tj 3.577778 0 Td 48.611111 Tz (the ) Tj 1.205556 0 Td 52.314815 Tz (polymerization ) Tj 4.763889 0 Td 50.925926 Tz (coating ) Tj 2.488889 0 Td 59.41358 Tz (dis ) Tj ET Q endstream endobj 302 0 obj << /Length 1 >> stream q endstream endobj 303 0 obj << /Length 47088 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.325 0 Td 83.522727 Tz (US ) Tj 1.240909 0 Td 58.038721 Tz (7,829,155 ) Tj 3.388636 0 Td 68.939394 Tz (B1 ) Tj 51.428571 0 0 51.428571 0 2968 Tm 14.875 0 Td 74.537037 Tz (5 ) Tj 51.428571 0 0 51.428571 0 2915.528302 Tm 6.358333 0 Td 51.851852 Tz (closed ) Tj 1.983333 0 Td 51.311728 Tz (herein ) Tj 2.002778 0 Td 54.282407 Tz (demonstrated ) Tj 4.044444 0 Td 57.523148 Tz (enhanced ) Tj 2.897222 0 Td 43.569959 Tz (Stability ) Tj 2.508333 0 Td 59.548611 Tz (compared ) Tj 2.994444 0 Td 46.990741 Tz (to ) Tj 0.719444 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 2875.289631 Tm 6.358333 0 Td 58.333333 Tz (monolayer ) Tj 3.422222 0 Td 61.574074 Tz (of ) Tj 0.952778 0 Td 50.694444 Tz (dodecanethiol. ) Tj 4.588889 0 Td 45.619658 Tz (Specifically, ) Tj 3.888889 0 Td 51.203704 Tz (electrochemical ) Tj 51.428571 0 0 51.428571 0 2833.265537 Tm 6.377778 0 Td 47.530864 Tz (stripping ) Tj 2.955556 0 Td 62.654321 Tz (was ) Tj 1.536111 0 Td 56.532922 Tz (performed ) Tj 3.441667 0 Td 43.75 Tz (in ) Tj 0.952778 0 Td 45.37037 Tz (0.1 ) Tj 1.302778 0 Td 103.703704 Tz (M ) Tj 1.030556 0 Td 45.775463 Tz (sulfuric ) Tj 2.605556 0 Td 51.041667 Tz (acid ) Tj 1.613889 0 Td 43.75 Tz (at ) Tj 0.913889 0 Td 61.574074 Tz (300 ) Tj 51.428571 0 0 51.428571 0 2793.049645 Tm 6.358333 0 Td 58.009259 Tz (mV/second. ) Tj 3.694444 0 Td 64.814815 Tz (The ) Tj 1.380556 0 Td 46.990741 Tz (cyclic ) Tj 1.905556 0 Td 62.222222 Tz (Voltamammograms ) Tj 5.833333 0 Td 59.143519 Tz (were ) Tj 1.594444 0 Td 57.253086 Tz (performed ) Tj 51.428571 0 0 51.428571 0 2751.271186 Tm 6.358333 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 38.888889 Tz (1 ) Tj 0.447222 0 Td 100.462963 Tz (mM ) Tj 1.302778 0 Td 54.73251 Tz (potassium ) Tj 3.111111 0 Td 48.341049 Tz (ferricyanide ) Tj 3.616667 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 67.515432 Tz (1MKC1. ) Tj 2.625 0 Td 44.560185 Tz (Finally, ) Tj 2.255556 0 Td 51.851852 Tz (as ) Tj 0.758333 0 Td 63.518519 Tz (shown ) Tj 51.428571 0 0 51.428571 0 2708.618557 Tm 6.358333 0 Td 45.37037 Tz (in ) Tj 0.875 0 Td 57.037037 Tz (FIGS. ) Tj 2.022222 0 Td 72.916667 Tz (7A ) Tj 1.147222 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 55.092593 Tz (7B, ) Tj 1.302778 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 52.546296 Tz (polymerization ) Tj 4.705556 0 Td 50.231481 Tz (coatings ) Tj 2.722222 0 Td 73.240741 Tz (demon ) Tj 51.428571 0 0 51.428571 0 2667.004878 Tm 6.377778 0 Td 45.833333 Tz (strated ) Tj 2.119444 0 Td 60.763889 Tz (good ) Tj 1.691667 0 Td 54.444444 Tz (mechanical ) Tj 3.461111 0 Td 40.833333 Tz (stability. ) Tj 2.722222 0 Td 42.669753 Tz (Little ) Tj 1.730556 0 Td 57.79321 Tz (change ) Tj 2.275 0 Td 43.75 Tz (in ) Tj 0.738889 0 Td 50.05144 Tz (thickness ) Tj 51.428571 0 0 51.428571 0 2625.597938 Tm 6.338889 0 Td 62.654321 Tz (was ) Tj 1.497222 0 Td 50.636574 Tz (detected ) Tj 2.761111 0 Td 46.018519 Tz (after ) Tj 1.672222 0 Td 50.771605 Tz (the ) Tj 1.263889 0 Td 52.083333 Tz (polymerization ) Tj 4.744444 0 Td 50.231481 Tz (coatings ) Tj 2.780556 0 Td 58.333333 Tz (had ) Tj 1.4 0 Td 58.333333 Tz (been ) Tj 51.428571 0 0 51.428571 0 2582.572979 Tm 6.358333 0 Td 50.636574 Tz (attached ) Tj 2.527778 0 Td 46.990741 Tz (to ) Tj 0.7 0 Td 51.851852 Tz (a ) Tj 0.427778 0 Td 50.378788 Tz (Vortexerset ) Tj 3.422222 0 Td 61.574074 Tz (on ) Tj 0.836111 0 Td 53.472222 Tz (high ) Tj 1.419444 0 Td 48.611111 Tz (for ) Tj 0.952778 0 Td 51.851852 Tz (a ) Tj 0.427778 0 Td 52.391975 Tz (period ) Tj 2.002778 0 Td 53.472222 Tz (of ) Tj 0.719444 0 Td 55.092593 Tz (5 ) Tj 0.505556 0 Td 50.636574 Tz (minutes, ) Tj 2.566667 0 Td 55.092593 Tz (nor ) Tj 51.428571 0 0 51.428571 0 2539.918193 Tm 6.338889 0 Td 65.625 Tz (when ) Tj 1.788889 0 Td 48.611111 Tz (the ) Tj 1.011111 0 Td 53.472222 Tz (coated ) Tj 2.080556 0 Td 50 Tz (surface ) Tj 2.255556 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 52.5 Tz (metal ) Tj 1.75 0 Td 62.654321 Tz (was ) Tj 1.263889 0 Td 50.771605 Tz (gently ) Tj 2.022222 0 Td 56.17284 Tz (rubbed ) Tj 2.197222 0 Td 54.282407 Tz (with ) Tj 48.571429 0 0 48.571429 0 2499 Tm 6.732353 0 Td 58.333333 Tz (a ) Tj 0.535294 0 Td 46.132898 Tz (lint-free ) Tj 2.697059 0 Td 51.470588 Tz (towel, ) Tj 2.058824 0 Td 51.470588 Tz (as ) Tj 0.823529 0 Td 65.882353 Tz (shown ) Tj 2.182353 0 Td 49.754902 Tz (in ) Tj 0.823529 0 Td 57.47549 Tz (FIG. ) Tj 1.605882 0 Td 46.323529 Tz (8. ) Tj 51.428571 0 0 51.428571 0 2457.085928 Tm 7.116667 0 Td 46.990741 Tz (In ) Tj 0.738889 0 Td 53.240741 Tz (another ) Tj 2.372222 0 Td 60.925926 Tz (embodiment ) Tj 3.830556 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 50.462963 Tz (present ) Tj 2.313889 0 Td 47.962963 Tz (invention, ) Tj 3.091667 0 Td 53.06713 Tz (nanothin ) Tj 51.428571 0 0 51.428571 0 2417.455446 Tm 6.358333 0 Td 52.314815 Tz (polymerization ) Tj 4.763889 0 Td 49.826389 Tz (coatings ) Tj 2.741667 0 Td 52.662037 Tz (with ) Tj 1.613889 0 Td 49.259259 Tz (controlled ) Tj 3.286111 0 Td 50.084175 Tz (thicknesses ) Tj 3.675 0 Td 58.333333 Tz (were ) Tj 48.571429 0 0 48.571429 0 2375 Tm 6.732353 0 Td 51.470588 Tz (also ) Tj 1.482353 0 Td 51.127451 Tz (fabricated ) Tj 3.252941 0 Td 54.901961 Tz (as ) Tj 0.905882 0 Td 51.041667 Tz (follows. ) Tj 2.717647 0 Td 49.754902 Tz (In ) Tj 0.844118 0 Td 45.465686 Tz (this ) Tj 1.379412 0 Td 58.333333 Tz (method, ) Tj 2.655882 0 Td 61.764706 Tz (a ) Tj 0.617647 0 Td 55.588235 Tz (metal ) Tj 1.914706 0 Td 50.708061 Tz (substrate ) Tj 51.428571 0 0 51.428571 0 2332.387755 Tm 6.377778 0 Td 54.282407 Tz (Such ) Tj 1.516667 0 Td 51.851852 Tz (as ) Tj 0.816667 0 Td 49.907407 Tz (gold, ) Tj 1.730556 0 Td 61.574074 Tz (was ) Tj 1.341667 0 Td 57.613169 Tz (Submersed ) Tj 3.344444 0 Td 45.37037 Tz (into ) Tj 1.341667 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 56.712963 Tz (hexane ) Tj 2.275 0 Td 48.206019 Tz (solution ) Tj 2.547222 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 63.734568 Tz (par ) Tj 51.428571 0 0 51.428571 0 2296.629108 Tm 6.338889 0 Td 41.589506 Tz (tially ) Tj 1.730556 0 Td 55.681818 Tz (polymerized ) Tj 3.908333 0 Td 50.925926 Tz (4-vinyl-benzenepropanethiol. ) Tj 8.788889 0 Td 84.259259 Tz (A ) Tj 0.758333 0 Td 48.611111 Tz (detailed ) Tj 51.428571 0 0 51.428571 0 2251.939698 Tm 6.358333 0 Td 58.333333 Tz (example ) Tj 2.644444 0 Td 61.574074 Tz (of ) Tj 0.875 0 Td 41.319444 Tz (this ) Tj 1.283333 0 Td 59.41358 Tz (method ) Tj 2.372222 0 Td 38.888889 Tz (is ) Tj 0.661111 0 Td 54.282407 Tz (provided ) Tj 2.838889 0 Td 43.75 Tz (in ) Tj 0.797222 0 Td 61.111111 Tz (Example ) Tj 2.761111 0 Td 43.75 Tz (5. ) Tj 0.797222 0 Td 51.446759 Tz (Detailed ) Tj 51.428571 0 0 51.428571 0 2211.983193 Tm 6.358333 0 Td 56.712963 Tz (examples ) Tj 2.936111 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 53.472222 Tz (applying ) Tj 2.761111 0 Td 52.256944 Tz (nanothin ) Tj 2.683333 0 Td 52.546296 Tz (polymerization ) Tj 4.627778 0 Td 50.231481 Tz (coatings ) Tj 2.605556 0 Td 46.990741 Tz (to ) Tj 0.758333 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 2167.091245 Tm 6.358333 0 Td 54.282407 Tz (gold ) Tj 1.458333 0 Td 52.932099 Tz (coated ) Tj 2.080556 0 Td 45.37037 Tz (silicon ) Tj 2.080556 0 Td 47.890947 Tz (Substrate ) Tj 2.722222 0 Td 50.771605 Tz (are ) Tj 1.05 0 Td 62.222222 Tz (shown ) Tj 2.041667 0 Td 46.990741 Tz (in ) Tj 0.777778 0 Td 58.738426 Tz (Examples ) Tj 2.994444 0 Td 55.092593 Tz (6 ) Tj 0.486111 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 42.12963 Tz (7. ) Tj 51.428571 0 0 51.428571 0 2126.752047 Tm 6.358333 0 Td 59.143519 Tz (Mild ) Tj 1.497222 0 Td 52.777778 Tz (polymerization ) Tj 4.569444 0 Td 60.493827 Tz (was ) Tj 1.205556 0 Td 55.555556 Tz (induced ) Tj 2.391667 0 Td 61.574074 Tz (by ) Tj 0.875 0 Td 54.6875 Tz (exposing ) Tj 2.702778 0 Td 49.691358 Tz (the ) Tj 1.030556 0 Td 53.148148 Tz (crude ) Tj 1.691667 0 Td 83.179012 Tz (com ) Tj 51.428571 0 0 51.428571 0 2087.222354 Tm 6.358333 0 Td 60.925926 Tz (pound ) Tj 1.944444 0 Td 46.990741 Tz (to ) Tj 0.7 0 Td 44.290123 Tz (air ) Tj 0.894444 0 Td 45.37037 Tz (at ) Tj 0.680556 0 Td 62.384259 Tz (room ) Tj 1.633333 0 Td 52.73569 Tz (temperature ) Tj 3.636111 0 Td 48.287037 Tz (overnight. ) Tj 3.013889 0 Td 64.814815 Tz (The ) Tj 1.263889 0 Td 58.796296 Tz (polymer ) Tj 2.586111 0 Td 61.574074 Tz (was ) Tj 40 0 0 40 0 2048 Tm 8.175 0 Td 61.904762 Tz (diluted ) Tj 3 0 Td 56.25 Tz (to ) Tj 1.175 0 Td 93.75 Tz (1% ) Tj 1.55 0 Td 86.111111 Tz (w/w ) Tj 2 0 Td 56.25 Tz (in ) Tj 1.05 0 Td 67.045455 Tz (chloroform. ) Tj 4.8 0 Td 69.791667 Tz (This ) Tj 2.075 0 Td 61.979167 Tz (solution ) Tj 3.375 0 Td 79.166667 Tz (was ) Tj 1.85 0 Td 67.708333 Tz (then ) Tj 51.428571 0 0 51.428571 0 2003.9437 Tm 6.358333 0 Td 48.148148 Tz (diluted ) Tj 2.45 0 Td 45.37037 Tz (to ) Tj 0.972222 0 Td 49.691358 Tz (the ) Tj 1.263889 0 Td 50.555556 Tz (equivalent ) Tj 3.441667 0 Td 58.333333 Tz (of ) Tj 1.088889 0 Td 32.407407 Tz (1 ) Tj 0.719444 0 Td 98.842593 Tz (mM ) Tj 1.594444 0 Td 54.912551 Tz (4-vinyl-benzenepro ) Tj 51.428571 0 0 51.428571 0 1958.347879 Tm 6.358333 0 Td 50.05144 Tz (panethiol ) Tj 2.916667 0 Td 53.472222 Tz (with ) Tj 1.438889 0 Td 57.79321 Tz (hexane ) Tj 2.236111 0 Td 60.493827 Tz (and ) Tj 1.263889 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 47.638889 Tz (substrates ) Tj 3.052778 0 Td 59.143519 Tz (were ) Tj 1.613889 0 Td 57.613169 Tz (submersed ) Tj 3.286111 0 Td 50.231481 Tz (in ) Tj 51.428571 0 0 51.428571 0 1915.591398 Tm 6.338889 0 Td 44.560185 Tz (this ) Tj 1.380556 0 Td 46.090535 Tz (solution. ) Tj 2.838889 0 Td 34.027778 Tz (It ) Tj 0.7 0 Td 40.509259 Tz (is ) Tj 0.797222 0 Td 53.148148 Tz (noted ) Tj 1.866667 0 Td 46.180556 Tz (that ) Tj 1.419444 0 Td 53.148148 Tz (while ) Tj 1.886111 0 Td 57.253086 Tz (hexane ) Tj 2.352778 0 Td 60.493827 Tz (was ) Tj 1.4 0 Td 49.907407 Tz (used, ) Tj 1.788889 0 Td 59.41358 Tz (any ) Tj 51.428571 0 0 51.428571 0 1875.821053 Tm 6.358333 0 Td 51.388889 Tz (organic ) Tj 2.411111 0 Td 50 Tz (solvent ) Tj 2.352778 0 Td 66.975309 Tz (may ) Tj 1.458333 0 Td 48.611111 Tz (also ) Tj 1.4 0 Td 56.712963 Tz (be ) Tj 0.913889 0 Td 49.907407 Tz (used. ) Tj 1.711111 0 Td 66.435185 Tz (As ) Tj 1.069444 0 Td 61.574074 Tz (shown ) Tj 2.1 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 54.282407 Tz (FIG. ) Tj 1.536111 0 Td 46.990741 Tz (9, ) Tj 0.797222 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 1836.216606 Tm 6.338889 0 Td 50.411523 Tz (thickness ) Tj 2.916667 0 Td 56.712963 Tz (of ) Tj 0.738889 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 52.546296 Tz (polymerization ) Tj 4.608333 0 Td 50.925926 Tz (coating ) Tj 2.313889 0 Td 54.552469 Tz (ranged ) Tj 2.158333 0 Td 56.712963 Tz (from ) Tj 1.555556 0 Td 54.444444 Tz (about ) Tj 1.808333 0 Td 55.092593 Tz (2 ) Tj 48.571429 0 0 48.571429 0 1793 Tm 6.773529 0 Td 77.205882 Tz (nm ) Tj 1.132353 0 Td 46.323529 Tz (to ) Tj 0.720588 0 Td 61.764706 Tz (5 ) Tj 0.597059 0 Td 77.205882 Tz (nm ) Tj 1.091176 0 Td 61.764706 Tz (and ) Tj 1.255882 0 Td 58.333333 Tz (could ) Tj 1.894118 0 Td 61.764706 Tz (be ) Tj 0.885294 0 Td 52.156863 Tz (controlled ) Tj 3.294118 0 Td 55.759804 Tz (with ) Tj 1.523529 0 Td 50.784314 Tz (time. ) Tj 1.729412 0 Td 50.183824 Tz (Further, ) Tj 2.552941 0 Td 60.392157 Tz (based ) Tj 51.428571 0 0 51.428571 0 1753.293671 Tm 6.338889 0 Td 59.953704 Tz (upon ) Tj 1.711111 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 56.388889 Tz (phase ) Tj 1.925 0 Td 48.206019 Tz (contrast ) Tj 2.527778 0 Td 55.092593 Tz (atomic ) Tj 2.255556 0 Td 49.259259 Tz (force ) Tj 1.730556 0 Td 55.740741 Tz (microscopy ) Tj 3.616667 0 Td 58.981481 Tz (image ) Tj 2.022222 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 1712.815725 Tm 6.338889 0 Td 52.211934 Tz (bare-gold ) Tj 3.013889 0 Td 46.018519 Tz (Substrate, ) Tj 2.955556 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 55.092593 Tz (3 ) Tj 0.583333 0 Td 74.537037 Tz (nm ) Tj 1.127778 0 Td 52.314815 Tz (polymerization ) Tj 4.608333 0 Td 48.206019 Tz (coating, ) Tj 2.527778 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1669.811944 Tm 6.358333 0 Td 52.314815 Tz (polymerization ) Tj 4.686111 0 Td 50.925926 Tz (coating ) Tj 2.411111 0 Td 58.333333 Tz (had ) Tj 1.322222 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 59.41358 Tz (smooth ) Tj 2.391667 0 Td 48.148148 Tz (texture ) Tj 2.294444 0 Td 50.231481 Tz (as ) Tj 0.875 0 Td 62.222222 Tz (shown ) Tj 2.138889 0 Td 63.194444 Tz (by ) Tj 52.857143 0 0 52.857143 0 1627.631056 Tm 6.186486 0 Td 45.195195 Tz (analysis. ) Tj 2.705405 0 Td 36.261261 Tz (It ) Tj 0.643243 0 Td 39.414414 Tz (is ) Tj 0.7 0 Td 46.846847 Tz (further ) Tj 2.194595 0 Td 51.081081 Tz (noted ) Tj 1.721622 0 Td 46.509009 Tz (that ) Tj 1.324324 0 Td 49.399399 Tz (the ) Tj 1.116216 0 Td 50.675676 Tz (polymerization ) Tj 4.483784 0 Td 50.45045 Tz (coating ) Tj 48.571429 0 0 48.571429 0 1584 Tm 6.711765 0 Td 66.339869 Tz (was ) Tj 1.379412 0 Td 48.039216 Tz (resistant ) Tj 2.738235 0 Td 49.754902 Tz (to ) Tj 0.761765 0 Td 66.911765 Tz (30 ) Tj 1.008824 0 Td 56.862745 Tz (minutes ) Tj 2.594118 0 Td 60.04902 Tz (of ) Tj 0.802941 0 Td 60.620915 Tz (immersion ) Tj 3.458824 0 Td 48.039216 Tz (in ) Tj 0.761765 0 Td 56.372549 Tz (hexane, ) Tj 2.532353 0 Td 51.041667 Tz (toluene, ) Tj 51.428571 0 0 51.428571 0 1542.133333 Tm 6.358333 0 Td 47.800926 Tz (ethanol, ) Tj 2.469444 0 Td 60.493827 Tz (and ) Tj 1.302778 0 Td 77.777778 Tz (1M ) Tj 1.088889 0 Td 54.73251 Tz (potassium ) Tj 3.15 0 Td 46.450617 Tz (chloride. ) Tj 2.722222 0 Td 50.771605 Tz (Stated ) Tj 1.983333 0 Td 52.777778 Tz (another ) Tj 2.372222 0 Td 55.092593 Tz (way, ) Tj 1.497222 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1502.096459 Tm 6.338889 0 Td 50.411523 Tz (thickness ) Tj 2.877778 0 Td 52.932099 Tz (did ) Tj 1.127778 0 Td 49.691358 Tz (not ) Tj 1.069444 0 Td 45.619658 Tz (significantly ) Tj 3.713889 0 Td 54.282407 Tz (changed, ) Tj 2.741667 0 Td 51.851852 Tz (as ) Tj 0.777778 0 Td 62.222222 Tz (shown ) Tj 2.041667 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 54.282407 Tz (FIG. ) Tj 1.516667 0 Td 47.530864 Tz (10. ) Tj 51.428571 0 0 51.428571 0 1461.672566 Tm 6.358333 0 Td 51.851852 Tz (Also, ) Tj 1.847222 0 Td 43.75 Tz (in ) Tj 0.797222 0 Td 53.796296 Tz (terms ) Tj 1.886111 0 Td 56.712963 Tz (of ) Tj 0.855556 0 Td 41.157407 Tz (Stability, ) Tj 2.722222 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 52.314815 Tz (polymerization ) Tj 4.686111 0 Td 50.462963 Tz (coating ) Tj 2.391667 0 Td 61.574074 Tz (was ) Tj 40 0 0 40 0 1423 Tm 8.175 0 Td 62.5 Tz (also ) Tj 1.8 0 Td 57.407407 Tz (resistant ) Tj 3.35 0 Td 58.333333 Tz (to ) Tj 1.05 0 Td 75 Tz (100 ) Tj 1.6 0 Td 66.666667 Tz (scans ) Tj 2.25 0 Td 75 Tz (from ) Tj 2.075 0 Td 69.791667 Tz (-1.5 ) Tj 1.975 0 Td 58.333333 Tz (volts ) Tj 2.025 0 Td 58.333333 Tz (to ) Tj 1 0 Td 68.75 Tz (-0.5 ) Tj 1.925 0 Td 59.166667 Tz (volts ) Tj 2.025 0 Td 77.777778 Tz (and ) Tj 51.428571 0 0 51.428571 0 1375.57775 Tm 6.358333 0 Td 46.450617 Tz (0.1 ) Tj 1.186111 0 Td 55.740741 Tz (molar ) Tj 1.905556 0 Td 45.37037 Tz (sulfuric ) Tj 2.411111 0 Td 46.018519 Tz (acid, ) Tj 1.652778 0 Td 58.333333 Tz (which ) Tj 2.002778 0 Td 47.222222 Tz (readily ) Tj 2.275 0 Td 56.944444 Tz (removes ) Tj 2.605556 0 Td 58.333333 Tz (any ) Tj 1.283333 0 Td 50.925926 Tz (self-as ) Tj 51.428571 0 0 51.428571 0 1333.52019 Tm 6.377778 0 Td 57.407407 Tz (sembled ) Tj 2.566667 0 Td 57.613169 Tz (monolayer ) Tj 3.208333 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 50.231481 Tz (dodecanethiol. ) Tj 4.336111 0 Td 55.092593 Tz (Thus, ) Tj 1.769444 0 Td 50.231481 Tz (as ) Tj 0.758333 0 Td 62.222222 Tz (shown ) Tj 2.022222 0 Td 43.75 Tz (in ) Tj 0.7 0 Td 54.282407 Tz (FIG. ) Tj 51.428571 0 0 51.428571 0 1296.094431 Tm 6.377778 0 Td 49.691358 Tz (11, ) Tj 1.088889 0 Td 48.611111 Tz (the ) Tj 1.088889 0 Td 52.314815 Tz (polymerization ) Tj 4.588889 0 Td 51.388889 Tz (coating ) Tj 2.333333 0 Td 62.654321 Tz (was ) Tj 1.322222 0 Td 47.115385 Tz (substantially ) Tj 3.908333 0 Td 61.574074 Tz (more ) Tj 1.652778 0 Td 60.763889 Tz (insu ) Tj 51.428571 0 0 51.428571 0 1251.677596 Tm 6.358333 0 Td 45.910494 Tz (lating ) Tj 2.197222 0 Td 50.231481 Tz (than ) Tj 1.788889 0 Td 49.691358 Tz (the ) Tj 1.438889 0 Td 51.157407 Tz (self-assembled ) Tj 4.841667 0 Td 57.613169 Tz (monolayer ) Tj 3.616667 0 Td 59.953704 Tz (of ) Tj 1.225 0 Td 56.018519 Tz (1.6-hex ) Tj 51.428571 0 0 51.428571 0 1209.578544 Tm 6.358333 0 Td 48.287037 Tz (anedithiol ) Tj 3.072222 0 Td 55.632716 Tz (having ) Tj 2.158333 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 48.611111 Tz (similar ) Tj 2.197222 0 Td 47.638889 Tz (thickness. ) Tj 51.428571 0 0 51.428571 0 1168.851175 Tm 7.116667 0 Td 55.902778 Tz (Evidence ) Tj 2.936111 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 55.902778 Tz (complete ) Tj 2.916667 0 Td 54.6875 Tz (coverage ) Tj 2.858333 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 53.148148 Tz (metal ) Tj 1.866667 0 Td 50 Tz (surface ) Tj 40 0 0 40 0 1132 Tm 8.15 0 Td 80.555556 Tz (was ) Tj 1.675 0 Td 65.47619 Tz (derived ) Tj 2.925 0 Td 75 Tz (from ) Tj 2 0 Td 68.75 Tz (both ) Tj 1.85 0 Td 58.75 Tz (structural ) Tj 3.675 0 Td 76.388889 Tz (and ) Tj 1.55 0 Td 63.333333 Tz (functional ) Tj 3.95 0 Td 67.361111 Tz (characteriza ) Tj 51.428571 0 0 51.428571 0 1085.226506 Tm 6.338889 0 Td 47.800926 Tz (tion ) Tj 1.341667 0 Td 45.37037 Tz (studies. ) Tj 2.372222 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 45.694444 Tz (structural ) Tj 2.936111 0 Td 53.877315 Tz (evidence ) Tj 2.761111 0 Td 38.888889 Tz (is ) Tj 0.719444 0 Td 57.523148 Tz (most ) Tj 1.575 0 Td 49.907407 Tz (straightforward ) Tj 51.428571 0 0 51.428571 0 1045.667516 Tm 6.358333 0 Td 45.37037 Tz (in ) Tj 0.894444 0 Td 59.953704 Tz (Atomic ) Tj 2.547222 0 Td 54.444444 Tz (Force ) Tj 1.963889 0 Td 57.685185 Tz (Microscopy ) Tj 3.85 0 Td 67.407407 Tz (\(AFM\) ) Tj 2.411111 0 Td 52.662037 Tz (imaging, ) Tj 2.897222 0 Td 48.611111 Tz (especially ) Tj 51.428571 0 0 51.428571 0 1005.525872 Tm 6.358333 0 Td 51.49177 Tz (involving ) Tj 2.955556 0 Td 48.179012 Tz (polycrystalline ) Tj 4.55 0 Td 53.148148 Tz (metal ) Tj 1.808333 0 Td 46.8107 Tz (Surfaces. ) Tj 2.8 0 Td 45.37037 Tz (In ) Tj 0.777778 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 48.148148 Tz (representative ) Tj 51.428571 0 0 51.428571 0 959.820972 Tm 6.358333 0 Td 87.5 Tz (AFM ) Tj 1.847222 0 Td 52.441077 Tz (experiment, ) Tj 3.772222 0 Td 60.493827 Tz (random ) Tj 2.488889 0 Td 49.259259 Tz (areas ) Tj 1.788889 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 51.851852 Tz (bare ) Tj 1.575 0 Td 52.5 Tz (metal ) Tj 1.847222 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 53.472222 Tz (coated ) Tj 51.428571 0 0 51.428571 0 920.686369 Tm 6.358333 0 Td 53.796296 Tz (metal ) Tj 1.769444 0 Td 59.143519 Tz (were ) Tj 1.575 0 Td 54.166667 Tz (imaged. ) Tj 2.488889 0 Td 57.407407 Tz (Samples ) Tj 2.625 0 Td 55.092593 Tz (of ) Tj 0.738889 0 Td 51.851852 Tz (bare ) Tj 1.419444 0 Td 53.148148 Tz (metal ) Tj 1.769444 0 Td 59.953704 Tz (showed ) Tj 2.333333 0 Td 57.118056 Tz (polycrys ) Tj 51.428571 0 0 51.428571 0 877.542787 Tm 6.338889 0 Td 43.981481 Tz (talline ) Tj 2.061111 0 Td 47.530864 Tz (structure ) Tj 2.8 0 Td 52.662037 Tz (with ) Tj 1.516667 0 Td 48.287037 Tz (individual ) Tj 3.169444 0 Td 45.37037 Tz (crystals ) Tj 2.430556 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 53.148148 Tz (metal ) Tj 1.808333 0 Td 53.292181 Tz (averaging ) Tj 51.428571 0 0 51.428571 0 836.411471 Tm 6.358333 0 Td 61.574074 Tz (300x300 ) Tj 2.897222 0 Td 57.253086 Tz (nm. ) Tj 1.302778 0 Td 63.734568 Tz (The ) Tj 1.4 0 Td 54.398148 Tz (polymer-coated ) Tj 4.822222 0 Td 57.79321 Tz (sample ) Tj 2.333333 0 Td 61.033951 Tz (showed ) Tj 2.488889 0 Td 45.37037 Tz (that ) Tj 1.341667 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 795.989744 Tm 6.358333 0 Td 48.395062 Tz (polycrystalline ) Tj 4.802778 0 Td 47.530864 Tz (structure ) Tj 3.013889 0 Td 60.493827 Tz (was ) Tj 1.575 0 Td 53.472222 Tz (completely ) Tj 3.675 0 Td 51.851852 Tz (obscured. ) Tj 3.266667 0 Td 63.734568 Tz (The ) Tj 51.428571 0 0 51.428571 0 753.855181 Tm 6.358333 0 Td 54.372428 Tz (roughness ) Tj 3.208333 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 54.398148 Tz (polymer-coated ) Tj 4.822222 0 Td 49.537037 Tz (Surface ) Tj 2.313889 0 Td 40.509259 Tz (is ) Tj 0.738889 0 Td 46.090535 Tz (identical ) Tj 2.741667 0 Td 45.37037 Tz (to ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 712.700234 Tm 6.358333 0 Td 54.372428 Tz (roughness ) Tj 3.072222 0 Td 55.092593 Tz (ofbare ) Tj 2.1 0 Td 53.148148 Tz (metal ) Tj 1.711111 0 Td 53.703704 Tz (proving ) Tj 2.372222 0 Td 45.37037 Tz (that ) Tj 1.186111 0 Td 50.771605 Tz (the ) Tj 0.991667 0 Td 59.259259 Tz (polymer ) Tj 2.586111 0 Td 49.016204 Tz (material ) Tj 2.45 0 Td 55.092593 Tz (has ) Tj 51.428571 0 0 51.428571 0 668.873536 Tm 6.358333 0 Td 55.092593 Tz (a ) Tj 0.447222 0 Td 55.555556 Tz (uniform ) Tj 2.469444 0 Td 47.638889 Tz (thickness. ) Tj 3.013889 0 Td 49.85755 Tz (Ellipsometric ) Tj 4.063889 0 Td 57.253086 Tz (measurements ) Tj 4.258333 0 Td 53.472222 Tz (of ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.011111 0 Td 63.194444 Tz (same ) Tj 51.428571 0 0 51.428571 0 628.363171 Tm 6.377778 0 Td 56.712963 Tz (sample ) Tj 2.313889 0 Td 61.574074 Tz (showed ) Tj 2.469444 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 46.450617 Tz (3.1 ) Tj 1.244444 0 Td 71.296296 Tz (nm ) Tj 1.127778 0 Td 50.411523 Tz (thickness ) Tj 3.033333 0 Td 55.092593 Tz (of ) Tj 0.855556 0 Td 58.333333 Tz (polymer ) Tj 2.702778 0 Td 46.8107 Tz (material. ) Tj 51.428571 0 0 51.428571 0 587.130435 Tm 6.358333 0 Td 58.333333 Tz (These ) Tj 2.002778 0 Td 50.771605 Tz (observations ) Tj 3.927778 0 Td 50.231481 Tz (conclusively ) Tj 3.927778 0 Td 53.324916 Tz (demonstrate ) Tj 3.811111 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 55.902778 Tz (complete ) Tj 51.428571 0 0 51.428571 0 544.894032 Tm 6.358333 0 Td 54.282407 Tz (coverage ) Tj 2.780556 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 52.5 Tz (metal ) Tj 1.769444 0 Td 50.462963 Tz (Surface ) Tj 2.275 0 Td 59.953704 Tz (by ) Tj 0.875 0 Td 51.851852 Tz (the ) Tj 1.108333 0 Td 52.662037 Tz (nanothin ) Tj 2.722222 0 Td 58.333333 Tz (polymer ) Tj 2.625 0 Td 59.143519 Tz (coat ) Tj 38.571429 0 0 38.571429 0 507 Tm 8.477778 0 Td 60.493827 Tz (1ng. ) Tj 51.428571 0 0 51.428571 0 460.729167 Tm 7.116667 0 Td 46.990741 Tz (In ) Tj 0.816667 0 Td 49.421296 Tz (addition ) Tj 2.625 0 Td 45.37037 Tz (to ) Tj 0.855556 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 45.959596 Tz (Substrates, ) Tj 3.247222 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 53.796296 Tz (technology ) Tj 3.5 0 Td 50.411523 Tz (disclosed ) Tj 51.428571 0 0 51.428571 0 421.166461 Tm 6.338889 0 Td 50.771605 Tz (herein ) Tj 2.041667 0 Td 68.055556 Tz (may ) Tj 1.419444 0 Td 48.611111 Tz (also ) Tj 1.361111 0 Td 58.333333 Tz (be ) Tj 0.855556 0 Td 51.851852 Tz (applied ) Tj 2.333333 0 Td 48.611111 Tz (to ) Tj 0.777778 0 Td 51.041667 Tz (coat ) Tj 1.4 0 Td 50.555556 Tz (other ) Tj 1.711111 0 Td 46.450617 Tz (Surfaces. ) Tj 2.741667 0 Td 59.143519 Tz (Ellipsom ) Tj 51.428571 0 0 51.428571 0 377.82473 Tm 6.358333 0 Td 46.990741 Tz (etry ) Tj 1.302778 0 Td 53.472222 Tz (provided ) Tj 2.761111 0 Td 53.877315 Tz (evidence ) Tj 2.761111 0 Td 45.37037 Tz (that ) Tj 1.283333 0 Td 43.287037 Tz (silicon/silica ) Tj 3.85 0 Td 47.314815 Tz (substrates ) Tj 3.013889 0 Td 54.444444 Tz (could ) Tj 1.788889 0 Td 59.953704 Tz (be ) Tj 51.428571 0 0 51.428571 0 338.786925 Tm 6.358333 0 Td 52.932099 Tz (coated ) Tj 2.1 0 Td 52.662037 Tz (with ) Tj 1.458333 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 58.796296 Tz (polymer ) Tj 2.625 0 Td 51.388889 Tz (coating ) Tj 2.313889 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 53.292181 Tz (63.8+18.8 ) Tj 3.072222 0 Td 55.092593 Tz (angstroms ) Tj 3.188889 0 Td 46.018519 Tz (after ) Tj 51.428571 0 0 51.428571 0 296.111682 Tm 6.416667 0 Td 56.712963 Tz (16 ) Tj 0.913889 0 Td 49.151235 Tz (hours. ) Tj 2.041667 0 Td 50.555556 Tz (Also, ) Tj 1.808333 0 Td 55.092593 Tz (copper ) Tj 2.197222 0 Td 46.254209 Tz (Substrates, ) Tj 3.325 0 Td 54.282407 Tz (such ) Tj 1.555556 0 Td 50.231481 Tz (as ) Tj 0.855556 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 55.632716 Tz (copper ) Tj 2.197222 0 Td 52.932099 Tz (penny, ) Tj 51.428571 0 0 51.428571 0 252.345695 Tm 6.338889 0 Td 59.953704 Tz (were ) Tj 1.769444 0 Td 57.253086 Tz (submersed ) Tj 3.402778 0 Td 45.37037 Tz (in ) Tj 0.875 0 Td 51.851852 Tz (a ) Tj 0.622222 0 Td 58.796296 Tz (polymer ) Tj 2.741667 0 Td 48.611111 Tz (solution ) Tj 2.663889 0 Td 48.611111 Tz (for ) Tj 1.205556 0 Td 55.092593 Tz (16 ) Tj 0.952778 0 Td 50.231481 Tz (hours. ) Tj 2.119444 0 Td 63.734568 Tz (The ) Tj 51.428571 0 0 51.428571 0 215.46848 Tm 6.358333 0 Td 53.240741 Tz (pennies ) Tj 2.469444 0 Td 55.092593 Tz (having ) Tj 2.197222 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 52.314815 Tz (polymerization ) Tj 4.666667 0 Td 50.925926 Tz (coating ) Tj 2.391667 0 Td 51.851852 Tz (did ) Tj 1.186111 0 Td 51.851852 Tz (not ) Tj 1.186111 0 Td 73.240741 Tz (demon ) Tj 51.428571 0 0 51.428571 0 169.186972 Tm 6.377778 0 Td 43.75 Tz (strate ) Tj 1.711111 0 Td 51.131687 Tz (corrosion ) Tj 2.955556 0 Td 48.611111 Tz (as ) Tj 0.797222 0 Td 50.771605 Tz (did ) Tj 1.108333 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 49.259259 Tz (controlled ) Tj 3.111111 0 Td 49.826389 Tz (pennies. ) Tj 2.644444 0 Td 56.442901 Tz (Electrochemi ) Tj 30 0 0 30 0 2755 Tm 41.833333 0 Td 72.222222 Tz (5 ) Tj 30 0 0 30 0 2547 Tm 41.666667 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.666667 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.6 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.6 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.6 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.566667 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.566667 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.6 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.6 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.633333 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.633333 0 Td 75 Tz (65 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.9 0 Td 69.369369 Tz (6 ) Tj 51.428571 0 0 51.428571 0 2917.798017 Tm 25.297222 0 Td 46.450617 Tz (cal ) Tj 1.166667 0 Td 50.231481 Tz (data ) Tj 1.516667 0 Td 50.231481 Tz (conclusively ) Tj 3.947222 0 Td 53.914141 Tz (demonstrate ) Tj 3.85 0 Td 47.962963 Tz (insulating ) Tj 3.15 0 Td 48.611111 Tz (properties ) Tj 3.247222 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 2875.493917 Tm 25.297222 0 Td 58.333333 Tz (polymer ) Tj 2.644444 0 Td 49.826389 Tz (coatings ) Tj 2.644444 0 Td 51.131687 Tz (described ) Tj 2.955556 0 Td 46.990741 Tz (in ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 50.925926 Tz (present ) Tj 2.352778 0 Td 47.314815 Tz (invention. ) Tj 3.072222 0 Td 64.814815 Tz (Corro ) Tj 51.428571 0 0 51.428571 0 2832.670199 Tm 25.316667 0 Td 50.231481 Tz (sion ) Tj 1.458333 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 51.851852 Tz (the ) Tj 1.205556 0 Td 55.092593 Tz (copper ) Tj 2.236111 0 Td 49.016204 Tz (material ) Tj 2.625 0 Td 61.574074 Tz (was ) Tj 1.4 0 Td 54.62963 Tz (induced ) Tj 2.527778 0 Td 61.574074 Tz (by ) Tj 0.991667 0 Td 51.851852 Tz (placing ) Tj 2.430556 0 Td 34.027778 Tz (it ) Tj 0.680556 0 Td 37.268519 Tz (is ) Tj 0.719444 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 2790.488665 Tm 25.316667 0 Td 47.800926 Tz (solution ) Tj 2.586111 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 52.932099 Tz (bleach ) Tj 2.177778 0 Td 51.49177 Tz (overnight ) Tj 3.033333 0 Td 51.851852 Tz (\(about ) Tj 2.138889 0 Td 56.712963 Tz (24 ) Tj 0.991667 0 Td 47.685185 Tz (hours\). ) Tj 2.255556 0 Td 64.814815 Tz (The ) Tj 1.419444 0 Td 56.17284 Tz (copper ) Tj 51.428571 0 0 51.428571 0 2748.246626 Tm 25.297222 0 Td 53.796296 Tz (metal ) Tj 1.808333 0 Td 50 Tz (surface ) Tj 2.275 0 Td 46.180556 Tz (that ) Tj 1.302778 0 Td 60.493827 Tz (was ) Tj 1.283333 0 Td 52.932099 Tz (coated ) Tj 2.1 0 Td 52.662037 Tz (with ) Tj 1.458333 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 58.796296 Tz (polymer ) Tj 2.644444 0 Td 51.49177 Tz (described ) Tj 2.955556 0 Td 50.231481 Tz (in ) Tj 51.428571 0 0 51.428571 0 2708.946796 Tm 25.277778 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 50.462963 Tz (present ) Tj 2.294444 0 Td 47.638889 Tz (invention, ) Tj 3.052778 0 Td 45.640432 Tz (specifically ) Tj 3.5 0 Td 60.185185 Tz (Example ) Tj 2.702778 0 Td 43.75 Tz (5, ) Tj 0.719444 0 Td 50.771605 Tz (did ) Tj 1.108333 0 Td 49.691358 Tz (not ) Tj 1.030556 0 Td 48.611111 Tz (exhibit ) Tj 51.428571 0 0 51.428571 0 2665.811321 Tm 25.316667 0 Td 47.962963 Tz (signs ) Tj 1.711111 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 48.611111 Tz (corrosion. ) Tj 3.15 0 Td 52.777778 Tz (Control ) Tj 2.45 0 Td 57.253086 Tz (sample ) Tj 2.255556 0 Td 46.180556 Tz (that ) Tj 1.322222 0 Td 61.574074 Tz (was ) Tj 1.361111 0 Td 50.771605 Tz (not ) Tj 1.147222 0 Td 52.391975 Tz (coated ) Tj 2.119444 0 Td 62.654321 Tz (cor ) Tj 51.428571 0 0 51.428571 0 2627.527273 Tm 25.297222 0 Td 55.092593 Tz (roded ) Tj 1.847222 0 Td 43.981481 Tz (significantly. ) Tj 51.428571 0 0 51.428571 0 2586.995134 Tm 26.016667 0 Td 53.472222 Tz (This ) Tj 1.419444 0 Td 49.691358 Tz (patent ) Tj 1.886111 0 Td 48.611111 Tz (application ) Tj 3.363889 0 Td 50.05144 Tz (expressly ) Tj 2.838889 0 Td 49.691358 Tz (incorporates ) Tj 3.694444 0 Td 58.333333 Tz (by ) Tj 0.836111 0 Td 50.411523 Tz (reference ) Tj 51.428571 0 0 51.428571 0 2542.010101 Tm 25.297222 0 Td 39.969136 Tz (all ) Tj 0.913889 0 Td 46.585648 Tz (patents, ) Tj 2.411111 0 Td 48.021886 Tz (references, ) Tj 3.363889 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 49.421296 Tz (publications ) Tj 3.772222 0 Td 49.691358 Tz (disclosed ) Tj 2.858333 0 Td 47.222222 Tz (herein. ) Tj 51.428571 0 0 51.428571 0 2499.482077 Tm 26.016667 0 Td 57.118056 Tz (Although ) Tj 2.877778 0 Td 49.691358 Tz (the ) Tj 0.991667 0 Td 50.925926 Tz (present ) Tj 2.236111 0 Td 50.411523 Tz (invention ) Tj 2.838889 0 Td 52.932099 Tz (has ) Tj 1.088889 0 Td 56.712963 Tz (been ) Tj 1.516667 0 Td 51.49177 Tz (described ) Tj 2.916667 0 Td 43.75 Tz (in ) Tj 0.661111 0 Td 53.796296 Tz (terms ) Tj 51.428571 0 0 51.428571 0 2458.669845 Tm 25.297222 0 Td 58.333333 Tz (of ) Tj 0.758333 0 Td 46.180556 Tz (specific ) Tj 2.372222 0 Td 57.253086 Tz (embodiments, ) Tj 4.297222 0 Td 32.407407 Tz (it ) Tj 0.563889 0 Td 38.888889 Tz (is ) Tj 0.602778 0 Td 48.905724 Tz (anticipated ) Tj 3.363889 0 Td 46.180556 Tz (that ) Tj 1.263889 0 Td 45.664983 Tz (alterations ) Tj 3.188889 0 Td 59.41358 Tz (and ) Tj 51.428571 0 0 51.428571 0 2415.215548 Tm 25.297222 0 Td 50.605413 Tz (modifications ) Tj 4.083333 0 Td 50.378788 Tz (thereofwill ) Tj 3.480556 0 Td 58.333333 Tz (no ) Tj 0.855556 0 Td 55.092593 Tz (doubt ) Tj 1.769444 0 Td 63.194444 Tz (become ) Tj 2.391667 0 Td 52.256944 Tz (apparent ) Tj 2.663889 0 Td 45.37037 Tz (to ) Tj 0.680556 0 Td 51.851852 Tz (those ) Tj 51.428571 0 0 51.428571 0 2374.491003 Tm 25.316667 0 Td 45.833333 Tz (skilled ) Tj 2.138889 0 Td 46.990741 Tz (in ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 38.888889 Tz (art. ) Tj 1.225 0 Td 35.648148 Tz (It ) Tj 0.661111 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 48.971193 Tz (therefore ) Tj 2.858333 0 Td 52.256944 Tz (intended ) Tj 2.741667 0 Td 45.37037 Tz (that ) Tj 1.322222 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 52.211934 Tz (following ) Tj 51.428571 0 0 51.428571 0 2333.866995 Tm 25.297222 0 Td 52.391975 Tz (claims ) Tj 2.080556 0 Td 59.953704 Tz (be ) Tj 0.933333 0 Td 47.727273 Tz (interpreted ) Tj 3.344444 0 Td 48.611111 Tz (as ) Tj 0.836111 0 Td 52.256944 Tz (covering ) Tj 2.683333 0 Td 41.049383 Tz (all ) Tj 0.952778 0 Td 45.664983 Tz (alterations ) Tj 3.208333 0 Td 60.493827 Tz (and ) Tj 1.322222 0 Td 58.333333 Tz (modifi ) Tj 51.428571 0 0 51.428571 0 2291.626098 Tm 25.297222 0 Td 48.611111 Tz (cations ) Tj 2.255556 0 Td 45.37037 Tz (that ) Tj 1.263889 0 Td 38.888889 Tz (fall ) Tj 1.147222 0 Td 50.771605 Tz (within ) Tj 2.041667 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 46.180556 Tz (true ) Tj 1.302778 0 Td 41.049383 Tz (spirit ) Tj 1.633333 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 55.740741 Tz (scope ) Tj 1.827778 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 60.277778 Tz (inven ) Tj 40 0 0 40 0 2256 Tm 32.5 0 Td 55.833333 Tz (tion. ) Tj 38.571429 0 0 38.571429 0 2175 Tm 42.82963 0 Td 105.864198 Tz (EXAMPLES ) Tj 51.428571 0 0 51.428571 0 2091.337931 Tm 32.472222 0 Td 61.574074 Tz (Example ) Tj 2.819444 0 Td 38.888889 Tz (1 ) Tj 51.428571 0 0 51.428571 0 2008.590044 Tm 27.261111 0 Td 50.378788 Tz (Preparation ) Tj 3.519444 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 55.208333 Tz (p-\(3-Bromopropl\)acetophenone ) Tj 51.428571 0 0 51.428571 0 1920.271845 Tm 26.075 0 Td 55.233494 Tz (1-bromo-3-phenylpropane ) Tj 7.738889 0 Td 62.654321 Tz (was ) Tj 1.263889 0 Td 54.372428 Tz (purchased ) Tj 3.091667 0 Td 57.523148 Tz (from ) Tj 1.516667 0 Td 58.333333 Tz (a ) Tj 0.466667 0 Td 72.376543 Tz (commer ) Tj 51.428571 0 0 51.428571 0 1875.003764 Tm 25.297222 0 Td 44.290123 Tz (cially ) Tj 1.788889 0 Td 48.611111 Tz (available ) Tj 2.8 0 Td 48.611111 Tz (source. ) Tj 2.294444 0 Td 46.990741 Tz (In ) Tj 0.758333 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 47.800926 Tz (reaction ) Tj 2.508333 0 Td 46.666667 Tz (flask ) Tj 1.613889 0 Td 55.092593 Tz (15 ) Tj 0.855556 0 Td 58.333333 Tz (g ) Tj 0.583333 0 Td 55.092593 Tz (of ) Tj 0.758333 0 Td 61.979167 Tz (aluminum ) Tj 51.428571 0 0 51.428571 0 1833.583653 Tm 25.297222 0 Td 49.826389 Tz (chloride ) Tj 2.625 0 Td 62.654321 Tz (was ) Tj 1.380556 0 Td 58.333333 Tz (added ) Tj 1.983333 0 Td 45.37037 Tz (to ) Tj 0.894444 0 Td 57.253086 Tz (100 ) Tj 1.283333 0 Td 82.638889 Tz (mL ) Tj 1.225 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 55.812757 Tz (methylene ) Tj 3.266667 0 Td 46.8107 Tz (chloride. ) Tj 2.8 0 Td 62.654321 Tz (The ) Tj 51.428571 0 0 51.428571 0 1792.391716 Tm 25.297222 0 Td 48.611111 Tz (reaction ) Tj 2.469444 0 Td 46.666667 Tz (flask ) Tj 1.516667 0 Td 60.493827 Tz (was ) Tj 1.225 0 Td 52.211934 Tz (incubated ) Tj 2.955556 0 Td 45.37037 Tz (in ) Tj 0.661111 0 Td 47.638889 Tz (apartially ) Tj 3.013889 0 Td 57.613169 Tz (Submersed ) Tj 3.227778 0 Td 47.530864 Tz (ice ) Tj 0.952778 0 Td 47.314815 Tz (bath. ) Tj 51.428571 0 0 51.428571 0 1752.333333 Tm 25.316667 0 Td 49.691358 Tz (5.6 ) Tj 1.166667 0 Td 61.574074 Tz (g ) Tj 0.661111 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 46.450617 Tz (acetic ) Tj 1.963889 0 Td 54.372428 Tz (anhydride ) Tj 3.208333 0 Td 61.574074 Tz (was ) Tj 1.4 0 Td 48.148148 Tz (diluted ) Tj 2.313889 0 Td 59.953704 Tz (by ) Tj 0.991667 0 Td 55.632716 Tz (adding ) Tj 2.313889 0 Td 55.092593 Tz (5 ) Tj 0.661111 0 Td 82.638889 Tz (mL ) Tj 1.263889 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 1709.540741 Tm 25.297222 0 Td 56.17284 Tz (methylene ) Tj 3.208333 0 Td 49.826389 Tz (chloride ) Tj 2.547222 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 51.041667 Tz (then ) Tj 1.419444 0 Td 58.333333 Tz (added ) Tj 1.925 0 Td 45.37037 Tz (to ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 47.395833 Tz (reaction ) Tj 2.488889 0 Td 46.018519 Tz (flask ) Tj 1.555556 0 Td 65.895062 Tz (dur ) Tj 51.428571 0 0 51.428571 0 1668.307305 Tm 25.297222 0 Td 50.771605 Tz (ing ) Tj 1.127778 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 54.282407 Tz (time ) Tj 1.477778 0 Td 52.391975 Tz (period ) Tj 2.061111 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 61.574074 Tz (30 ) Tj 0.991667 0 Td 53.240741 Tz (minutes ) Tj 2.45 0 Td 53.796296 Tz (while ) Tj 1.808333 0 Td 56.388889 Tz (under ) Tj 1.827778 0 Td 58.333333 Tz (an ) Tj 0.875 0 Td 55.092593 Tz (argon ) Tj 1.866667 0 Td 70.486111 Tz (atmo ) Tj 52.857143 0 0 52.857143 0 1624.105263 Tm 24.632432 0 Td 47.297297 Tz (sphere. ) Tj 2.289189 0 Td 49.81982 Tz (Next, ) Tj 1.778378 0 Td 48.348348 Tz (the ) Tj 1.191892 0 Td 51.801802 Tz (mixture ) Tj 2.421622 0 Td 60.960961 Tz (was ) Tj 1.381081 0 Td 42.342342 Tz (stirred ) Tj 2.081081 0 Td 46.246246 Tz (for ) Tj 1.059459 0 Td 56.756757 Tz (an ) Tj 0.945946 0 Td 47.297297 Tz (additional ) Tj 3.159459 0 Td 52.027027 Tz (15 ) Tj 51.428571 0 0 51.428571 0 1587.07619 Tm 25.297222 0 Td 56.17284 Tz (minute ) Tj 2.197222 0 Td 51.311728 Tz (period ) Tj 2.041667 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 48.611111 Tz (time. ) Tj 1.672222 0 Td 74.537037 Tz (5g ) Tj 1.05 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 55.233494 Tz (1-bromo-3-phenylpropane ) Tj 7.797222 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 1541.512195 Tm 25.297222 0 Td 48.148148 Tz (diluted ) Tj 2.158333 0 Td 46.180556 Tz (into ) Tj 1.263889 0 Td 55.092593 Tz (5 ) Tj 0.505556 0 Td 82.638889 Tz (mL ) Tj 1.088889 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 55.812757 Tz (methylene ) Tj 3.15 0 Td 49.421296 Tz (chloride ) Tj 2.508333 0 Td 58.333333 Tz (and ) Tj 1.186111 0 Td 50.231481 Tz (then ) Tj 1.380556 0 Td 57.685185 Tz (added ) Tj 1.886111 0 Td 43.75 Tz (to ) Tj 0.661111 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1500.864734 Tm 25.297222 0 Td 48.611111 Tz (reaction ) Tj 2.527778 0 Td 52.777778 Tz (mixture ) Tj 2.372222 0 Td 52.391975 Tz (during ) Tj 2.002778 0 Td 55.092593 Tz (a ) Tj 0.466667 0 Td 61.574074 Tz (30 ) Tj 0.875 0 Td 51.851852 Tz (period ) Tj 1.983333 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 54.282407 Tz (time ) Tj 1.438889 0 Td 53.796296 Tz (while ) Tj 1.75 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 53.240741 Tz (mixture ) Tj 51.428571 0 0 51.428571 0 1461.212048 Tm 25.277778 0 Td 62.654321 Tz (was ) Tj 1.302778 0 Td 56.388889 Tz (under ) Tj 1.788889 0 Td 58.333333 Tz (an ) Tj 0.875 0 Td 54.444444 Tz (argon ) Tj 1.788889 0 Td 53.324916 Tz (atmosphere. ) Tj 3.733333 0 Td 55.740741 Tz (Subsequent ) Tj 3.5 0 Td 43.75 Tz (to ) Tj 0.719444 0 Td 42.939815 Tz (this ) Tj 1.186111 0 Td 47.530864 Tz (addition, ) Tj 40 0 0 40 0 1423 Tm 32.5 0 Td 65.277778 Tz (the ) Tj 1.4 0 Td 68.452381 Tz (mixture ) Tj 3.05 0 Td 80.555556 Tz (was ) Tj 1.65 0 Td 57.142857 Tz (stirred ) Tj 2.575 0 Td 62.5 Tz (for ) Tj 1.25 0 Td 75 Tz (an ) Tj 1.075 0 Td 62.5 Tz (additional ) Tj 3.925 0 Td 79.166667 Tz (2 ) Tj 0.7 0 Td 68.333333 Tz (hours ) Tj 2.3 0 Td 68.333333 Tz (while ) Tj 2.225 0 Td 46.666667 Tz (still ) Tj 1.625 0 Td 60.416667 Tz (in ) Tj 51.428571 0 0 51.428571 0 1376.197253 Tm 25.277778 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 47.530864 Tz (ice ) Tj 1.030556 0 Td 46.666667 Tz (bath. ) Tj 1.575 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 53.703704 Tz (mixture ) Tj 2.411111 0 Td 61.574074 Tz (was ) Tj 1.283333 0 Td 51.851852 Tz (then ) Tj 1.458333 0 Td 52.391975 Tz (slowly ) Tj 2.061111 0 Td 56.17284 Tz (poured ) Tj 2.177778 0 Td 53.472222 Tz (onto ) Tj 1.497222 0 Td 60.493827 Tz (200 ) Tj 1.225 0 Td 61.574074 Tz (g ) Tj 51.428571 0 0 51.428571 0 1334.106952 Tm 25.297222 0 Td 58.333333 Tz (of ) Tj 0.913889 0 Td 54.62963 Tz (crushed ) Tj 2.625 0 Td 42.12963 Tz (ice, ) Tj 1.341667 0 Td 49.691358 Tz (the ) Tj 1.205556 0 Td 51.388889 Tz (organic ) Tj 2.488889 0 Td 55.740741 Tz (phase ) Tj 1.983333 0 Td 61.574074 Tz (was ) Tj 1.458333 0 Td 60.493827 Tz (washed ) Tj 2.488889 0 Td 53.472222 Tz (with ) Tj 1.711111 0 Td 69.135802 Tz (10% ) Tj 52.857143 0 0 52.857143 0 1291.905237 Tm 24.594595 0 Td 50.187688 Tz (hydrochloric ) Tj 3.878378 0 Td 48.873874 Tz (acid ) Tj 1.418919 0 Td 57.282282 Tz (\(2x100 ) Tj 2.289189 0 Td 57.545045 Tz (mL\). ) Tj 1.664865 0 Td 69.369369 Tz (NaHCO, ) Tj 2.837838 0 Td 56.231231 Tz (\(2x100 ) Tj 2.27027 0 Td 56.756757 Tz (mL\), ) Tj 1.608108 0 Td 58.858859 Tz (and ) Tj 51.428571 0 0 51.428571 0 1249 Tm 25.316667 0 Td 58.333333 Tz (sodium ) Tj 2.313889 0 Td 50.231481 Tz (chloride ) Tj 2.644444 0 Td 62.222222 Tz (2x100 ) Tj 2.080556 0 Td 59.143519 Tz (mL\), ) Tj 1.633333 0 Td 46.990741 Tz (in ) Tj 0.797222 0 Td 45.37037 Tz (that ) Tj 1.283333 0 Td 46.450617 Tz (order. ) Tj 1.886111 0 Td 64.814815 Tz (The ) Tj 1.380556 0 Td 50 Tz (solvent ) Tj 2.313889 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 1209.186972 Tm 25.277778 0 Td 52.662037 Tz (then ) Tj 1.4 0 Td 60.185185 Tz (removed ) Tj 2.663889 0 Td 55.740741 Tz (under ) Tj 1.769444 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 61.574074 Tz (vacuum ) Tj 2.391667 0 Td 43.75 Tz (in ) Tj 0.680556 0 Td 51.851852 Tz (order ) Tj 1.652778 0 Td 46.990741 Tz (to ) Tj 0.7 0 Td 52.314815 Tz (recover ) Tj 2.294444 0 Td 49.691358 Tz (the ) Tj 1.011111 0 Td 49.826389 Tz (product. ) Tj 51.428571 0 0 51.428571 0 1134.046358 Tm 32.472222 0 Td 61.574074 Tz (Example ) Tj 2.761111 0 Td 58.333333 Tz (2 ) Tj 51.428571 0 0 51.428571 0 1049.608696 Tm 31.966667 0 Td 50.378788 Tz (Preparation ) Tj 3.519444 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 1010 Tm 27.397222 0 Td 55.173611 Tz (p-\(3-bromopropyl-a-Methylbenzenemethanol ) Tj 51.428571 0 0 51.428571 0 920.708333 Tm 26.016667 0 Td 63.734568 Tz (The ) Tj 1.283333 0 Td 53.240741 Tz (product ) Tj 2.430556 0 Td 46.450617 Tz (retrieved ) Tj 2.683333 0 Td 57.523148 Tz (from ) Tj 1.594444 0 Td 60.185185 Tz (Example ) Tj 2.741667 0 Td 38.888889 Tz (1 ) Tj 0.466667 0 Td 38.888889 Tz (is ) Tj 0.641667 0 Td 55.902778 Tz (used ) Tj 1.477778 0 Td 50.231481 Tz (as ) Tj 0.738889 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 44.965278 Tz (starting ) Tj 51.428571 0 0 51.428571 0 879.353393 Tm 25.297222 0 Td 49.421296 Tz (material ) Tj 2.644444 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 42.12963 Tz (this ) Tj 1.283333 0 Td 48.341049 Tz (preparation. ) Tj 3.733333 0 Td 56.712963 Tz (That ) Tj 1.594444 0 Td 53.703704 Tz (product ) Tj 2.488889 0 Td 58.333333 Tz (from ) Tj 1.730556 0 Td 60.185185 Tz (Example ) Tj 2.838889 0 Td 38.888889 Tz (1 ) Tj 51.428571 0 0 51.428571 0 835.597531 Tm 25.277778 0 Td 62.654321 Tz (was ) Tj 1.341667 0 Td 47.685185 Tz (diluted ) Tj 2.177778 0 Td 46.180556 Tz (into ) Tj 1.302778 0 Td 61.574074 Tz (60 ) Tj 0.933333 0 Td 81.018519 Tz (mL ) Tj 1.147222 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 53.292181 Tz (methynol. ) Tj 3.052778 0 Td 59.62963 Tz (While ) Tj 1.963889 0 Td 45.37037 Tz (that ) Tj 1.244444 0 Td 53.240741 Tz (product ) Tj 2.411111 0 Td 61.574074 Tz (was ) Tj 40 0 0 40 0 800 Tm 32.525 0 Td 58.333333 Tz (in ) Tj 0.9 0 Td 75 Tz (a ) Tj 0.65 0 Td 62.5 Tz (reaction ) Tj 3.25 0 Td 58.333333 Tz (flask ) Tj 1.925 0 Td 60.416667 Tz (that ) Tj 1.65 0 Td 79.166667 Tz (was ) Tj 1.65 0 Td 73.611111 Tz (submersed ) Tj 4.225 0 Td 58.333333 Tz (in ) Tj 0.9 0 Td 72.916667 Tz (an ) Tj 1.15 0 Td 59.722222 Tz (ice ) Tj 1.275 0 Td 65.625 Tz (bath ) Tj 1.8 0 Td 76.388889 Tz (and ) Tj 1.575 0 Td 61.458333 Tz (also ) Tj 51.428571 0 0 51.428571 0 754.561661 Tm 25.277778 0 Td 57.685185 Tz (under ) Tj 1.866667 0 Td 54.444444 Tz (argon ) Tj 1.847222 0 Td 53.030303 Tz (atmosphere, ) Tj 3.752778 0 Td 51.041667 Tz (0.75 ) Tj 1.419444 0 Td 64.814815 Tz (g ) Tj 0.602778 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 58.333333 Tz (sodium ) Tj 2.333333 0 Td 53.914141 Tz (borohydride ) Tj 3.752778 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 712.763496 Tm 25.297222 0 Td 58.333333 Tz (added ) Tj 1.983333 0 Td 52.391975 Tz (during ) Tj 2.1 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 55.092593 Tz (5 ) Tj 0.622222 0 Td 55.092593 Tz (minute ) Tj 2.216667 0 Td 51.851852 Tz (period ) Tj 2.080556 0 Td 61.574074 Tz (of ) Tj 0.875 0 Td 47.962963 Tz (time. ) Tj 1.691667 0 Td 56.064815 Tz (Subsequent ) Tj 3.597222 0 Td 45.37037 Tz (to ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 48.571429 0 0 48.571429 0 669 Tm 26.785294 0 Td 50.326797 Tz (addition, ) Tj 2.985294 0 Td 52.614379 Tz (the ) Tj 1.255882 0 Td 56.372549 Tz (mixture ) Tj 2.635294 0 Td 65.196078 Tz (was ) Tj 1.461765 0 Td 47.058824 Tz (stirred ) Tj 2.264706 0 Td 50.326797 Tz (for ) Tj 1.152941 0 Td 60.04902 Tz (an ) Tj 1.008824 0 Td 51.127451 Tz (additional ) Tj 3.355882 0 Td 61.764706 Tz (2 ) Tj 0.638235 0 Td 57.647059 Tz (hours ) Tj 51.428571 0 0 51.428571 0 626.843137 Tm 25.277778 0 Td 54.444444 Tz (while ) Tj 1.769444 0 Td 35.648148 Tz (still ) Tj 1.186111 0 Td 55.092593 Tz (over ) Tj 1.419444 0 Td 55.092593 Tz (an ) Tj 0.816667 0 Td 47.530864 Tz (ice ) Tj 0.952778 0 Td 47.314815 Tz (bath. ) Tj 1.555556 0 Td 59.953704 Tz (At ) Tj 0.836111 0 Td 45.37037 Tz (that ) Tj 1.205556 0 Td 46.450617 Tz (point, ) Tj 1.886111 0 Td 56.17284 Tz (100 ) Tj 1.147222 0 Td 82.638889 Tz (mL ) Tj 1.108333 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 54.444444 Tz (water ) Tj 1.730556 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 586.397077 Tm 25.297222 0 Td 58.333333 Tz (added ) Tj 1.905556 0 Td 45.37037 Tz (to ) Tj 0.738889 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 53.240741 Tz (mixture ) Tj 2.391667 0 Td 59.41358 Tz (and ) Tj 1.205556 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 47.170782 Tz (resulting ) Tj 2.702778 0 Td 53.240741 Tz (product ) Tj 2.391667 0 Td 61.574074 Tz (was ) Tj 1.302778 0 Td 49.331276 Tz (extracted ) Tj 51.428571 0 0 51.428571 0 543.530864 Tm 25.277778 0 Td 54.282407 Tz (with ) Tj 1.555556 0 Td 55.812757 Tz (methylene ) Tj 3.227778 0 Td 46.8107 Tz (chloride. ) Tj 2.741667 0 Td 64.814815 Tz (The ) Tj 1.380556 0 Td 50.462963 Tz (solvent ) Tj 2.294444 0 Td 61.574074 Tz (was ) Tj 1.380556 0 Td 59.259259 Tz (removed ) Tj 2.702778 0 Td 56.388889 Tz (under ) Tj 1.886111 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 504.015015 Tm 25.297222 0 Td 62.654321 Tz (vacuum ) Tj 2.469444 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 52.5 Tz (order ) Tj 1.75 0 Td 43.75 Tz (to ) Tj 0.7 0 Td 52.5 Tz (allow ) Tj 1.847222 0 Td 51.446759 Tz (recovery ) Tj 2.663889 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 50.231481 Tz (product. ) Tj 51.428571 0 0 51.428571 0 427.093333 Tm 32.472222 0 Td 61.574074 Tz (Example ) Tj 2.761111 0 Td 55.092593 Tz (3 ) Tj 51.428571 0 0 51.428571 0 344.522388 Tm 28.038889 0 Td 50.084175 Tz (Preparation ) Tj 3.5 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 53.607253 Tz (p-\(3-Bromopropyl\)styrene ) Tj 51.428571 0 0 51.428571 0 254.531807 Tm 26.016667 0 Td 63.734568 Tz (The ) Tj 1.244444 0 Td 53.703704 Tz (product ) Tj 2.372222 0 Td 57.523148 Tz (from ) Tj 1.555556 0 Td 61.111111 Tz (Example ) Tj 2.683333 0 Td 58.333333 Tz (2 ) Tj 0.505556 0 Td 38.888889 Tz (is ) Tj 0.622222 0 Td 55.092593 Tz (used ) Tj 1.419444 0 Td 51.851852 Tz (as ) Tj 0.758333 0 Td 55.092593 Tz (a ) Tj 0.466667 0 Td 45.833333 Tz (stating ) Tj 2.080556 0 Td 48.611111 Tz (material ) Tj 2.469444 0 Td 48.611111 Tz (in ) Tj 51.428571 0 0 51.428571 0 215.383648 Tm 25.277778 0 Td 43.75 Tz (this ) Tj 1.302778 0 Td 51.203704 Tz (procedure. ) Tj 3.305556 0 Td 64.814815 Tz (The ) Tj 1.4 0 Td 47.170782 Tz (resulting ) Tj 2.780556 0 Td 53.240741 Tz (product ) Tj 2.469444 0 Td 58.333333 Tz (from ) Tj 1.711111 0 Td 60.648148 Tz (Example ) Tj 2.8 0 Td 55.092593 Tz (2 ) Tj 0.602778 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 168.194175 Tm 25.297222 0 Td 48.148148 Tz (diluted ) Tj 2.177778 0 Td 45.37037 Tz (in ) Tj 0.719444 0 Td 60.493827 Tz (200 ) Tj 1.263889 0 Td 81.018519 Tz (mL ) Tj 1.127778 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 47.800926 Tz (toluene. ) Tj 2.469444 0 Td 52.5 Tz (Next, ) Tj 1.730556 0 Td 53.796296 Tz (0.125 ) Tj 1.769444 0 Td 64.814815 Tz (g ) Tj 0.525 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 49.305556 Tz (toluensulfonic ) Tj ET Q endstream endobj 304 0 obj << /Length 1 >> stream q endstream endobj 305 0 obj << /Length 35114 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.325 0 Td 83.522727 Tz (US ) Tj 1.240909 0 Td 58.038721 Tz (7,829,155 ) Tj 3.388636 0 Td 68.939394 Tz (B1 ) Tj 51.428571 0 0 51.428571 0 2968 Tm 14.875 0 Td 77.777778 Tz (7 ) Tj 40 0 0 40 0 2921 Tm 8.175 0 Td 65.625 Tz (acid ) Tj 1.8 0 Td 76.388889 Tz (was ) Tj 1.6 0 Td 75 Tz (added ) Tj 2.45 0 Td 58.333333 Tz (to ) Tj 0.95 0 Td 62.5 Tz (the ) Tj 1.35 0 Td 61.979167 Tz (reaction ) Tj 3.225 0 Td 64.0625 Tz (mixture. ) Tj 3.275 0 Td 81.944444 Tz (The ) Tj 1.675 0 Td 62.5 Tz (reaction ) Tj 3.275 0 Td 68.452381 Tz (mixture ) Tj 51.428571 0 0 51.428571 0 2874.483755 Tm 6.338889 0 Td 62.654321 Tz (was ) Tj 1.302778 0 Td 49.826389 Tz (refluxed ) Tj 2.527778 0 Td 56.388889 Tz (under ) Tj 1.808333 0 Td 55.092593 Tz (argon ) Tj 1.827778 0 Td 56.064815 Tz (atmosphere ) Tj 3.5 0 Td 49.691358 Tz (for ) Tj 0.991667 0 Td 63.194444 Tz (44 ) Tj 0.894444 0 Td 49.691358 Tz (hours. ) Tj 1.963889 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 74.537037 Tz (mix ) Tj 40 0 0 40 0 2838 Tm 8.15 0 Td 62.5 Tz (ture ) Tj 1.65 0 Td 77.777778 Tz (was ) Tj 1.575 0 Td 75.833333 Tz (thenwashed ) Tj 4.725 0 Td 66.666667 Tz (with ) Tj 1.775 0 Td 79.166667 Tz (50 ) Tj 1.125 0 Td 104.166667 Tz (mL ) Tj 1.425 0 Td 68.75 Tz (of ) Tj 0.925 0 Td 70 Tz (water ) Tj 2.2 0 Td 76.388889 Tz (and ) Tj 1.5 0 Td 65.277778 Tz (the ) Tj 1.325 0 Td 63.690476 Tz (solvent ) Tj 2.825 0 Td 79.166667 Tz (was ) Tj 51.428571 0 0 51.428571 0 2791.045346 Tm 6.358333 0 Td 60.185185 Tz (removed ) Tj 2.683333 0 Td 55.740741 Tz (under ) Tj 1.827778 0 Td 56.944444 Tz (vacuum. ) Tj 2.527778 0 Td 64.814815 Tz (The ) Tj 1.302778 0 Td 47.530864 Tz (resulting ) Tj 2.683333 0 Td 53.240741 Tz (product ) Tj 2.391667 0 Td 60.493827 Tz (was ) Tj 1.225 0 Td 51.851852 Tz (then ) Tj 1.419444 0 Td 58.333333 Tz (puri ) Tj 51.428571 0 0 51.428571 0 2750.155875 Tm 6.358333 0 Td 46.180556 Tz (fied ) Tj 1.205556 0 Td 61.574074 Tz (by ) Tj 0.894444 0 Td 42.12963 Tz (silica ) Tj 1.633333 0 Td 49.691358 Tz (gel ) Tj 1.030556 0 Td 56.712963 Tz (chromatography ) Tj 4.919444 0 Td 52.662037 Tz (with ) Tj 1.380556 0 Td 51.851852 Tz (the ) Tj 1.05 0 Td 54.012346 Tz (use ) Tj 1.108333 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 71.296296 Tz (90% ) Tj 1.438889 0 Td 57.253086 Tz (hexane ) Tj 51.428571 0 0 51.428571 0 2708.148831 Tm 6.358333 0 Td 58.333333 Tz (and ) Tj 1.322222 0 Td 69.135802 Tz (10% ) Tj 1.458333 0 Td 47.962963 Tz (ethyl ) Tj 1.633333 0 Td 45.37037 Tz (acetate. ) Tj 2.372222 0 Td 64.814815 Tz (The ) Tj 1.380556 0 Td 47.170782 Tz (resulting ) Tj 2.702778 0 Td 53.240741 Tz (product ) Tj 2.45 0 Td 60.493827 Tz (was ) Tj 1.322222 0 Td 52.932099 Tz (recovered ) Tj 40 0 0 40 0 2672 Tm 8.175 0 Td 64.583333 Tz (as ) Tj 1 0 Td 65.277778 Tz (the ) Tj 1.425 0 Td 63.690476 Tz (solvent ) Tj 2.9 0 Td 79.166667 Tz (was ) Tj 1.675 0 Td 77.380952 Tz (removed ) Tj 3.5 0 Td 71.666667 Tz (under ) Tj 2.375 0 Td 73.809524 Tz (vacuum. ) Tj 51.428571 0 0 51.428571 0 2590.04 Tm 13.552778 0 Td 61.111111 Tz (Example ) Tj 2.741667 0 Td 58.333333 Tz (4 ) Tj 51.428571 0 0 51.428571 0 2507.532385 Tm 8.808333 0 Td 50.378788 Tz (Preparation ) Tj 3.519444 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 52.973647 Tz (4-Vinylbenzenepropanethiol ) Tj 51.428571 0 0 51.428571 0 2417.764706 Tm 7.097222 0 Td 62.654321 Tz (The ) Tj 1.225 0 Td 53.703704 Tz (product ) Tj 2.391667 0 Td 46.8107 Tz (resulting ) Tj 2.644444 0 Td 58.333333 Tz (from ) Tj 1.575 0 Td 60.185185 Tz (Example ) Tj 2.663889 0 Td 55.092593 Tz (3 ) Tj 0.505556 0 Td 62.654321 Tz (was ) Tj 1.244444 0 Td 48.148148 Tz (diluted ) Tj 2.138889 0 Td 46.180556 Tz (into ) Tj 1.244444 0 Td 61.574074 Tz (200 ) Tj 51.428571 0 0 51.428571 0 2375.191633 Tm 6.358333 0 Td 85.87963 Tz (mL ) Tj 1.322222 0 Td 59.953704 Tz (of ) Tj 0.952778 0 Td 53.652263 Tz (methynol, ) Tj 3.208333 0 Td 51.041667 Tz (then ) Tj 1.575 0 Td 87.5 Tz (5g ) Tj 1.361111 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 49.016204 Tz (thiourea ) Tj 2.702778 0 Td 60.493827 Tz (was ) Tj 1.419444 0 Td 58.333333 Tz (added ) Tj 2.080556 0 Td 43.75 Tz (to ) Tj 0.855556 0 Td 43.75 Tz (this ) Tj 51.428571 0 0 51.428571 0 2331.986877 Tm 6.377778 0 Td 47.800926 Tz (solution ) Tj 2.605556 0 Td 58.981481 Tz (which ) Tj 2.061111 0 Td 61.574074 Tz (was ) Tj 1.380556 0 Td 54.62963 Tz (allowed ) Tj 2.586111 0 Td 43.75 Tz (to ) Tj 0.797222 0 Td 50.771605 Tz (gently ) Tj 2.158333 0 Td 46.450617 Tz (reflux ) Tj 1.944444 0 Td 48.611111 Tz (for ) Tj 1.166667 0 Td 55.092593 Tz (16 ) Tj 0.933333 0 Td 49.691358 Tz (hours. ) Tj 51.428571 0 0 51.428571 0 2291.503686 Tm 6.358333 0 Td 48.021886 Tz (Thereafter, ) Tj 3.422222 0 Td 55.092593 Tz (15 ) Tj 0.875 0 Td 82.638889 Tz (mL ) Tj 1.166667 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 70.216049 Tz (12% ) Tj 1.477778 0 Td 58.333333 Tz (sodium ) Tj 2.275 0 Td 55.092593 Tz (hydroxide ) Tj 3.169444 0 Td 60.493827 Tz (was ) Tj 1.263889 0 Td 58.981481 Tz (added ) Tj 1.905556 0 Td 61.574074 Tz (and ) Tj 48.571429 0 0 48.571429 0 2250 Tm 6.711765 0 Td 53.75817 Tz (the ) Tj 1.152941 0 Td 56.372549 Tz (mixture ) Tj 2.511765 0 Td 65.196078 Tz (was ) Tj 1.317647 0 Td 58.333333 Tz (allowed ) Tj 2.614706 0 Td 46.323529 Tz (to ) Tj 0.720588 0 Td 50.326797 Tz (reflux ) Tj 1.955882 0 Td 51.470588 Tz (for ) Tj 1.029412 0 Td 65.196078 Tz (4 ) Tj 0.555882 0 Td 52.042484 Tz (hours. ) Tj 2.038235 0 Td 55.588235 Tz (Next, ) Tj 1.811765 0 Td 66.911765 Tz (20 ) Tj 0.967647 0 Td 87.5 Tz (mL ) Tj 1.214706 0 Td 60.04902 Tz (of ) Tj 51.428571 0 0 51.428571 0 2207.56 Tm 6.358333 0 Td 56.17284 Tz (methylene ) Tj 3.247222 0 Td 50.231481 Tz (chloride ) Tj 2.663889 0 Td 60.493827 Tz (was ) Tj 1.322222 0 Td 58.981481 Tz (added ) Tj 2.002778 0 Td 58.333333 Tz (and ) Tj 1.341667 0 Td 58.333333 Tz (10 ) Tj 0.933333 0 Td 56.712963 Tz (normal ) Tj 2.294444 0 Td 45.775463 Tz (sulfuric ) Tj 2.430556 0 Td 52.662037 Tz (acid ) Tj 51.428571 0 0 51.428571 0 2168.02091 Tm 6.338889 0 Td 62.654321 Tz (was ) Tj 1.322222 0 Td 58.333333 Tz (added ) Tj 1.925 0 Td 55.497685 Tz (dropwise ) Tj 2.838889 0 Td 44.074074 Tz (until ) Tj 1.536111 0 Td 48.611111 Tz (the ) Tj 1.030556 0 Td 76.157407 Tz (pH ) Tj 1.088889 0 Td 56.944444 Tz (dropped ) Tj 2.566667 0 Td 45.37037 Tz (to ) Tj 0.738889 0 Td 44.560185 Tz (9.5. ) Tj 1.263889 0 Td 47.727273 Tz (Thereafter, ) Tj 51.428571 0 0 51.428571 0 2124.198966 Tm 6.436111 0 Td 58.333333 Tz (100 ) Tj 1.263889 0 Td 82.638889 Tz (mL ) Tj 1.186111 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 54.444444 Tz (water ) Tj 1.847222 0 Td 60.493827 Tz (was ) Tj 1.302778 0 Td 58.981481 Tz (added ) Tj 2.002778 0 Td 43.75 Tz (to ) Tj 0.777778 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 52.777778 Tz (mixture ) Tj 2.430556 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 48.611111 Tz (the ) Tj 1.088889 0 Td 53.703704 Tz (product ) Tj 51.428571 0 0 51.428571 0 2084.783055 Tm 6.338889 0 Td 62.654321 Tz (was ) Tj 1.477778 0 Td 49.331276 Tz (extracted ) Tj 3.013889 0 Td 52.662037 Tz (with ) Tj 1.613889 0 Td 56.17284 Tz (methylene ) Tj 3.325 0 Td 47.530864 Tz (chloride. ) Tj 2.897222 0 Td 63.734568 Tz (The ) Tj 1.477778 0 Td 53.240741 Tz (product ) Tj 2.566667 0 Td 61.574074 Tz (was ) Tj 40 0 0 40 0 2048 Tm 8.175 0 Td 68.055556 Tz (recovered ) Tj 3.875 0 Td 64.583333 Tz (as ) Tj 1 0 Td 65.277778 Tz (the ) Tj 1.4 0 Td 64.880952 Tz (solvent ) Tj 2.95 0 Td 79.166667 Tz (was ) Tj 1.7 0 Td 76.785714 Tz (removed ) Tj 3.45 0 Td 71.666667 Tz (under ) Tj 2.375 0 Td 74.404762 Tz (vacuum. ) Tj 51.428571 0 0 51.428571 0 1966.135135 Tm 13.552778 0 Td 61.111111 Tz (Example ) Tj 2.761111 0 Td 51.851852 Tz (5 ) Tj 51.428571 0 0 51.428571 0 1882.292887 Tm 7.894444 0 Td 63.194444 Tz (Method ) Tj 2.45 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 56.30787 Tz (Applying ) Tj 2.897222 0 Td 52.973647 Tz (4-Vinylbenzenepropanethiol ) Tj 51.428571 0 0 51.428571 0 1838.888889 Tm 12.308333 0 Td 59.41358 Tz (Monolayer ) Tj 3.383333 0 Td 45.37037 Tz (to ) Tj 0.719444 0 Td 62.384259 Tz (Gold ) Tj 51.428571 0 0 51.428571 0 1749.722444 Tm 7.097222 0 Td 87.5 Tz (A ) Tj 0.680556 0 Td 55.092593 Tz (gold ) Tj 1.497222 0 Td 51.851852 Tz (coated ) Tj 2.080556 0 Td 44.907407 Tz (silicon ) Tj 2.119444 0 Td 47.890947 Tz (Substrate ) Tj 2.761111 0 Td 61.574074 Tz (was ) Tj 1.302778 0 Td 57.613169 Tz (Submersed ) Tj 3.305556 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 32.407407 Tz (1 ) Tj 0.505556 0 Td 98.842593 Tz (mM ) Tj 51.428571 0 0 51.428571 0 1713.566434 Tm 6.377778 0 Td 48.206019 Tz (Solution ) Tj 2.488889 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 52.10114 Tz (4-vinylbenzenepropanethiol ) Tj 8.322222 0 Td 43.75 Tz (at ) Tj 0.680556 0 Td 64.00463 Tz (room ) Tj 1.711111 0 Td 52.73569 Tz (temperature ) Tj 40 0 0 40 0 1674 Tm 8.175 0 Td 62.5 Tz (for ) Tj 1.525 0 Td 75 Tz (two ) Tj 1.75 0 Td 63.888889 Tz (hours. ) Tj 2.7 0 Td 81.944444 Tz (The ) Tj 1.9 0 Td 61.111111 Tz (substrate ) Tj 3.725 0 Td 77.777778 Tz (was ) Tj 1.825 0 Td 66.666667 Tz (then ) Tj 2.05 0 Td 76.785714 Tz (removed ) Tj 3.625 0 Td 73.958333 Tz (from ) Tj 2.225 0 Td 63.888889 Tz (the ) Tj 52.857143 0 0 52.857143 0 1625.320388 Tm 6.205405 0 Td 46.509009 Tz (solution ) Tj 2.440541 0 Td 56.756757 Tz (and ) Tj 1.22973 0 Td 56.056056 Tz (submersed ) Tj 3.216216 0 Td 44.932432 Tz (into ) Tj 1.267568 0 Td 56.756757 Tz (a ) Tj 0.52973 0 Td 48.085586 Tz (separate ) Tj 2.497297 0 Td 49.399399 Tz (container ) Tj 2.8 0 Td 58.333333 Tz (of ) Tj 0.775676 0 Td 52.702703 Tz (tetrahy ) Tj 40 0 0 40 0 1590 Tm 8.175 0 Td 66.145833 Tz (drofuran ) Tj 3.4 0 Td 62.5 Tz (for ) Tj 1.35 0 Td 72.916667 Tz (10 ) Tj 1.025 0 Td 66.145833 Tz (seconds. ) Tj 3.375 0 Td 80.555556 Tz (The ) Tj 1.65 0 Td 61.111111 Tz (substrate ) Tj 3.5 0 Td 77.777778 Tz (was ) Tj 1.625 0 Td 76.785714 Tz (removed ) Tj 3.425 0 Td 72.916667 Tz (from ) Tj 1.975 0 Td 63.888889 Tz (the ) Tj 51.428571 0 0 51.428571 0 1542.249697 Tm 6.338889 0 Td 50.123457 Tz (tetrahydrofuran ) Tj 4.705556 0 Td 48.206019 Tz (solution ) Tj 2.488889 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 60.493827 Tz (was ) Tj 1.283333 0 Td 50.231481 Tz (then ) Tj 1.419444 0 Td 48.611111 Tz (rinsed ) Tj 1.905556 0 Td 52.662037 Tz (with ) Tj 1.458333 0 Td 47.530864 Tz (water. ) Tj 1.866667 0 Td 63.734568 Tz (The ) Tj 51.428571 0 0 51.428571 0 1502.327434 Tm 6.377778 0 Td 47.530864 Tz (Substrate ) Tj 2.761111 0 Td 61.574074 Tz (was ) Tj 1.302778 0 Td 54.79798 Tz (immediately ) Tj 3.791667 0 Td 60.277778 Tz (blown ) Tj 2.002778 0 Td 52.932099 Tz (dry ) Tj 1.147222 0 Td 46.990741 Tz (in ) Tj 0.738889 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 52.932099 Tz (stream ) Tj 2.119444 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 50.771605 Tz (argon. ) Tj 51.428571 0 0 51.428571 0 1425.087248 Tm 13.552778 0 Td 61.111111 Tz (Example ) Tj 2.761111 0 Td 55.092593 Tz (6 ) Tj 51.428571 0 0 51.428571 0 1340.292887 Tm 7.894444 0 Td 63.194444 Tz (Method ) Tj 2.45 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 56.30787 Tz (Applying ) Tj 2.897222 0 Td 52.973647 Tz (4-Vinylbenzenepropanethiol ) Tj 51.428571 0 0 51.428571 0 1297.793893 Tm 12.366667 0 Td 56.532922 Tz (Oligomers ) Tj 3.247222 0 Td 46.990741 Tz (to ) Tj 0.758333 0 Td 61.574074 Tz (Gold ) Tj 51.428571 0 0 51.428571 0 1208.722444 Tm 7.097222 0 Td 87.5 Tz (A ) Tj 0.680556 0 Td 55.092593 Tz (gold ) Tj 1.497222 0 Td 51.851852 Tz (coated ) Tj 2.080556 0 Td 44.907407 Tz (silicon ) Tj 2.119444 0 Td 47.890947 Tz (Substrate ) Tj 2.761111 0 Td 61.574074 Tz (was ) Tj 1.302778 0 Td 57.613169 Tz (Submersed ) Tj 3.305556 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 32.407407 Tz (1 ) Tj 0.505556 0 Td 98.842593 Tz (mM ) Tj 51.428571 0 0 51.428571 0 1172.16771 Tm 6.377778 0 Td 48.206019 Tz (Solution ) Tj 2.819444 0 Td 58.333333 Tz (of ) Tj 1.108333 0 Td 53.472222 Tz (oligomerized ) Tj 4.336111 0 Td 52.10114 Tz (4-vinylbenzenepropanethiol ) Tj 8.652778 0 Td 45.37037 Tz (at ) Tj 51.428571 0 0 51.428571 0 1125.881735 Tm 6.358333 0 Td 63.194444 Tz (room ) Tj 1.866667 0 Td 52.73569 Tz (temperature ) Tj 3.830556 0 Td 48.611111 Tz (for ) Tj 1.166667 0 Td 58.333333 Tz (two ) Tj 1.4 0 Td 49.151235 Tz (hours. ) Tj 2.1 0 Td 63.734568 Tz (The ) Tj 1.477778 0 Td 47.890947 Tz (substrate ) Tj 2.936111 0 Td 60.493827 Tz (was ) Tj 1.438889 0 Td 53.472222 Tz (then ) Tj 51.428571 0 0 51.428571 0 1084.263158 Tm 6.358333 0 Td 60.185185 Tz (removed ) Tj 2.819444 0 Td 57.523148 Tz (from ) Tj 1.691667 0 Td 49.691358 Tz (the ) Tj 1.186111 0 Td 48.206019 Tz (Solution ) Tj 2.605556 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 57.613169 Tz (Submersed ) Tj 3.383333 0 Td 46.990741 Tz (into ) Tj 1.419444 0 Td 55.092593 Tz (a ) Tj 0.622222 0 Td 49.826389 Tz (separate ) Tj 51.428571 0 0 51.428571 0 1043.284302 Tm 6.358333 0 Td 50.771605 Tz (container ) Tj 2.955556 0 Td 61.574074 Tz (of ) Tj 0.913889 0 Td 49.907407 Tz (tetrahydrofuran ) Tj 4.763889 0 Td 48.611111 Tz (for ) Tj 1.166667 0 Td 58.333333 Tz (10 ) Tj 0.952778 0 Td 51.041667 Tz (seconds. ) Tj 2.722222 0 Td 63.734568 Tz (The ) Tj 1.419444 0 Td 47.890947 Tz (substrate ) Tj 51.428571 0 0 51.428571 0 1002.226506 Tm 6.338889 0 Td 62.654321 Tz (was ) Tj 1.341667 0 Td 59.259259 Tz (removed ) Tj 2.644444 0 Td 57.523148 Tz (from ) Tj 1.575 0 Td 48.611111 Tz (the ) Tj 1.030556 0 Td 49.907407 Tz (tetrahydrofuran ) Tj 4.686111 0 Td 48.206019 Tz (solution ) Tj 2.45 0 Td 59.41358 Tz (and ) Tj 1.225 0 Td 61.574074 Tz (was ) Tj 1.283333 0 Td 53.472222 Tz (then ) Tj 51.428571 0 0 51.428571 0 960.294046 Tm 6.358333 0 Td 49.691358 Tz (rinsed ) Tj 1.963889 0 Td 53.472222 Tz (with ) Tj 1.458333 0 Td 48.070988 Tz (water. ) Tj 1.905556 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 47.530864 Tz (substrate ) Tj 2.741667 0 Td 60.493827 Tz (was ) Tj 1.302778 0 Td 54.79798 Tz (immediately ) Tj 3.791667 0 Td 60.277778 Tz (blown ) Tj 2.002778 0 Td 54.012346 Tz (dry ) Tj 51.428571 0 0 51.428571 0 919.754579 Tm 6.358333 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 52.932099 Tz (stream ) Tj 2.119444 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 50.771605 Tz (argon. ) Tj 51.428571 0 0 51.428571 0 843.04 Tm 13.552778 0 Td 61.111111 Tz (Example ) Tj 2.741667 0 Td 58.333333 Tz (7 ) Tj 51.428571 0 0 51.428571 0 758.067114 Tm 7.525 0 Td 63.194444 Tz (Method ) Tj 2.45 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 56.712963 Tz (Applying ) Tj 2.916667 0 Td 52.973647 Tz (4-Vinylbenzenepropanethiol ) Tj 8.458333 0 Td 45.37037 Tz (to ) Tj 40 0 0 40 0 719 Tm 13.4 0 Td 78.125 Tz (Gold ) Tj 2.1 0 Td 68.75 Tz (with ) Tj 1.9 0 Td 66.666667 Tz (Controlled ) Tj 4.225 0 Td 69.907407 Tz (Thickness ) Tj 51.428571 0 0 51.428571 0 626.722444 Tm 7.097222 0 Td 87.5 Tz (A ) Tj 0.680556 0 Td 55.092593 Tz (gold ) Tj 1.497222 0 Td 51.851852 Tz (coated ) Tj 2.080556 0 Td 44.907407 Tz (silicon ) Tj 2.119444 0 Td 47.890947 Tz (Substrate ) Tj 2.761111 0 Td 61.574074 Tz (was ) Tj 1.302778 0 Td 57.613169 Tz (Submersed ) Tj 3.305556 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 32.407407 Tz (1 ) Tj 0.505556 0 Td 98.842593 Tz (mM ) Tj 51.428571 0 0 51.428571 0 589.566434 Tm 6.377778 0 Td 48.206019 Tz (Solution ) Tj 2.488889 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 52.10114 Tz (4-vinylbenzenepropanethiol ) Tj 8.322222 0 Td 43.75 Tz (at ) Tj 0.680556 0 Td 64.00463 Tz (room ) Tj 1.711111 0 Td 52.73569 Tz (temperature ) Tj 51.428571 0 0 51.428571 0 543.144266 Tm 6.358333 0 Td 49.691358 Tz (for ) Tj 1.05 0 Td 59.41358 Tz (one ) Tj 1.244444 0 Td 48.611111 Tz (hour. ) Tj 1.652778 0 Td 64.814815 Tz (The ) Tj 1.361111 0 Td 50.411523 Tz (container ) Tj 2.877778 0 Td 53.703704 Tz (holding ) Tj 2.469444 0 Td 48.611111 Tz (the ) Tj 1.088889 0 Td 48.251029 Tz (substrate ) Tj 2.780556 0 Td 50.771605 Tz (within ) Tj 2.061111 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 505.328834 Tm 6.377778 0 Td 48.206019 Tz (Solution ) Tj 2.547222 0 Td 61.574074 Tz (was ) Tj 1.322222 0 Td 53.472222 Tz (placed ) Tj 2.138889 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 58.333333 Tz (a ) Tj 0.622222 0 Td 56.481481 Tz (Rayonet ) Tj 2.605556 0 Td 44.781145 Tz (ultraviolet ) Tj 3.169444 0 Td 54.843305 Tz (photochemical ) Tj 51.428571 0 0 51.428571 0 461.308261 Tm 6.358333 0 Td 50.462963 Tz (cabinet ) Tj 2.255556 0 Td 55.902778 Tz (equipped ) Tj 2.858333 0 Td 52.662037 Tz (with ) Tj 1.458333 0 Td 51.041667 Tz (two, ) Tj 1.4 0 Td 59.953704 Tz (35 ) Tj 0.913889 0 Td 46.666667 Tz (watt, ) Tj 1.575 0 Td 54.444444 Tz (253.7 ) Tj 1.808333 0 Td 74.537037 Tz (nm ) Tj 1.088889 0 Td 51.851852 Tz (lamps. ) Tj 2.041667 0 Td 64.814815 Tz (The ) Tj 1.302778 0 Td 44.290123 Tz (lid ) Tj 51.428571 0 0 51.428571 0 418.905852 Tm 6.338889 0 Td 62.654321 Tz (was ) Tj 1.458333 0 Td 59.259259 Tz (removed ) Tj 2.741667 0 Td 58.333333 Tz (from ) Tj 1.711111 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 50.411523 Tz (container ) Tj 2.975 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 45.075758 Tz (ultraviolet ) Tj 3.227778 0 Td 57.685185 Tz (lamps ) Tj 40 0 0 40 0 384 Tm 8.15 0 Td 77.083333 Tz (were ) Tj 2.325 0 Td 66.666667 Tz (turned ) Tj 2.875 0 Td 75 Tz (on ) Tj 1.425 0 Td 61.111111 Tz (for ) Tj 1.525 0 Td 81.25 Tz (30 ) Tj 1.45 0 Td 65.104167 Tz (minutes. ) Tj 3.625 0 Td 79.166667 Tz (The ) Tj 1.925 0 Td 61.574074 Tz (substrate ) Tj 3.8 0 Td 79.166667 Tz (was ) Tj 1.95 0 Td 67.708333 Tz (then ) Tj 51.428571 0 0 51.428571 0 336.263158 Tm 6.358333 0 Td 60.185185 Tz (removed ) Tj 2.819444 0 Td 57.523148 Tz (from ) Tj 1.691667 0 Td 49.691358 Tz (the ) Tj 1.186111 0 Td 48.206019 Tz (Solution ) Tj 2.605556 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 57.613169 Tz (Submersed ) Tj 3.383333 0 Td 46.990741 Tz (into ) Tj 1.419444 0 Td 55.092593 Tz (a ) Tj 0.622222 0 Td 49.826389 Tz (separate ) Tj 51.428571 0 0 51.428571 0 295.284302 Tm 6.358333 0 Td 50.771605 Tz (container ) Tj 2.955556 0 Td 61.574074 Tz (of ) Tj 0.913889 0 Td 49.907407 Tz (tetrahydrofuran ) Tj 4.763889 0 Td 48.611111 Tz (for ) Tj 1.166667 0 Td 58.333333 Tz (10 ) Tj 0.952778 0 Td 51.041667 Tz (seconds. ) Tj 2.722222 0 Td 63.734568 Tz (The ) Tj 1.419444 0 Td 47.890947 Tz (substrate ) Tj 51.428571 0 0 51.428571 0 253.226506 Tm 6.338889 0 Td 62.654321 Tz (was ) Tj 1.341667 0 Td 59.259259 Tz (removed ) Tj 2.644444 0 Td 57.523148 Tz (from ) Tj 1.575 0 Td 48.611111 Tz (the ) Tj 1.030556 0 Td 49.907407 Tz (tetrahydrofuran ) Tj 4.686111 0 Td 48.206019 Tz (solution ) Tj 2.45 0 Td 59.41358 Tz (and ) Tj 1.225 0 Td 61.574074 Tz (was ) Tj 1.283333 0 Td 53.472222 Tz (then ) Tj 51.428571 0 0 51.428571 0 212.294046 Tm 6.358333 0 Td 49.691358 Tz (rinsed ) Tj 1.963889 0 Td 53.472222 Tz (with ) Tj 1.458333 0 Td 48.070988 Tz (water. ) Tj 1.905556 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 47.530864 Tz (substrate ) Tj 2.741667 0 Td 60.493827 Tz (was ) Tj 1.302778 0 Td 54.79798 Tz (immediately ) Tj 3.791667 0 Td 60.277778 Tz (blown ) Tj 2.002778 0 Td 54.012346 Tz (dry ) Tj 51.428571 0 0 51.428571 0 171.97558 Tm 6.358333 0 Td 45.37037 Tz (in ) Tj 0.7 0 Td 58.333333 Tz (a ) Tj 0.486111 0 Td 52.932099 Tz (stream ) Tj 2.1 0 Td 53.472222 Tz (of ) Tj 0.719444 0 Td 50.231481 Tz (argon. ) Tj 1.944444 0 Td 63.734568 Tz (The ) Tj 1.263889 0 Td 58.333333 Tz (above ) Tj 1.866667 0 Td 54.372428 Tz (procedure ) Tj 3.091667 0 Td 61.574074 Tz (was ) Tj 1.263889 0 Td 51.446759 Tz (repeated ) Tj 2.605556 0 Td 58.333333 Tz (up ) Tj 0.855556 0 Td 46.990741 Tz (to ) Tj 30 0 0 30 0 2755 Tm 41.833333 0 Td 72.222222 Tz (5 ) Tj 30 0 0 30 0 2547 Tm 41.666667 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.666667 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.6 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.6 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.6 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.566667 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.566667 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.6 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.6 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.633333 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.633333 0 Td 75 Tz (65 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.881081 0 Td 72.522523 Tz (8 ) Tj 51.428571 0 0 51.428571 0 2914.138462 Tm 25.297222 0 Td 51.851852 Tz (four ) Tj 1.497222 0 Td 51.203704 Tz (times ) Tj 1.847222 0 Td 43.75 Tz (to ) Tj 0.797222 0 Td 49.074074 Tz (control ) Tj 2.333333 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 49.331276 Tz (thickness ) Tj 2.916667 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 51.388889 Tz (coating ) Tj 2.411111 0 Td 58.333333 Tz (between ) Tj 40 0 0 40 0 2880 Tm 32.525 0 Td 70 Tz (about ) Tj 2.3 0 Td 76.388889 Tz (one ) Tj 1.575 0 Td 75 Tz (and ) Tj 1.625 0 Td 57.291667 Tz (five ) Tj 1.65 0 Td 67.80303 Tz (nanometers. ) Tj 40 0 0 40 0 2826 Tm 33.45 0 Td 85.416667 Tz (What ) Tj 2.275 0 Td 50 Tz (is ) Tj 0.85 0 Td 70.833333 Tz (claimed ) Tj 3.2 0 Td 45.833333 Tz (is: ) Tj 51.428571 0 0 51.428571 0 2780.279835 Tm 26.036111 0 Td 42.12963 Tz (1. ) Tj 0.680556 0 Td 87.5 Tz (A ) Tj 0.719444 0 Td 63.599537 Tz (compound ) Tj 3.208333 0 Td 55.632716 Tz (having ) Tj 2.158333 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 51.041667 Tz (formula: ) Tj 51.428571 0 0 51.428571 0 2650 Tm 33.969444 0 Td 89.12037 Tz (21 ) Tj 31.428571 0 0 31.428571 0 2214 Tm 54.536364 0 Td 90.151515 Tz (HS ) Tj 51.428571 0 0 51.428571 0 2111.021314 Tm 26.016667 0 Td 43.75 Tz (2. ) Tj 0.7 0 Td 87.5 Tz (A ) Tj 0.7 0 Td 58.333333 Tz (polymer ) Tj 2.625 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 63.599537 Tz (compound ) Tj 3.227778 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 53.796296 Tz (claim ) Tj 1.827778 0 Td 42.12963 Tz (1. ) Tj 51.428571 0 0 51.428571 0 2067.830769 Tm 26.016667 0 Td 43.75 Tz (3. ) Tj 0.836111 0 Td 62.654321 Tz (The ) Tj 1.419444 0 Td 58.333333 Tz (polymer ) Tj 2.722222 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 53.148148 Tz (claim ) Tj 1.925 0 Td 42.12963 Tz (2, ) Tj 0.836111 0 Td 55.092593 Tz (wherein ) Tj 2.644444 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 58.796296 Tz (polymer ) Tj 2.722222 0 Td 54.012346 Tz (has ) Tj 1.244444 0 Td 58.333333 Tz (a ) Tj 40 0 0 40 0 2031 Tm 32.5 0 Td 64.814815 Tz (thickness ) Tj 3.75 0 Td 75 Tz (of ) Tj 1 0 Td 75 Tz (from ) Tj 2.05 0 Td 70 Tz (about ) Tj 2.425 0 Td 45.833333 Tz (1 ) Tj 0.6 0 Td 58.333333 Tz (to ) Tj 0.95 0 Td 70 Tz (about ) Tj 2.425 0 Td 70.833333 Tz (10 ) Tj 1.1 0 Td 67.80303 Tz (nanometers. ) Tj 51.428571 0 0 51.428571 0 1986.351421 Tm 26.016667 0 Td 43.75 Tz (4. ) Tj 0.680556 0 Td 87.5 Tz (A ) Tj 0.738889 0 Td 58.873457 Tz (method ) Tj 2.333333 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 53.06713 Tz (applying ) Tj 2.702778 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 63.599537 Tz (compound ) Tj 3.208333 0 Td 46.990741 Tz (to ) Tj 0.738889 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 49.151235 Tz (metal, ) Tj 1.944444 0 Td 61.574074 Tz (compris ) Tj 38.571429 0 0 38.571429 0 1946 Tm 33.72963 0 Td 60.493827 Tz (1ng: ) Tj 51.428571 0 0 51.428571 0 1904.678392 Tm 26.016667 0 Td 52.572016 Tz (providing ) Tj 3.033333 0 Td 52.225783 Tz (4-vinylbenzenepropanethiol ) Tj 8.361111 0 Td 48.611111 Tz (as ) Tj 0.797222 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 48.611111 Tz (solution ) Tj 2.566667 0 Td 43.75 Tz (in ) Tj 0.758333 0 Td 58.333333 Tz (an ) Tj 51.428571 0 0 51.428571 0 1860.894737 Tm 26.755556 0 Td 51.388889 Tz (organic ) Tj 2.333333 0 Td 47.395833 Tz (solvent; ) Tj 51.428571 0 0 51.428571 0 1820.580392 Tm 26.016667 0 Td 52.572016 Tz (providing ) Tj 2.994444 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 49.151235 Tz (metal; ) Tj 51.428571 0 0 51.428571 0 1778.247694 Tm 26.016667 0 Td 51.388889 Tz (placing ) Tj 2.430556 0 Td 49.691358 Tz (the ) Tj 1.205556 0 Td 52.5 Tz (metal ) Tj 1.886111 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 49.691358 Tz (the ) Tj 1.186111 0 Td 48.206019 Tz (Solution ) Tj 2.625 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 55.664488 Tz (4-vinylbenzenepro ) Tj 51.428571 0 0 51.428571 0 1733.488621 Tm 26.755556 0 Td 50.05144 Tz (panethiol ) Tj 2.858333 0 Td 51.851852 Tz (so ) Tj 0.777778 0 Td 45.37037 Tz (that ) Tj 1.225 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 47.800926 Tz (solution ) Tj 2.45 0 Td 40.509259 Tz (is ) Tj 0.622222 0 Td 46.990741 Tz (in ) Tj 0.7 0 Td 50.462963 Tz (contact ) Tj 2.255556 0 Td 53.472222 Tz (with ) Tj 1.419444 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 52.5 Tz (metal ) Tj 48.571429 0 0 48.571429 0 1693 Tm 28.35 0 Td 49.32598 Tz (Surface; ) Tj 51.428571 0 0 51.428571 0 1650.73913 Tm 26.016667 0 Td 54.6875 Tz (exposing ) Tj 2.780556 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 53.703704 Tz (mixture ) Tj 2.430556 0 Td 46.990741 Tz (to ) Tj 0.758333 0 Td 45.075758 Tz (ultraviolet ) Tj 3.15 0 Td 45.694444 Tz (radiation. ) Tj 51.428571 0 0 51.428571 0 1608.390863 Tm 26.016667 0 Td 43.75 Tz (5. ) Tj 0.680556 0 Td 64.814815 Tz (The ) Tj 1.302778 0 Td 59.953704 Tz (method ) Tj 2.275 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 53.148148 Tz (claim ) Tj 1.75 0 Td 45.37037 Tz (4, ) Tj 0.719444 0 Td 55.092593 Tz (wherein ) Tj 2.45 0 Td 55.497685 Tz (exposing ) Tj 2.780556 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 53.240741 Tz (mixture ) Tj 2.391667 0 Td 43.75 Tz (to ) Tj 51.428571 0 0 51.428571 0 1567.724014 Tm 25.277778 0 Td 45.664983 Tz (ultraviolet ) Tj 3.208333 0 Td 47.530864 Tz (radiation ) Tj 2.780556 0 Td 47.685185 Tz (further ) Tj 2.197222 0 Td 54.012346 Tz (comprises ) Tj 3.130556 0 Td 54.6875 Tz (exposing ) Tj 2.8 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 53.240741 Tz (mixture ) Tj 51.428571 0 0 51.428571 0 1526.56872 Tm 25.277778 0 Td 45.37037 Tz (to ) Tj 0.719444 0 Td 44.781145 Tz (ultraviolet ) Tj 3.111111 0 Td 47.170782 Tz (radiation ) Tj 2.644444 0 Td 55.092593 Tz (having ) Tj 2.061111 0 Td 58.333333 Tz (a ) Tj 0.447222 0 Td 54.768519 Tz (wavelength ) Tj 3.441667 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 55.902778 Tz (from ) Tj 1.477778 0 Td 54.444444 Tz (about ) Tj 1.730556 0 Td 60.493827 Tz (200 ) Tj 40 0 0 40 0 1490 Tm 32.575 0 Td 70.833333 Tz (nanometers ) Tj 4.525 0 Td 60.416667 Tz (to ) Tj 1 0 Td 70 Tz (about ) Tj 2.35 0 Td 79.166667 Tz (300 ) Tj 1.675 0 Td 71.25 Tz (nanometers ) Tj 4.6 0 Td 61.111111 Tz (for ) Tj 1.325 0 Td 70.833333 Tz (a ) Tj 0.675 0 Td 64.583333 Tz (duration ) Tj 3.425 0 Td 70.833333 Tz (of ) Tj 1.025 0 Td 75 Tz (from ) Tj 40 0 0 40 0 1448 Tm 32.525 0 Td 70 Tz (about ) Tj 2.375 0 Td 75 Tz (10 ) Tj 1.125 0 Td 69.642857 Tz (minutes ) Tj 3.2 0 Td 56.25 Tz (to ) Tj 0.925 0 Td 70 Tz (about ) Tj 2.4 0 Td 50 Tz (1 ) Tj 0.625 0 Td 62.5 Tz (hour. ) Tj 51.428571 0 0 51.428571 0 1400.389527 Tm 26.036111 0 Td 42.12963 Tz (6. ) Tj 0.661111 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 59.41358 Tz (method ) Tj 2.255556 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 53.148148 Tz (claim ) Tj 1.75 0 Td 45.37037 Tz (5, ) Tj 0.719444 0 Td 55.092593 Tz (wherein ) Tj 2.45 0 Td 55.092593 Tz (exposing ) Tj 2.8 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 53.240741 Tz (mixture ) Tj 2.391667 0 Td 43.75 Tz (to ) Tj 51.428571 0 0 51.428571 0 1359.724014 Tm 25.277778 0 Td 45.664983 Tz (ultraviolet ) Tj 3.208333 0 Td 47.530864 Tz (radiation ) Tj 2.780556 0 Td 47.685185 Tz (further ) Tj 2.197222 0 Td 54.012346 Tz (comprises ) Tj 3.130556 0 Td 54.6875 Tz (exposing ) Tj 2.8 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 53.240741 Tz (mixture ) Tj 51.428571 0 0 51.428571 0 1318.807742 Tm 25.277778 0 Td 45.37037 Tz (to ) Tj 0.894444 0 Td 45.075758 Tz (ultraviolet ) Tj 3.305556 0 Td 46.8107 Tz (radiation ) Tj 2.838889 0 Td 55.092593 Tz (having ) Tj 2.255556 0 Td 55.092593 Tz (a ) Tj 0.641667 0 Td 55.092593 Tz (wavelength ) Tj 3.616667 0 Td 59.953704 Tz (of ) Tj 0.913889 0 Td 54.444444 Tz (about ) Tj 1.925 0 Td 58.333333 Tz (255 ) Tj 40 0 0 40 0 1282 Tm 32.575 0 Td 70.833333 Tz (nanometers ) Tj 4.475 0 Td 62.5 Tz (for ) Tj 1.275 0 Td 75 Tz (a ) Tj 0.675 0 Td 63.541667 Tz (duration ) Tj 3.325 0 Td 75 Tz (of ) Tj 1 0 Td 73.958333 Tz (from ) Tj 2.025 0 Td 69.166667 Tz (about ) Tj 2.35 0 Td 75 Tz (10 ) Tj 1.1 0 Td 69.642857 Tz (minutes ) Tj 3.175 0 Td 58.333333 Tz (to ) Tj 0.9 0 Td 70.833333 Tz (about ) Tj 40 0 0 40 0 1241 Tm 32.6 0 Td 50 Tz (1 ) Tj 0.625 0 Td 62.5 Tz (hour. ) Tj 48.571429 0 0 48.571429 0 1193 Tm 27.547059 0 Td 46.323529 Tz (7. ) Tj 0.802941 0 Td 68.627451 Tz (The ) Tj 1.523529 0 Td 63.480392 Tz (method ) Tj 2.532353 0 Td 61.764706 Tz (of ) Tj 0.905882 0 Td 56.27451 Tz (claim ) Tj 1.997059 0 Td 44.607843 Tz (6, ) Tj 0.823529 0 Td 57.843137 Tz (wherein ) Tj 2.717647 0 Td 52.614379 Tz (the ) Tj 1.214706 0 Td 56.27451 Tz (metal ) Tj 1.955882 0 Td 41.176471 Tz (is ) Tj 0.782353 0 Td 51.89951 Tz (selected ) Tj 51.428571 0 0 51.428571 0 1154.579336 Tm 25.297222 0 Td 58.333333 Tz (from ) Tj 1.594444 0 Td 55.092593 Tz (a ) Tj 0.486111 0 Td 57.037037 Tz (group ) Tj 1.925 0 Td 48.935185 Tz (consisting ) Tj 3.130556 0 Td 55.092593 Tz (of ) Tj 0.758333 0 Td 50.925926 Tz (copper, ) Tj 2.294444 0 Td 49.259259 Tz (gold, ) Tj 1.691667 0 Td 51.131687 Tz (platinum, ) Tj 2.936111 0 Td 60.493827 Tz (and ) Tj 1.263889 0 Td 43.425926 Tz (iron. ) Tj 51.428571 0 0 51.428571 0 1110.351421 Tm 26.016667 0 Td 43.75 Tz (8. ) Tj 0.680556 0 Td 87.5 Tz (A ) Tj 0.738889 0 Td 58.873457 Tz (method ) Tj 2.333333 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 53.06713 Tz (applying ) Tj 2.702778 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 63.599537 Tz (compound ) Tj 3.208333 0 Td 46.990741 Tz (to ) Tj 0.738889 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 49.151235 Tz (metal, ) Tj 1.944444 0 Td 61.574074 Tz (compris ) Tj 38.571429 0 0 38.571429 0 1070 Tm 33.72963 0 Td 60.493827 Tz (1ng: ) Tj 51.428571 0 0 51.428571 0 1029 Tm 26.016667 0 Td 52.572016 Tz (providing ) Tj 3.013889 0 Td 51.371742 Tz (4-vinylbenzenepropanethiol: ) Tj 51.428571 0 0 51.428571 0 980.025907 Tm 26.016667 0 Td 52.572016 Tz (providing ) Tj 2.994444 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 51.851852 Tz (metal ) Tj 1.788889 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 52.777778 Tz (hexane: ) Tj 51.428571 0 0 51.428571 0 938.139394 Tm 26.016667 0 Td 51.388889 Tz (placing ) Tj 2.255556 0 Td 50.771605 Tz (the ) Tj 1.030556 0 Td 52.225783 Tz (4-vinylbenzenepropanethiol ) Tj 8.302778 0 Td 43.75 Tz (in ) Tj 0.661111 0 Td 50.771605 Tz (the ) Tj 1.011111 0 Td 58.333333 Tz (hexane ) Tj 2.197222 0 Td 53.472222 Tz (with ) Tj 51.428571 0 0 51.428571 0 893.717602 Tm 26.736111 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 52.5 Tz (metal ) Tj 1.75 0 Td 46.990741 Tz (in ) Tj 0.758333 0 Td 51.851852 Tz (order ) Tj 1.711111 0 Td 48.611111 Tz (to ) Tj 0.758333 0 Td 51.388889 Tz (prepare ) Tj 2.352778 0 Td 51.851852 Tz (a ) Tj 0.544444 0 Td 49.826389 Tz (mixture; ) Tj 51.428571 0 0 51.428571 0 850.432877 Tm 26.016667 0 Td 55.632716 Tz (adding ) Tj 2.294444 0 Td 58.333333 Tz (a ) Tj 0.661111 0 Td 52.777778 Tz (thermal ) Tj 2.547222 0 Td 46.990741 Tz (free ) Tj 1.458333 0 Td 46.759259 Tz (radical ) Tj 2.294444 0 Td 42.849794 Tz (initiator ) Tj 2.625 0 Td 54.282407 Tz (Such ) Tj 1.633333 0 Td 50.231481 Tz (as ) Tj 0.913889 0 Td 55.092593 Tz (benzoyl ) Tj 51.428571 0 0 51.428571 0 809.214724 Tm 26.755556 0 Td 53.06713 Tz (peroxide ) Tj 2.741667 0 Td 43.75 Tz (to ) Tj 0.758333 0 Td 48.611111 Tz (the ) Tj 1.088889 0 Td 49.826389 Tz (mixture; ) Tj 51.428571 0 0 51.428571 0 765.764557 Tm 26.016667 0 Td 51.851852 Tz (incubating ) Tj 3.247222 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 53.240741 Tz (mixture ) Tj 2.372222 0 Td 43.75 Tz (at ) Tj 0.680556 0 Td 57.523148 Tz (from ) Tj 1.555556 0 Td 53.796296 Tz (about ) Tj 1.769444 0 Td 61.574074 Tz (50 ) Tj 0.855556 0 Td 52.314815 Tz (degrees ) Tj 2.333333 0 Td 51.388889 Tz (Celsius ) Tj 2.333333 0 Td 43.75 Tz (to ) Tj 51.428571 0 0 51.428571 0 723.538244 Tm 26.755556 0 Td 54.444444 Tz (about ) Tj 1.788889 0 Td 63.194444 Tz (90 ) Tj 0.933333 0 Td 51.851852 Tz (degrees ) Tj 2.372222 0 Td 47.800926 Tz (Celsius. ) Tj 51.428571 0 0 51.428571 0 679.610256 Tm 26.016667 0 Td 43.75 Tz (9. ) Tj 0.719444 0 Td 62.654321 Tz (The ) Tj 1.322222 0 Td 60.493827 Tz (method ) Tj 2.333333 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 52.5 Tz (claim ) Tj 1.769444 0 Td 46.990741 Tz (8, ) Tj 0.758333 0 Td 55.092593 Tz (wherein ) Tj 2.508333 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 50.87963 Tz (incubating ) Tj 3.247222 0 Td 53.703704 Tz (mixture ) Tj 51.428571 0 0 51.428571 0 639.126904 Tm 25.297222 0 Td 47.685185 Tz (further ) Tj 2.236111 0 Td 54.372428 Tz (comprises ) Tj 3.208333 0 Td 50.87963 Tz (incubating ) Tj 3.325 0 Td 47.530864 Tz (for ) Tj 1.088889 0 Td 57.523148 Tz (from ) Tj 1.633333 0 Td 54.444444 Tz (about ) Tj 1.944444 0 Td 53.472222 Tz (15 ) Tj 0.933333 0 Td 54.166667 Tz (minutes ) Tj 2.527778 0 Td 45.37037 Tz (to ) Tj 40 0 0 40 0 602 Tm 32.525 0 Td 70 Tz (about ) Tj 2.275 0 Td 81.25 Tz (24 ) Tj 1.175 0 Td 63.888889 Tz (hours. ) Tj 48.571429 0 0 48.571429 0 553 Tm 27.567647 0 Td 51.470588 Tz (10. ) Tj 1.070588 0 Td 66.339869 Tz (The ) Tj 1.358824 0 Td 62.908497 Tz (method ) Tj 2.388235 0 Td 58.333333 Tz (of ) Tj 0.782353 0 Td 57.352941 Tz (claim8, ) Tj 2.532353 0 Td 59.313725 Tz (wherein ) Tj 2.614706 0 Td 52.614379 Tz (the ) Tj 1.091176 0 Td 54.901961 Tz (thermal ) Tj 2.45 0 Td 50.612745 Tz (free ) Tj 1.297059 0 Td 50.490196 Tz (radical ) Tj 51.428571 0 0 51.428571 0 514.134328 Tm 25.297222 0 Td 43.209877 Tz (initiator ) Tj 2.488889 0 Td 38.888889 Tz (is ) Tj 0.641667 0 Td 55.092593 Tz (benzoyl ) Tj 2.488889 0 Td 50.05144 Tz (peroxide. ) Tj 51.428571 0 0 51.428571 0 470.27204 Tm 26.036111 0 Td 48.611111 Tz (11. ) Tj 0.991667 0 Td 90.740741 Tz (A ) Tj 0.7 0 Td 59.41358 Tz (method ) Tj 2.294444 0 Td 53.472222 Tz (of ) Tj 0.7 0 Td 53.472222 Tz (applying ) Tj 2.702778 0 Td 51.851852 Tz (a ) Tj 0.447222 0 Td 64.409722 Tz (compound ) Tj 3.208333 0 Td 46.990741 Tz (to ) Tj 0.680556 0 Td 58.333333 Tz (a ) Tj 0.505556 0 Td 49.151235 Tz (metal, ) Tj 1.905556 0 Td 61.574074 Tz (compris ) Tj 51.428571 0 0 51.428571 0 432 Tm 25.297222 0 Td 45.37037 Tz (ing: ) Tj 51.428571 0 0 51.428571 0 388 Tm 26.016667 0 Td 52.572016 Tz (providing ) Tj 3.013889 0 Td 51.371742 Tz (4-vinylbenzenepropanethiol: ) Tj 51.428571 0 0 51.428571 0 342.676093 Tm 26.016667 0 Td 54.6875 Tz (exposing ) Tj 2.877778 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 51.976496 Tz (4-vinylbenzenepropanethiol ) Tj 8.4 0 Td 48.611111 Tz (to ) Tj 0.855556 0 Td 45.37037 Tz (air ) Tj 1.05 0 Td 45.37037 Tz (at ) Tj 0.816667 0 Td 64.00463 Tz (room ) Tj 51.428571 0 0 51.428571 0 297.108346 Tm 26.736111 0 Td 53.030303 Tz (temperature ) Tj 3.85 0 Td 47.530864 Tz (for ) Tj 1.166667 0 Td 59.143519 Tz (from ) Tj 1.730556 0 Td 55.092593 Tz (about ) Tj 1.983333 0 Td 61.574074 Tz (30 ) Tj 1.108333 0 Td 53.703704 Tz (minutes ) Tj 2.605556 0 Td 45.37037 Tz (to ) Tj 0.894444 0 Td 53.796296 Tz (about ) Tj 1.963889 0 Td 58.333333 Tz (24 ) Tj 48.571429 0 0 48.571429 0 255 Tm 28.308824 0 Td 53.186275 Tz (hours; ) Tj 51.428571 0 0 51.428571 0 216.674787 Tm 26.016667 0 Td 47.395833 Tz (diluting ) Tj 2.430556 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 52.225783 Tz (4-vinylbenzenepropanethiol ) Tj 8.283333 0 Td 59.41358 Tz (and ) Tj 1.225 0 Td 37.808642 Tz (its ) Tj 0.855556 0 Td 53.652263 Tz (oligomers ) Tj 51.428571 0 0 51.428571 0 169.712062 Tm 26.755556 0 Td 45.37037 Tz (in ) Tj 0.719444 0 Td 58.333333 Tz (an ) Tj 0.913889 0 Td 50.925926 Tz (organic ) Tj 2.352778 0 Td 49.537037 Tz (solvent ) Tj 2.236111 0 Td 46.990741 Tz (to ) Tj 0.738889 0 Td 55.092593 Tz (about ) Tj 1.866667 0 Td 74.537037 Tz (1% ) Tj 1.108333 0 Td 59.143519 Tz (w/w: ) Tj ET Q endstream endobj 306 0 obj << /Length 1 >> stream q endstream endobj 307 0 obj << /Length 8791 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.325 0 Td 83.522727 Tz (US ) Tj 1.240909 0 Td 58.038721 Tz (7,829,155 ) Tj 3.388636 0 Td 68.939394 Tz (B1 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.472973 0 Td 72.522523 Tz (9 ) Tj 51.428571 0 0 51.428571 0 2916.630345 Tm 7.097222 0 Td 50.555556 Tz (contacting ) Tj 3.402778 0 Td 49.691358 Tz (the ) Tj 1.302778 0 Td 52.5 Tz (metal ) Tj 1.983333 0 Td 52.662037 Tz (with ) Tj 1.672222 0 Td 49.691358 Tz (the ) Tj 1.263889 0 Td 49.016204 Tz (solution ) Tj 2.702778 0 Td 59.953704 Tz (of ) Tj 1.030556 0 Td 56.064815 Tz (4-vinylben ) Tj 51.428571 0 0 51.428571 0 2876.587302 Tm 7.816667 0 Td 52.054398 Tz (Zenepropanethiol ) Tj 5.172222 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 36.728395 Tz (its ) Tj 0.855556 0 Td 51.203704 Tz (oligomers. ) Tj 51.428571 0 0 51.428571 0 2821.245658 Tm 7.136111 0 Td 46.450617 Tz (12. ) Tj 0.972222 0 Td 64.814815 Tz (The ) Tj 1.302778 0 Td 59.953704 Tz (method ) Tj 2.275 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 53.148148 Tz (claim ) Tj 1.769444 0 Td 48.611111 Tz (11, ) Tj 1.030556 0 Td 47.685185 Tz (further ) Tj 2.1 0 Td 54.768519 Tz (comprising ) Tj 3.422222 0 Td 51.203704 Tz (incubating ) Tj 51.428571 0 0 51.428571 0 2780.073082 Tm 6.338889 0 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) Tj 51.428571 0 0 51.428571 0 2647.024067 Tm 6.358333 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 48.611111 Tz (solution ) Tj 2.527778 0 Td 61.574074 Tz (of ) Tj 0.836111 0 Td 52.10114 Tz (4-vinylbenzenepropanethiol ) Tj 8.341667 0 Td 40.509259 Tz (is ) Tj 0.680556 0 Td 58.333333 Tz (from ) Tj 1.613889 0 Td 54.444444 Tz (about ) Tj 40 0 0 40 0 2609 Tm 8.25 0 Td 75 Tz (10 ) Tj 1.1 0 Td 70.238095 Tz (seconds ) Tj 3.225 0 Td 56.25 Tz (to ) Tj 0.925 0 Td 70 Tz (about ) Tj 2.3 0 Td 81.25 Tz (30 ) Tj 1.2 0 Td 65.625 Tz (minutes. ) Tj 51.428571 0 0 51.428571 0 2556.703704 Tm 7.116667 0 Td 47.530864 Tz (14. ) Tj 1.244444 0 Td 87.5 Tz (A ) Tj 0.972222 0 Td 59.953704 Tz (method ) Tj 2.566667 0 Td 56.712963 Tz (of ) Tj 1.030556 0 Td 59.953704 Tz (making ) Tj 2.547222 0 Td 51.371742 Tz (4-vinylbenzenepropanethiol, ) Tj 38.571429 0 0 38.571429 0 2516 Tm 8.477778 0 Td 69.135802 Tz (compr1S1ng: ) Tj 51.428571 0 0 51.428571 0 2468 Tm 7.097222 0 Td 52.211934 Tz (providing ) Tj 3.052778 0 Td 55.233494 Tz (1-bromo-3-phenylpropane ) Tj 51.428571 0 0 51.428571 0 2412.983655 Tm 7.097222 0 Td 54.552469 Tz (adding ) Tj 2.158333 0 Td 46.450617 Tz (acetic ) Tj 1.866667 0 Td 54.012346 Tz (anhydride ) Tj 3.091667 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 61.168981 Tz (aluminum ) Tj 3.15 0 Td 47.170782 Tz (chloride; ) Tj 51.428571 0 0 51.428571 0 2361.787836 Tm 7.097222 0 Td 51.203704 Tz (incubating ) Tj 3.402778 0 Td 48.611111 Tz (the ) Tj 1.244444 0 Td 52.777778 Tz (mixture ) Tj 2.547222 0 Td 43.75 Tz (at ) Tj 0.836111 0 Td 57.523148 Tz (from ) Tj 1.730556 0 Td 54.444444 Tz (about ) Tj 1.983333 0 Td 62.654321 Tz (-20 ) Tj 1.438889 0 Td 45.37037 Tz (to ) Tj 0.855556 0 Td 55.092593 Tz (about ) Tj 1.983333 0 Td 59.953704 Tz (20 ) Tj 51.428571 0 0 51.428571 0 2320.213423 Tm 7.816667 0 Td 52.314815 Tz (degrees ) Tj 2.333333 0 Td 50.925926 Tz (Celsius ) Tj 2.313889 0 Td 47.530864 Tz (for ) Tj 0.972222 0 Td 57.523148 Tz (from ) Tj 1.536111 0 Td 55.092593 Tz (about ) Tj 1.808333 0 Td 38.888889 Tz (1 ) Tj 0.447222 0 Td 56.712963 Tz (hour ) Tj 1.458333 0 Td 46.990741 Tz (to ) Tj 0.7 0 Td 54.444444 Tz (about ) Tj 1.808333 0 Td 55.092593 Tz (12 ) Tj 0.797222 0 Td 50.231481 Tz (hours; ) Tj 51.428571 0 0 51.428571 0 2276.541147 Tm 7.097222 0 Td 46.090535 Tz (isolating ) Tj 2.683333 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 46.8107 Tz (resulting ) Tj 2.683333 0 Td 53.796296 Tz (p-\(3-bromopropyl\)acetophenone; ) Tj 30 0 0 30 0 2547 Tm 41.666667 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.666667 0 Td 72.222222 Tz (15 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.672973 0 Td 74.099099 Tz (10 ) Tj 51.428571 0 0 51.428571 0 2919.165414 Tm 26.016667 0 Td 55.632716 Tz (adding ) Tj 2.236111 0 Td 58.873457 Tz (Sodium ) Tj 2.372222 0 Td 54.208754 Tz (borohydride ) Tj 3.811111 0 Td 45.37037 Tz (to ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 55.945419 Tz (p-\(3-bromopropyl\)ac ) Tj 51.428571 0 0 51.428571 0 2874.969957 Tm 26.755556 0 Td 56.064815 Tz 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